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New entries since:Wed Dec 31 16:00:00 1969
ID Date Author Target Material Target Oven W.O# Source Status Subject
  110   Thursday, January 23, 2014, 16:22 Laura LambertEmpty40282-4TARGET BOATProblems resolvedSintering Ta target boat with TaC coating

John Wong wrote:

John Wong wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

 Wednesday, January 22, 2014, 18:09

After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2). 

Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN 

Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes. 

Maybe a fault in the water signal.  If it happens again, the water signal should be replaced.

Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK!

Chamber is a bit warm now.  Will allow time to cool down.

Will vent the chamber tomorrow and the boat will be inspected. 


 

 Thursday, January 23, 2014, 16:18

Chamber vented overnight and was opened up this morning.

Target boat not fully sintered [see attached photos].

Chamber currently being pumped down again in order to continue with sintering TaC coating.

HS cooling water valves were opened, no leaks detected.

Will ramp up to 700A again over the weekend.

Attachment 1: IMG_20140123_144725917.jpg
IMG_20140123_144725917.jpg
Attachment 2: IMG_20140123_144736614.jpg
IMG_20140123_144736614.jpg
  109   Wednesday, January 22, 2014, 18:22 John WongEmpty40282-4TARGET BOATProblemsSintering Ta target boat with TaC coating (IEVAP2:TBHT2 water signal problem)

John Wong wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

 Wednesday, January 22, 2014, 18:09

After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2). 

Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN 

Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes. 

Maybe a fault in the water signal.  If it happens again, the water signal should be replaced.

Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK!

Chamber is a bit warm now.  Will allow time to cool down.

Will vent the chamber tomorrow and the boat will be inspected. 


 

Attachment 1: Screen_Shot_2014-01-22_at_6.10.50_PM.png
Screen_Shot_2014-01-22_at_6.10.50_PM.png
Attachment 2: Targetboat_heatingup2.JPEG
Targetboat_heatingup2.JPEG
  108   Wednesday, January 22, 2014, 15:13 John WongEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Note: This is the "old" design boat.  The new design boat was able to heat up to 900A/16.88 - the temperature was measured at about 1500C.  (see elog: https://elog.triumf.ca/TIS/Evaporator_2/15)

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

  107   Wednesday, January 22, 2014, 13:46 Laura LambertEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

  106   Wednesday, January 22, 2014, 09:49 Laura LambertEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

  105   Tuesday, January 21, 2014, 11:56 Laura LambertEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

  104   Tuesday, January 21, 2014, 11:33 Laura LambertEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

  103   Monday, January 20, 2014, 16:35 Laura LambertEmptyTa-Target boat  Sintering Ta target boat with TaC coating

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

  102   Monday, January 20, 2014, 16:30 Laura LambertEmpty39165-9LP-SISDoneSintering TaC coating container

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

 Thursday, January 16, 2014, 11:35

Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.

TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.

Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.


 

 Friday, January 17, 2014, 09:28

TGHT/TBHT @ 300/200A.  TBHT voltage is limited at 3A.  

TGHT ramping rate increased to 2A/min.  Pressure @ 4.5e-7 Torr.  


 

 Friday, January 17, 2014, 10:14

TBHT stopped at 200A with voltage limit sitting at 3V.

Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.

IGP1 @ 5.0e-7 Torr

 Friday, January 17, 2014, 12:45

TGHT voltage limiting at 9.9V, and  current stayed at 560A.  Increased the TGHT voltage to 10.5V and continued ramping the heater up.

TGHT/TBHT stabilized at 850A (~10V) and 230A(3.6V). 

Pressure at 1.03e-6 Torr and coming down... 

Target will be heated until 5pm (4hrs) before cooling down at the ramping rate of 2A/min. 

Chamber will be vented in air, next week.


 Friday, January 17, 2014, 16:51

Auto-cooling initiated at 2A/min.

Vac @ 5.3e-7 Torr.


 

 

  101   Friday, January 17, 2014, 12:52 John WongEmpty39165-9LP-SISIn progressSintering TaC coating container

Laura Lambert wrote:

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

 Thursday, January 16, 2014, 11:35

Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.

TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.

Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.


 

 Friday, January 17, 2014, 09:28

TGHT/TBHT @ 300/200A.  TBHT voltage is limited at 3A.  

TGHT ramping rate increased to 2A/min.  Pressure @ 4.5e-7 Torr.  


 

 Friday, January 17, 2014, 10:14

TBHT stopped at 200A with voltage limit sitting at 3V.

Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.

IGP1 @ 5.0e-7 Torr

 Friday, January 17, 2014, 12:45

TGHT voltage limiting at 9.9V, and  current stayed at 560A.  Increased the TGHT voltage to 10.5V and continued ramping the heater up.

TGHT/TBHT stabilized at 580A (~10V) and 230A(3.6V). 

Pressure at 1.03e-6 Torr and coming down... 

Target will be heated until 5pm (4hrs) before cooling down at the ramping rate of 2A/min. 

Chamber will be vented in air, next week.


