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  Evaporator_2, Page 29 of 34  Not logged in ELOG logo
  ID Date Author Target Material Target Oven W.O# Source Status Subject
  119   Tuesday, February 25, 2014, 16:10 Laura Lambert 40282-3TARGET BOATDoneSintering TaC coated end caps

 Tuesday, February 25, 2014, 16:08

The target containers end-caps were coated with TaC spray and let dry.

The caps are inserted in the target boat vertically with no heat shield and no graphite foil. [see attached photo]

The chamber is currently being pumped down overnight.


 Wednesday, February 26, 2014, 09:54

Chamber was pumped down overnight to 4.2e-7 Torr.

HS cooling water valves opened; no leaks detected.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently at 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 700A.

Will ramp up to 700A rather than the usual 580A due to last round of endcaps not fully sintering at 580A with new target boat design.

Good vacuum: 3.00e-5 Torr; Bad vacuum: 4.00e-5 Torr.


 Thursday, February 27, 2014, 09:38

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.8e-7 Torr; TGHT = 311A, 4.3V

Stepping ramping rate up to 2.0A/min.


 Friday, February 28, 2014, 08:53

TGHT reached max setpoint of 700A yesterday evening.

Internal temp measured with Mikron = 1700C

IGP1 = 3e-7 Torr 

Power = 12.95V

Initiating auto-cooling at 2.0A/min.


 Monday, March 03, 2014, 11:46

Vented and opened chamber this morning.

End caps not fully sintered! 

See attached photo comparison of fully sintered [grey], partially sintered from this round [light green] and pre-sinter [dark green].

Will not bother re-sintering, as partial sinter is enough.


 

  118   Tuesday, February 18, 2014, 12:19 Laura LambertEmpty40282-3TARGET BOATDoneSintering Ta target boat with TaC coating

 Tuesday, February 18, 2014, 12:12

A new target boat was sprayed with TaC coating and let dry.
The target boat is NOT wrapped with Ta-heat shield.

Thermocouples have been attached to the target boat in order to monitor the internal temperature of the new target boat design. 

The boat was installed in Evap#2, chamber is currently being pumped down.


 Tuesday, February 18, 2014, 14:20

Chamber was pumped down this morning to 2.9e-6 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently at 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr; Bad vacuum: 4.00e-5 Torr.

Temperature reading on left: thermocouple touching edge of target boat; temperature reading on right: thermocouple floating in center of target boat.


 Wednesday, February 19, 2014, 09:11

TGHT has been slowly ramping up overnight at a rate of 0.2A/min

IGP1 = 3.9e-7 Torr, TGHT = 260A; stepping ramping rate up to 2.0A/min


 Wednesday, February 19, 2014, 15:25

IGP1 = 9.4e-7 Torr

Thermocouple T2 = 1267.8C

Internal temp measured with Mikron = 1600C

Increasing max setpoint to 720A due to previous not fully sintered new design of target boat.


 Thursday, February 20, 2014, 09:17

Thermocouple T2 = 1254.5C

Internal temp measured with Mikron = 1811C

IGP1 = 2.6e-7 Torr

Reached max setpoint yesterday evening.

Initiating auto-cooling at 2.0A/min.


 Friday, February 21, 2014, 10:47

Vented and opened chamber this morning.

Target boat not fully sintered. [see attached photos]

Close to a full sinter, and will re-sinter next week with endcaps, so will not re-sinter by itself.


 

  117   Tuesday, February 11, 2014, 13:49 Laura LambertEmpty38817-8HP-SISDoneSintering TaC coating container for TiC

 Tuesday, February 11, 2014, 13:43

Target container is coated with TaC and wrapped with 3-Ta heat shields.

TGHT and TBHT will be ramped up to 820A and 300A, respectively.

Ramping rate set to 0.2A/min.

Good vac = 3e-5 Torr, Bad vac = 4e-5 Torr.

Chamber currently being pumped down...


 Tuesday, February 11, 2014, 16:33

Chamber pumped down to 2e-6 Torr.

HS cooling water valves opened; no leaks detected.

Will step up in the a.m.


 Wednesday, February 12, 2014, 11:41

IGP1 = 1.5e-7 Torr

TGHT max voltage = 17.05V, TBHT max voltage = 5V

Stepped TGHT and TBHT up to 35A

Waited 1hr15 before vacuum stabilized/ started to drop.

Initiating auto-ramping.


 Thursday, February 13, 2014, 10:19

TBHT and TGHT have both reached 300A

IGP1 = 2.4e-7 Torr.

Increasing TGHT auto-ramp to 2.0A/min


 Friday, February 14, 2014, 08:58

TGHT reached 820A yesterday afternoon. Measured internal temp this morning at 1300C.

Initiated TGHT auto-cooling at 2.0A/min and TBHT at 1.0A/min.

