Friday, March 21, 2014, 16:18, John Wong, TiC, 38817-8, HP-SIS, In progress, Sintering TiC
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Wednesday, March 26, 2014, 11:07, Laura Lambert, TiC, 38817-8, HP-SIS, In progress, Sintering TiC
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Wednesday, March 26, 2014, 18:23, John Wong, TiC, 38817-8, HP-SIS, Done, Sintering TiC#4
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Laura Lambert wrote: |
John Wong wrote: |
Friday, March 21, 2014, 16:09
Target container is loaded with 360 Discs of TiC.
Target length = 11.7cm.
Total green mass = 40.945g
Container is wrapped with 3 Ta-heat shields, and have been pumped down in the chamber.
For the sintering process:
TGHT ramp up to 820A, and TGHT to 300A at 0.1A/min.
Friday, March 21, 2014, 16:15
TGHT/TBHT were manually stepped up to 40A.
Vac stabilizes at 1.7e-6 Torr.
Initiate auto-ramping...
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Wednesday, March 26, 2014, 11:05
TBHT reached max desired current of 300A
IGP1 = 1.4e-6 Torr
TGHT = 543A
Increasing TGHT auto-ramp to 2.0A/min
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Wednesday, March 26, 2014, 18:18
TGHT has reached to 820A\13.4V and target has been heated at that current for 4.5 hours.
Vac is coming down to 1.1e-6 Torr.
See link for RGA results: https://www.dropbox.com/sh/08dcxskux21aqap/1SF_dTJB4l
Cooling down in process at 2A/min for TGHT and 1A/min for TBHT.
Thursday, March 27, 2014, 11:14
Target is cooled down. TGHT/TBHT have reached to 0A.
All pumps off; chamber will be vented soon.
Friday, March 28, 2014, 15:00
Target has been assembled. Heat shield WO#39956-10
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