Logbooks Lab Maintenance Evaporator_1 Evaporator_2 Laser cutter Target Production Test-Stand RH-ISAC RH-Cyclotron RH-Meson Hall RH-Beamlines RH-ARIEL
  Evaporator_2, Page 18 of 35  Not logged in ELOG logo
ID Date Author Target Material Target Oven W.O# Source Status Subject
  350   Tuesday, February 21, 2017, 15:21 Laura LambertEmpty42218-1LP-IG-LISDonesintering TaC coating on UCx#20 container

Tuesday, February 21, 2017, 15:19

Container coated with TaC using 'flushing technique' and let dry overnight.

Cleaned ionizer tube with acetone, no coating inside ionizer tube

Wrapped with 3 x Ta heat shields, incl center block

Currently pumping down in evap2

OMEGA slope = 0.98

Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.


 Wednesday, February 22, 2017, 09:41

HS water valves opened, no leaks detected.

Tapped up manually to 35A

Waited ~45min

Vacuum stable.

IGP1 = 1.2e-6 Torr

Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 350A

Initiating auto ramp for TBHT @ 0.1A/min to a max setpoint of 230A

Once max setpoints achieved, will tap up manually to final desired temperature of 1900C


Friday, February 24, 2017 by Anders

Continue manually to 1900 C

Friday, February 24, 2017, 16:24: TGHT at 400 A 6.35V IG1 = 4.5e-7 Torr 1660 C

Friday, February 24, 2017, 16:57: TGHT at 410 A 6.6 V IG1 = 5.0e-7 Torr 1700 C


Sunday, February 26, 2017 by Anders

Sunday, February 26, 2017, 14:13: TGHT at 425 A 6.9 V IG1 = 2.5e-7 Torr 

Lab closed for weekend. No access to temp reading.


 Monday, February 27, 2017, 16:12

Tapped up manually to 1900C this morning.

TGHT = 490A, 8.14V

TBHT = 230A, 2.98V

MIKRON = 1911C

OMEGA = 1904C

evap2 has remained at max setpoints for ~6hrs

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Tuesday, February 28, 2017, 11:57

Container finished sintering.

Vented in air and opened up this morning.

Container looks good 


 

Attachment 1: IMG_1562.JPG
IMG_1562.JPG
Attachment 2: IMG_1564.JPG
IMG_1564.JPG
  349   Tuesday, February 14, 2017, 15:48 Laura LambertEndcaps TARGET BOATDoneSintering TaC coating on Ta endcaps and springs

Laura Lambert wrote:

Laura Lambert wrote:

 Friday, February 03, 2017, 14:17

The endcaps are stacked together with a punched out disc of graphite foil placed in between each endcap for separation so endcaps won't fuse together.

The end caps are further wrapped in a larger piece of graphite foil to hold together as a tube [same method used in elogID # 158 and 235]

There are also 4 coated springs, 2 on each side of the endcaps tube, with the endcaps tube residing in the middle of the boat.

The boat is wrapped with 3-layers of Ta heatshields.

Chamber is currently being pumped down.

Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.

OMEGA slope = 0.98


 Monday, February 06, 2017, 09:29

Power outage this weekend and evap2 tripped off.

Re-pumping down now...


 Tuesday, February 07, 2017, 08:54

HS water valves opened, no leaks detected.

IGP1 = 1.9e-7 Torr

Tapped up manually to 35A

Vacuum stable.

IGP1 = 2.0e-7 Torr

Initiating auto-ramp at 0.2A/min with a final setpoint of 450A.

Final desired temperature = 1800C


 Wednesday, February 08, 2017, 09:52

IGP1 = 2.98e-7 Torr

TGHT = 325A, 3.5V

Vacuum stable.

Increasing ramping rate to 1.0A/min


 Wednesday, February 08, 2017, 11:46

IGP1 = 6.3e-7 Torr

TGHT = 433A, 4.89V

Increasing max setpoint to TGHT = 500A

OMEGA has still yet to show a temperature...should be reading points at this high in current

Will go down to the lab and follow up on OMEGA settings to confirm everything is set up ok before proceeding to a higher current...