IGP1 = 3.2e-7 Torr.


 Monday, February 17, 2014, 12:02

Cooled down friday. Vented this morning.

Container fully sintered, smooth run!


 

  116   Friday, January 31, 2014, 12:10 Laura LambertEmpty39165-10LP-SISDoneSintering TaC coating container for Ta?

 Friday, January 31, 2014, 11:28

Target container is coated with TaC.

The container is wrapped with 3 x Ta heat-shield.

Chamber was pumped down to 1.9e-7 Torr.

HS water valves were opened, no leak detected.

TGHT and TBHT were stepped up to 35A. Waited ~20min, current stabilized and vacuum starting to drop.

TGHT will be ramped up to 580A at 0.2A/min, max voltage = 11.05V.

TBHT will be ramped up to 230A at 0.2A/min, max volatge = 5V.

Initiating auto-ramping: Good Vac = 3.0e-5 Torr, Bad Vac = 4.0e-5 Torr.


 Monday, February 03, 2014, 10:21

TGHT reached 580A pver the weekend.

TBHT sitting at 1.4A, checked archive: never went over 1.6A. Aborted auto-ramp, re-starting auto ramp process for TBHT.

IGP1 = 1.6e-7 Torr.


 Monday, February 03, 2014, 15:23

TBHT running smoothly, must have been and electrical problem.

TBHT currently at 85A, vacuum has not changed, increasing TBHT auto-ramp to 2.0A/min


 Tuesday, February 04, 2014, 10:10

TBHT reached 230A yesterday pm. Measured temp this morning at 1800C.

Initiated TGHT/TBHT auto-cooling at 2.0A/min.


 Wednesday, February 05, 2014, 11:33

Chamber cooled down overnight, vented and opened up this morning.

Smooth run! Container fully sintered.

  115   Tuesday, January 28, 2014, 15:46 Laura Lambert 40282-4TARGET BOATFailedSintering TaC coated end caps

 Tuesday, January 28, 2014, 15:43

The target containers end-caps were coated with TaC spray and let dry.

Each cap is wrapped with a small piece of graphite foil and inserted in the target boat. [see attached photo]

The chamber is currently being pumped down overnight.


 Wednesday, January 29, 2014, 11:32

Chamber was pumped down to 1.6e-7 Torr overnight.

HS cooling water valve opened; no leaks detected.

TGHT was stepped up to 35A, voltage max set at 11.05V. TBHT currently at 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 580A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 Thursday, January 30, 2014, 09:06

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.4e-7 Torr, TGHT = 283A; stepping ramping rate up to 2.0A/min.


 Thursday, January 30, 2014, 15:53

TGHT reached 580A at 11:45. Measured temp @1650C.

Initiating TGHT auto-cooling now at 2.0A/min.


 Friday, January 31, 2014, 09:04

Chamber cooled down overnight, vented and opened this morning.

Smooth run!


 Friday, January 31, 2014, 11:21

Opened up the end caps, turns out it wasn't such a smooth run...they're not fully sintered 

See attached photo comparison between fully sintered end cap [silver] and end cap from this run [green].

Will re-install and re-sinter next week.


 Wednesday, February 05, 2014, 11:34

End-caps re-installed into EVAP2

Target boat is wrapped with 3 x Ta heat-shield.

Chamber is currently being pumped down.


 Wednesday, February 05, 2014, 14:31

Chamber was pumped down to 5e-7 Torr this morning.

HS cooling water valve opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 11.05V. TBHT currently at 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 580A.

Good Vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 Thursday, February 06, 2014, 09:06

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 1.1e-7 Torr, TGHT = 259A; stepping ramping rate up to 2.0A/min.


 Friday, February 07, 2014, 10:10

TGHT reached 580A yesterday. Measured internal temp @ 1500C.

Initiated TGHT auto-cooling this morning at 2.0A/min


 Tuesday, February 11, 2014, 13:30

Vented and opened chamber this morning.

Endcaps are toast  [see pictures attached]

Some of the endcaps broke/fried, others deformed-none useable.

Possibly due to new target boat resulting in more current?

Too much heat with Ta heat shields?

Bad News Bears 


 

  114   Tuesday, January 28, 2014, 13:09 Laura LambertEmpty40282-4TARGET BOATDoneSintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

John Wong wrote:

John Wong wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

 Wednesday, January 22, 2014, 18:09

After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2). 

Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN 

Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes. 

Maybe a fault in the water signal.  If it happens again, the water signal should be replaced.

Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK!

Chamber is a bit warm now.  Will allow time to cool down.

Will vent the chamber tomorrow and the boat will be inspected. 


 

 Thursday, January 23, 2014, 16:18

Chamber vented overnight and was opened up this morning.

Target boat not fully sintered [see attached photos].

Chamber currently being pumped down again in order to continue with sintering TaC coating.