 Friday, January 17, 2014, 16:51

Auto-cooling initiated at 2A/min.

Vac @ 5.3e-7 Torr.


 

  100   Friday, January 17, 2014, 10:18 Laura LambertEmpty39165-9LP-SISIn progressSintering TaC coating container

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

 Thursday, January 16, 2014, 11:35

Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.

TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.

Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.


 

 Friday, January 17, 2014, 09:28

TGHT/TBHT @ 300/200A.  TBHT voltage is limited at 3A.  

TGHT ramping rate increased to 2A/min.  Pressure @ 4.5e-7 Torr.  


 

 Friday, January 17, 2014, 10:14

TBHT stopped at 200A with voltage limit sitting at 3V.

Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.

IGP1 @ 5.0e-7 Torr

  99   Friday, January 17, 2014, 09:34 John WongEmpty39165-9LP-SISIn progressSintering TaC coating container

Laura Lambert wrote:

John Wong wrote:

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

 Thursday, January 16, 2014, 11:35

Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.

TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.

Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.


 

 Friday, January 17, 2014, 09:28

TGHT/TBHT @ 300/200A.  TBHT voltage is limited at 3A.  

TGHT ramping rate increased to 2A/min.  Pressure @ 4.5e-7 Torr.  


 

  98   Thursday, January 16, 2014, 13:06 Laura LambertEmpty39165-9LP-SISIn progressSintering TaC coating container

John Wong wrote:

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

 Thursday, January 16, 2014, 11:35

Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.

TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.

Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.


 

  97   Wednesday, January 15, 2014, 17:45 John WongEmpty39165-9LP-SISIn progressSintering TaC coating container

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

  96   Thursday, November 07, 2013, 09:38 Anders Mjos   Problems resolvedHeat Shield cooling line twisted

See attached photo.

The Heat Shield has been taken to the Machine Shop for repair.

Friday, November 08, 2013

 The Heat Shield cooling line has been repaired and the lid re-installed in the evaporator. Photo attached.

Friday, November 08, 2013, 10:58 : Roughing Started

Friday, November 08, 2013, 11:05: Turbo started 

Friday, November 08, 2013, 11:15: Turbo at speed Vacuum at (IGP1) 5.7E-5 T 

Attachment 1: Twisted_Tube.jpg
Twisted_Tube.jpg
Attachment 2: Twisted_Tube_Repaired.jpg
Twisted_Tube_Repaired.jpg
  95   Wednesday, November 06, 2013, 17:36 John WongTaCTarget Boat #2 In progressTesting TaC matrix coating

The purpose of this experiment is to improve the TaC coating mixed with other metals as additives.  The coating solution will be sprayed on Ta metal (0.015" thick, same thickness as the target container).

The samples will be sintered at ~ 1800C.  Once the process is completed, a graphite tube will be inserted into the tube, and then re-heated it up to 1800C. 

This test will show how good the protective layer to prevent the graphite to react with the Ta metal.


Wednesday, November 06, 2013, 17:11

Step #1

Two samples: 

1.  A short tube (same diameter as the usual container)

2.  A cross section of the tube.

Both samples are coated with the TaC matrix spray: 

0.05 moles TaC

0.005 moles of Mo2C, VC, Cr3C2, NbC 

A Rh foil is used as a protective under layer.

see links for pictures:  https://www.dropbox.com/sh/866zsp44nnjeg2z/LqCThu-G_0

The target boat is wrapped with 3 layers of heat shields. 

Samples will be heated up to 600A ~1800C

Chamber is currently being pumped down.


 Friday, November 08, 2013, 17:13

Chamber was pumped down to ~2e-6 Torr.  HS water valve is opened and no leaks were detected. 

TGHT will be ramped up to 580A at 1A/min. 


Monday, November 11, 2013, 08:10  

TGHT has reached to 580A; samples has been heated at that current for over the weekend. 

IGP2 currently at 3.5e-7 Torr.

Auto cooling initiated, ramping rate at -2.0A/min.


 Step 2:

The coated tube is sintered with TaC-matrix.

The graphite tube is inserted in the tube and will be heated back up; see link for details:

https://www.dropbox.com/sh/ji0rhlj0v1tfj1w/cRv1I3VJXE

Chamber is currently pumped down to 1.8e-6 Torr.

TGHT will first be ramped up to 450A (1A/min) to see how the reaction behaves, then a caution ramp up to 600A will take place. 


 Friday, November 15, 2013, 11:04

TGHT reached to 450A.  Cooling down to 0A.  Chamber will be vented for inspection.


 Monday, November 18, 2013, 17:22

Continue Step#2:

The sample looks ok after heating at 450A.

Re-heating it to 500A. 

Chamber has been pumped down to 4.0e-6 Torr. 

Initiated auto-ramping...


 

  94   Monday, November 04, 2013, 14:02 Anders Mjos   MaintenanceBacking pump replaced

 

Anders Mjos wrote:

The source of the poor vacuum in the backing line seems to be related to a dirty filter. We will try to find a replacement filter next week.