 Wednesday, February 08, 2017, 16:03

IGP1 = 4e-7 Torr

TGHT = 500A, 5.75V

OMEGA still not reading

Initiating auto-cool at -2A/min

Will update elog with more details tomorrow


 Thursday, February 09, 2017, 10:52

Evap2 was cooled down and opened up this morning.

Turns out both legs on the target boat were touching the new heatshield and therefore had been loosing power.

Normally a boat at 500A would read ~1800C, in this scenario at 500A the boat read ~1000C.

A lot of power was being lost into the heatshield.

See photos attached of target boat sitting at 500A.

The heatshield is currently being ground down in those two spots to accommodate the target boat.


 

 Tuesday, February 14, 2017, 15:43

Heatshield was ground back and target boat now fits nicely into heatshield without contact.


 

 Tuesday, February 14, 2017, 15:44

Boat with endcaps and springs reloaded today and pumped back down this afternoon.

HS water valves opened, no leaks detected.

Tapped up manually to 35A

Vacuum stable.

IGP1 = 3.5e-6 Torr

Initiating auto-ramp at 0.2A/min with a final setpoint of 400A.

Final desired temperature = 1800C


 Wednesday, February 15, 2017, 10:24

IGP1 = 7.2e-7 Torr

TGHT = 260A, 3.95V

OMEGA = 1158C

Vacuum stable.

Increasing ramping rate to 1.0A/min.


 Wednesday, February 15, 2017, 13:02

IGP1 = 2.0e-6 Torr

TGHT = 400A, 6.67V

OMEGA = 1530C

Increasing final setpoint to 450A


 Wednesday, February 15, 2017, 13:55

IGP1 = 2.5e-6 Torr

TGHT =450A, 7.7V

OMEGA = 1640C

Increasing final setpoint to 500A


 Wednesday, February 15, 2017, 15:13

IGP1 = 1.8e-6 Torr

TGHT = 500A, 8.59V

OMEGA = 1770C

MIKRON = 1740C

Tapping up manually to ~1800C...


 Thursday, February 16, 2017, 09:09

IGP1 = 5.28e-7 Torr

TGHT = 520A, 9.1V

OMEGA = 1821C

Target boat has remained at max setpoints for 17.5hrs.

Initiating auto-cool at 1A/min


 Thursday, February 16, 2017, 13:49

Increasing auto-cool to 2.0A/min


 Friday, February 17, 2017, 16:00

Vented in air and opened up today.

Endcaps looks good  see photos attached


 

Attachment 1: IMG_1542.JPG
IMG_1542.JPG
Attachment 2: IMG_1545.JPG
IMG_1545.JPG
Attachment 3: IMG_1549.JPG
IMG_1549.JPG
Attachment 4: IMG_1552.JPG
IMG_1552.JPG
  348   Tuesday, February 14, 2017, 15:44 Laura LambertEndcaps TARGET BOATProblems resolvedSintering TaC coating on Ta endcaps and springs

Laura Lambert wrote:

 Friday, February 03, 2017, 14:17

The endcaps are stacked together with a punched out disc of graphite foil placed in between each endcap for separation so endcaps won't fuse together.

The end caps are further wrapped in a larger piece of graphite foil to hold together as a tube [same method used in elogID # 158 and 235]

There are also 4 coated springs, 2 on each side of the endcaps tube, with the endcaps tube residing in the middle of the boat.

The boat is wrapped with 3-layers of Ta heatshields.

Chamber is currently being pumped down.

Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.

OMEGA slope = 0.98


 Monday, February 06, 2017, 09:29

Power outage this weekend and evap2 tripped off.

Re-pumping down now...


 Tuesday, February 07, 2017, 08:54

HS water valves opened, no leaks detected.

IGP1 = 1.9e-7 Torr

Tapped up manually to 35A

Vacuum stable.