HS cooling water valves were opened, no leaks detected.

Will ramp up to 700A again over the weekend.

 Friday, January 24, 2014, 14:21

Chamber was pumped down to 1.7e-7 Torr.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A.

Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.


 

 Monday, January 27, 2014, 10:05

TGHT reached 700A over the weekend. Measured temp @ 2000C.

TGHT auto-cool inititated at 2.0A/min.


 

 Tuesday, January 28, 2014, 11:53

Chamber cooled down overnight, vented and opened up this morning.

Target boat still has a strip of green, still not fully sintered! [see attached photos].

Chamber currently being pumped down again to attempt sintering - round 3.


 

 Tuesday, January 28, 2014, 13:06

Discussed with Peter. Instead of re-sintering the whole boat by itself, end caps will be inserted for sintering and will be placed further down the boat where the sintering process appears complete.


 

  113   Tuesday, January 28, 2014, 11:57 Laura LambertEmpty40282-4TARGET BOATIn progressSintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

John Wong wrote:

John Wong wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

 Wednesday, January 22, 2014, 18:09

After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2). 

Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN 

Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes. 

Maybe a fault in the water signal.  If it happens again, the water signal should be replaced.

Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK!

Chamber is a bit warm now.  Will allow time to cool down.

Will vent the chamber tomorrow and the boat will be inspected. 


 

 Thursday, January 23, 2014, 16:18

Chamber vented overnight and was opened up this morning.

Target boat not fully sintered [see attached photos].

Chamber currently being pumped down again in order to continue with sintering TaC coating.

HS cooling water valves were opened, no leaks detected.

Will ramp up to 700A again over the weekend.

 Friday, January 24, 2014, 14:21

Chamber was pumped down to 1.7e-7 Torr.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A.

Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.


 

 Monday, January 27, 2014, 10:05

TGHT reached 700A over the weekend. Measured temp @ 2000C.

TGHT auto-cool inititated at 2.0A/min.


 

 Tuesday, January 28, 2014, 11:53

Chamber cooled down overnight, vented and opened up this morning.

Target boat still has a strip of green, still not fully sintered! [see attached photos].

Chamber currently being pumped down again to attempt sintering - round 3.


 

  112   Monday, January 27, 2014, 10:59 Laura LambertEmpty40282-4TARGET BOATIn progressSintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

John Wong wrote:

John Wong wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

 Wednesday, January 22, 2014, 18:09

After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2). 

Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN 

Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes. 

Maybe a fault in the water signal.  If it happens again, the water signal should be replaced.

Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK!

Chamber is a bit warm now.  Will allow time to cool down.

Will vent the chamber tomorrow and the boat will be inspected. 


 

 Thursday, January 23, 2014, 16:18

Chamber vented overnight and was opened up this morning.

Target boat not fully sintered [see attached photos].

Chamber currently being pumped down again in order to continue with sintering TaC coating.

HS cooling water valves were opened, no leaks detected.

Will ramp up to 700A again over the weekend.

 Friday, January 24, 2014, 14:21

Chamber was pumped down to 1.7e-7 Torr.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A.

Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.


 

 Monday, January 27, 2014, 10:05

TGHT reached 700A over the weekend. Measured temp @ 2000C.

TGHT auto-cool inititated at 2.0A/min.


 

  111   Friday, January 24, 2014, 14:25 Laura LambertEmpty40282-4TARGET BOATIn progressSintering Ta target boat with TaC coating

Laura Lambert wrote:

John Wong wrote:

John Wong wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

 Wednesday, January 22, 2014, 18:09

After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2). 

Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN 

Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes. 

Maybe a fault in the water signal.  If it happens again, the water signal should be replaced.

Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK!

Chamber is a bit warm now.  Will allow time to cool down.

Will vent the chamber tomorrow and the boat will be inspected. 


 

 Thursday, January 23, 2014, 16:18

Chamber vented overnight and was opened up this morning.

Target boat not fully sintered [see attached photos].

Chamber currently being pumped down again in order to continue with sintering TaC coating.

HS cooling water valves were opened, no leaks detected.

Will ramp up to 700A again over the weekend.

 Friday, January 24, 2014, 14:21

Chamber was pumped down to 1.7e-7 Torr.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A.

Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.


 

  110   Thursday, January 23, 2014, 16:22 Laura LambertEmpty40282-4TARGET BOATProblems resolvedSintering Ta target boat with TaC coating

John Wong wrote:

John Wong wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

 Wednesday, January 22, 2014, 18:09

After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2). 

Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN 

Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes. 

Maybe a fault in the water signal.  If it happens again, the water signal should be replaced.

Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK!

Chamber is a bit warm now.  Will allow time to cool down.

Will vent the chamber tomorrow and the boat will be inspected. 


 

 Thursday, January 23, 2014, 16:18

Chamber vented overnight and was opened up this morning.

