Monday, January 11, 2016, 15:25
Small center block LP-SIS container previously sintered with TaC coating
3x Ta heat shields
Container is loaded with 260 discs of SiC with a total length of 8.5cm
Loaded into evap2 and pumped down this morning
HS water valves opened up, no leaks detected
Tapped up manually to 30A
Vacuum stable
IGP1 = 1e-6 Torr
Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively
Final setpoints: 400A for the TGHT and 230A for the TBHT
Final desired temperature: 1700C
Tuesday, January 12, 2016, 12:55
TGHT = 138A, TBHT = 80A
IGP1 = 7.7e-6 Torr.
Vacuum stable and coming down.
Increasing ramping rate to 0.5A/min and 0.2A/min for the TGHT and TBHT respectively.
Wednesday, January 13, 2016, 09:32
TGHT reached 400A ~11.5hrs ago
TBHT reached 230A ~8hrs ago
OMEGA = 1400C
IGP1 = 1.75e-7 Torr
Tapping up manually to 1700C...
Wednesday, January 13, 2016, 10:14
Previous temperature measurement of OMEGA = 1400C is wrong due to window port being coated with SiC [see attached photos]
Will remain at TGHT = 420A for 4hrs then cool down this afternoon
Wednesday, January 13, 2016, 14:29
Remained at max setpoints for 4.5hrs.
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Thursday, January 14, 2016, 09:47
Vented in air and opened up this morning
Target looks good
Will insert and expand endcaps this afternoon
|