IGP1 = 2.0e-7 Torr

Initiating auto-ramp at 0.2A/min with a final setpoint of 450A.

Final desired temperature = 1800C


 Wednesday, February 08, 2017, 09:52

IGP1 = 2.98e-7 Torr

TGHT = 325A, 3.5V

Vacuum stable.

Increasing ramping rate to 1.0A/min


 Wednesday, February 08, 2017, 11:46

IGP1 = 6.3e-7 Torr

TGHT = 433A, 4.89V

Increasing max setpoint to TGHT = 500A

OMEGA has still yet to show a temperature...should be reading points at this high in current

Will go down to the lab and follow up on OMEGA settings to confirm everything is set up ok before proceeding to a higher current...


 Wednesday, February 08, 2017, 16:03

IGP1 = 4e-7 Torr

TGHT = 500A, 5.75V

OMEGA still not reading

Initiating auto-cool at -2A/min

Will update elog with more details tomorrow


 Thursday, February 09, 2017, 10:52

Evap2 was cooled down and opened up this morning.

Turns out both legs on the target boat were touching the new heatshield and therefore had been loosing power.

Normally a boat at 500A would read ~1800C, in this scenario at 500A the boat read ~1000C.

A lot of power was being lost into the heatshield.

See photos attached of target boat sitting at 500A.

The heatshield is currently being ground down in those two spots to accommodate the target boat.


 

 Tuesday, February 14, 2017, 15:43

Heatshield was ground back and target boat now fits nicely into heatshield without contact.


 

  347   Thursday, February 09, 2017, 23:28 John Wongnp-SiC TARGET BOATDoneThermotest: SiC-SiO2-Lys and SiC pellets

Thursday, February 09, 2017, 23:26

There are two types of samples being test for thermal stability:

1.  SiC-SiO2-Lys nanofiber mats

2.  SiC pellets

(see Lab Book for more info)

Desired temperature: ~1500C

One-Ta heat shield is used, est. TGHT 450A.


 Thursday, February 09, 2017, 23:38

TGHT currently at 322A/5.28V, OMEGA 1204C.

Vac 2.9e-6 Torr.


 Friday, February 10, 2017, 08:58

TGHT at 400A, temp at 1425C for 8 hours.

Decided to cool down for analysis.  Check for carboreduction for SiO2 at 1400C.  Then continue to ramp up to 1500C. 

Ramping down at 2A/min


 Friday, February 10, 2017, 10:47

Rapid out-gas (2.7e-6 to 3.8e-6 Torr) from TGHT 330A until current stopped at 400A (see attachment).  Could be the evolution of O2 from SiO2... 


 

Attachment 1: striptool_01.JPG
striptool_01.JPG
  346   Thursday, February 09, 2017, 11:49 Laura Lambert   MaintenanceNew heatshield with flexible water lines

 Thursday, February 09, 2017, 11:47

A new heatshield with flexible water lines has been put into evap2 last Friday Feb3rd


 

  345   Monday, February 06, 2017, 11:17 Anders Mjos   Problems resolvedIOC restart after power outagae

 Dave Morris did a remote restart of the IOC after the outage. Turbo pump started.

  344   Friday, February 03, 2017, 14:18 Laura LambertEndcaps TARGET BOATProblemsSintering TaC coating on Ta endcaps and springs

 Friday, February 03, 2017, 14:17

The endcaps are stacked together with a punched out disc of graphite foil placed in between each endcap for separation so endcaps won't fuse together.

The end caps are further wrapped in a larger piece of graphite foil to hold together as a tube [same method used in elogID # 158 and 235]

There are also 4 coated springs, 2 on each side of the endcaps tube, with the endcaps tube residing in the middle of the boat.

The boat is wrapped with 3-layers of Ta heatshields.

Chamber is currently being pumped down.

Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.

OMEGA slope = 0.98


 Monday, February 06, 2017, 09:29

Power outage this weekend and evap2 tripped off.

Re-pumping down now...