Target boat not fully sintered [see attached photos].

Chamber currently being pumped down again in order to continue with sintering TaC coating.

HS cooling water valves were opened, no leaks detected.

Will ramp up to 700A again over the weekend.

  109   Wednesday, January 22, 2014, 18:22 John WongEmpty40282-4TARGET BOATProblemsSintering Ta target boat with TaC coating (IEVAP2:TBHT2 water signal problem)

John Wong wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

 Wednesday, January 22, 2014, 18:09

After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2). 

Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN 

Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes. 

Maybe a fault in the water signal.  If it happens again, the water signal should be replaced.

Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK!

Chamber is a bit warm now.  Will allow time to cool down.

Will vent the chamber tomorrow and the boat will be inspected. 


 

  108   Wednesday, January 22, 2014, 15:13 John WongEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Note: This is the "old" design boat.  The new design boat was able to heat up to 900A/16.88 - the temperature was measured at about 1500C.  (see elog: https://elog.triumf.ca/TIS/Evaporator_2/15)

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.


 

  107   Wednesday, January 22, 2014, 13:46 Laura LambertEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.


 

  106   Wednesday, January 22, 2014, 09:49 Laura LambertEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.


 

  105   Tuesday, January 21, 2014, 11:56 Laura LambertEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!


 

  104   Tuesday, January 21, 2014, 11:33 Laura LambertEmpty40282-4TARGET BOAT Sintering Ta target boat with TaC coating

Laura Lambert wrote:

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.


 

  103   Monday, January 20, 2014, 16:35 Laura LambertEmptyTa-Target boat  Sintering Ta target boat with TaC coating

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.


 

  102   Monday, January 20, 2014, 16:30 Laura LambertEmpty39165-9LP-SISDoneSintering TaC coating container

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

 Thursday, January 16, 2014, 11:35

Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.

TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.

Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.


 

 Friday, January 17, 2014, 09:28

TGHT/TBHT @ 300/200A.  TBHT voltage is limited at 3A.  

TGHT ramping rate increased to 2A/min.  Pressure @ 4.5e-7 Torr.  


 

 Friday, January 17, 2014, 10:14

TBHT stopped at 200A with voltage limit sitting at 3V.

Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.

IGP1 @ 5.0e-7 Torr

 Friday, January 17, 2014, 12:45

TGHT voltage limiting at 9.9V, and  current stayed at 560A.  Increased the TGHT voltage to 10.5V and continued ramping the heater up.

TGHT/TBHT stabilized at 850A (~10V) and 230A(3.6V). 

Pressure at 1.03e-6 Torr and coming down... 

Target will be heated until 5pm (4hrs) before cooling down at the ramping rate of 2A/min. 

Chamber will be vented in air, next week.


 Friday, January 17, 2014, 16:51

Auto-cooling initiated at 2A/min.

Vac @ 5.3e-7 Torr.


 

 

  101   Friday, January 17, 2014, 12:52 John WongEmpty39165-9LP-SISIn progressSintering TaC coating container

Laura Lambert wrote:

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

 Thursday, January 16, 2014, 11:35

Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.

TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.

Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.


 

 Friday, January 17, 2014, 09:28

TGHT/TBHT @ 300/200A.  TBHT voltage is limited at 3A.  

TGHT ramping rate increased to 2A/min.  Pressure @ 4.5e-7 Torr.  


 

 Friday, January 17, 2014, 10:14

TBHT stopped at 200A with voltage limit sitting at 3V.

Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.

IGP1 @ 5.0e-7 Torr

 Friday, January 17, 2014, 12:45

TGHT voltage limiting at 9.9V, and  current stayed at 560A.  Increased the TGHT voltage to 10.5V and continued ramping the heater up.

TGHT/TBHT stabilized at 580A (~10V) and 230A(3.6V). 

Pressure at 1.03e-6 Torr and coming down... 

Target will be heated until 5pm (4hrs) before cooling down at the ramping rate of 2A/min. 

Chamber will be vented in air, next week.


 Friday, January 17, 2014, 16:51

Auto-cooling initiated at 2A/min.

Vac @ 5.3e-7 Torr.


 

  100   Friday, January 17, 2014, 10:18 Laura LambertEmpty39165-9LP-SISIn progressSintering TaC coating container

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

 Thursday, January 16, 2014, 11:35

Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.

TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.

Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.


 

 Friday, January 17, 2014, 09:28

TGHT/TBHT @ 300/200A.  TBHT voltage is limited at 3A.  

TGHT ramping rate increased to 2A/min.  Pressure @ 4.5e-7 Torr.  


 

 Friday, January 17, 2014, 10:14

TBHT stopped at 200A with voltage limit sitting at 3V.

Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.

IGP1 @ 5.0e-7 Torr

ELOG V2.9.2-2455