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Entry  Friday, June 20, 2014, 12:01, Laura Lambert, SiC, 39530-8, HP-FEBIAD, In progress, Conditioning SiC#31 target 
    Reply  Friday, June 20, 2014, 16:22, John Wong, SiC, 39530-8, HP-FEBIAD, In progress, Conditioning SiC#31 target 
       Reply  Monday, June 23, 2014, 09:47, Laura Lambert, SiC, 39530-8, HP-FEBIAD, In progress, Conditioning SiC#31 target current_vs_temp.jpeg
          Reply  Tuesday, June 24, 2014, 23:57, John Wong, SiC, 39530-8, HP-FEBIAD, In progress, Conditioning SiC#31 target 2014-06-24_16.57.17.jpg
Message ID: 141     Entry time: Monday, June 23, 2014, 09:47     In reply to: 140     Reply to this: 142
Author: Laura Lambert 
Target Material: SiC 
Target Oven W.O#: 39530-8 
Source: HP-FEBIAD 
Status: In progress 
Subject: Conditioning SiC#31 target 

John Wong wrote:

Laura Lambert wrote:

 Friday, June 20, 2014, 11:14

Total number of foils: 515 discs

Total mass of materials [incl graphite foils]: 64.7224g

Total length packed: 17.8cm

Container is wrapped with 3x Ta-heat shields.

Currently being pumped down.


 Friday, June 20, 2014, 14:56

HS cooling water valves opened, no leaks detected.

IGP1 = 6.2e-6 Torr

TGHT max = 820A/ 17V

TBHT max = 300A/ 5V

Stepping up manually to 40A


 Friday, June 20, 2014, 16:04

IGP1 = 8e-6 Torr

Slowly stepped up to 35A manually.

Vacuum has stabilized.

Initiating auto-ramp at 0.1A/min


 

 Friday, June 20, 2014, 16:16

Changing the heating current... 

From the previous SiC targets, TGHT was ramped up to 800A and yellow crystals were found; the end caps and target legs were also found broken (see my iPad).  This might be too hot for the Ta-boat to handle the sintering process. 

For this process,

TGHT will ramp up to 600A and TBHT to 230A over the weekend. 

Then, the temperature will be measured.  The sintering temperature of SiC is ~1800 - 2000C. 


 

 Monday, June 23, 2014, 09:45

IGP1 = 5e-6 Torr

TGHT and TBHT are at ~200A

Increasing ramping rate to 0.2A/min


 Monday, June 23, 2014, 11:19

IGP1 = 6.9e-6 Torr

Increasing ramping rate to 2.0A/min


Monday, June 23, 2014, 12:09

JW:  Pressure went up too fast... lower the TGHT ramping up rate to 1A/min.


 Tuesday, June 24, 2014, 16:06

Increasing current with respect to temperature: See attached table


 

Attachment 1: current_vs_temp.jpeg  2.759 MB  Uploaded Tuesday, June 24, 2014, 17:11  | Show | Hide all
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