The problem seem to have started September 17th, when backing preassure CG1A went from 40 mTorr to 130 mTorr. CG1B remained around 30 mTorr.

With the help of Anthony Ip from vacuum group, the problem was diagnosed to be the roughing pump itself. The pump was replaced and pumping improved. The chamber can now be evacuated and turbo ready to start in less than 10 minutes.

The filter is not stocked by vacuum group and could not be replaced.

Last week parts of the roughing line was cleaned by Rick. The PVC roughing line has been replaced with a SST bellows. The SST bellows is KF25 and should be replaced by a KF40 bellows in the long run.

  93   Friday, November 01, 2013, 17:20 Anders Mjos   ProblemsBacking pump needs new filter

The source of the poor vacuum in the backing line seems to be related to a dirty filter. We will try to find a replacement filter next week.

The problem seem to have started September 17th, when backing preassure CG1A went from 40 mTorr to 130 mTorr. CG1B remained around 30 mTorr.

  92   Tuesday, October 29, 2013, 15:50 Anders Mjos   In progressCopper bars on TGHT and TBHT

 Tuesday, October 29, 2013, 15:50: Pumping down

Wednesday, October 30, 2013, 09:32: Turbo started

Wednesday, October 30, 2013, 14:50: The Cu-bars were heated to 600A and 300A for TGHT and TBHT respectively.

Wednesday, October 30, 2013, 15:17: PS off. Turbo off.

Results can be found on DocuShare and in the attached plot.

Attachment 1: Current_and_Voltage.pdf
Current_and_Voltage.pdf
  91   Friday, October 04, 2013, 16:21 John WongEmpty LP-SISDoneSintering TaC coating on a LP target container to be used for C-grv tube test

Friday, October 04, 2013, 15:37

A LP target container is coated with TaC.  The container is wrapped with 3 layers to heat shield.  

This container will be used for the graphite tube test.  

Chamber is being pumped down.

 The HS cooling water valves are open and no leaks are detected. 


 

TGHT will be ramped up to 580A at 0.2A/min

TBHT will be ramped up to 230A at 0.2A/min.

The temperature will be monitored and measured. 


 Sunday, October 06, 2013, 19:55

 
TGHT and TBHT have reached to 580A/230A, respectively.  And the target has been heated for about 5 hours.  
 
The temperature inside the tube is measure at 1000C; this is much lower than expected as to previously measured at 1700C.
 
The temperature outside the container is at 1400C.

I'm suspecting the thermocouple inside the tube could be shorted.  
 
Cooling down the heaters down to zero at 2A/min for TGHT and 1A/min for TBHT. 
 
Tomorrow, the chamber will be vented and the target will be inspected.  
 
I like to re-adjust the thermocouple again, and re-heat the target back up, hoping to reach 1700C at TGHT = 580A.  

 Monday, October 07, 2013, 15:24
 
The sintering of the TaC coating is complete.
 
The chamber was vented this morning.  Apparently, there was a short in the thermocouple so the temperature measure was recorded much lower.
 
The thermocouples are adjusted, and the chamber is pumped down. 
 
Vac currently at 1.17e-6 Torr. 
 
TGHT and TBHT will be ramped up to 580A/230A at 2A/min. 
 
Continue monitoring the temperature...

 Monday, October 07, 2013, 16:13
 
TGHT and TBHT were ramped up to 90A.  Temperature inside the tube was measure just at 75C and the outside surface was at 207C.
Maybe the thermocouple is F up; will replace with a new one tomorrow.
Cooling down the target down...

Tuesday, October 22, 2013, 16:49

The target was heated up to 580A and the temperature inside the tube was measured to be ~1800C and the outside surface was ~1400C.

The target was cooled down.  Then the graphite tube was inserted.

There are two thermcouples inserted inside the tube on both ends.

Chamber has been pumped down to 4.33 e-7 Torr.  No leaks were detected.

Target will be heated up again to TGHT @ 580A / TBHT @ 230A at 0.2A/min.

The temperatures will be monitored.

T1 = left (floating)

T2 = right (toughing C-grv tube)

(wtf ionizer pointing into the page).


 Thursday, October 24, 2013, 16:35

TGHT/TBHT reached to 580A/230A. 

T1 = 1642C

T2 = Error?? Reading goes on/off intermittently, showing 900 - 1900C


Thursday, October 24, 2013, 16:45 

Ramping up TGHT to 680A to see if T1 can reach 1700C.

IG1 currently at 5.2e-7 Torr.


 Friday, October 25, 2013, 12:30

TGHT was ramped up to 632A (stopped due to voltage limiting). 

T1 was measured at 1960C.  Vac went up as it was heated up.  (see attachment #2)

Target was cooled down at 5A/min, now at 0A.

The chamber will be vented and the target will be inspected.

This run is complete.


 

Attachment 1: LP_C_grv_tempcurve.PNG
LP_C_grv_tempcurve.PNG
Attachment 2: LP_C_grv_TGHT632_1960C.PNG
LP_C_grv_TGHT632_1960C.PNG
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