 Tuesday, February 07, 2017, 08:54

HS water valves opened, no leaks detected.

IGP1 = 1.9e-7 Torr

Tapped up manually to 35A

Vacuum stable.

IGP1 = 2.0e-7 Torr

Initiating auto-ramp at 0.2A/min with a final setpoint of 450A.

Final desired temperature = 1800C


 Wednesday, February 08, 2017, 09:52

IGP1 = 2.98e-7 Torr

TGHT = 325A, 3.5V

Vacuum stable.

Increasing ramping rate to 1.0A/min


 Wednesday, February 08, 2017, 11:46

IGP1 = 6.3e-7 Torr

TGHT = 433A, 4.89V

Increasing max setpoint to TGHT = 500A

OMEGA has still yet to show a temperature...should be reading points at this high in current

Will go down to the lab and follow up on OMEGA settings to confirm everything is set up ok before proceeding to a higher current...


 Wednesday, February 08, 2017, 16:03

IGP1 = 4e-7 Torr

TGHT = 500A, 5.75V

OMEGA still not reading

Initiating auto-cool at -2A/min

Will update elog with more details tomorrow


 Thursday, February 09, 2017, 10:52

Evap2 was cooled down and opened up this morning.

Turns out both legs on the target boat were touching the new heatshield and therefore had been loosing power.

Normally a boat at 500A would read ~1800C, in this scenario at 500A the boat read ~1000C.

A lot of power was being lost into the heatshield.

See photos attached of target boat sitting at 500A.

The heatshield is currently being ground down in those two spots to accommodate the target boat.


 

Attachment 1: IMG_1526.JPG
IMG_1526.JPG
Attachment 2: IMG_1527.JPG
IMG_1527.JPG
  343   Tuesday, January 31, 2017, 16:03 Laura LambertEmpty39530-10HP-FEBIADDoneSintering TaC coated container for backup

 Tuesday, January 31, 2017, 13:43

Container coated with TaC using new method: Ends taped off,  with liquid poured in and swirled around entire container, then poured back out - 'flushing technique'

Container is wrapped with 3 x Ta heat shields, not incl center block.

Loaded into EVAP2 and currently pumping down.


Tuesday, January 31, 2017, 16:02 

IGP1 = 3.9e-6 Torr.

HS water valves opened.

No leaks detected.

Tapped up manually to 35A.

Vacuum stable.

Initiated auto ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

Final setpoints for TGHT = 450A and TBHT = 230A, with final desired temp of 1900C

OMEGA slope = 0.98


 Wednesday, February 01, 2017, 10:01

IGP1 = 5.7e-7 Torr.

TGHT = 254A, 3.0V

TBHT = 142A, 1.8V

Increasing ramping rate to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Wednesday, February 01, 2017, 11:48

IGP1 = 1.7e-6 Torr.

TGHT = 450A, 6.27V

TBHT = 230A, 3.14V

OMEGA = 1176C

Increasing max setpoint of TGHT = 600A


 Wednesday, February 01, 2017, 13:09

IGP1 = 3.7e-6 Torr.

TGHT = 600A, 9.0V

TBHT = 230A, 3.18V

OMEGA = 1480C

Increasing max setpoint of TGHT = 700A


 Wednesday, February 01, 2017, 14:08

IGP1 = 3.8e-6 Torr.

TGHT = 700A, 10.96V

TBHT = 230A, 3.2V

OMEGA = 1705C

Increasing max setpoint of TGHT = 750A


 Wednesday, February 01, 2017, 15:02

IGP1 = 5.1e-6 Torr.

TGHT = 750A, 11.87V

TBHT = 230A, 3.2V

OMEGA = 1808C

Increasing max setpoint of TGHT = 800A


 Wednesday, February 01, 2017, 15:30

IGP1 = 6.6e-6 Torr.

TGHT = 800A, 12.86V

TBHT = 230A, 3.2V

OMEGA = 1903C

Will remain at max setpoints overnight.


 Thursday, February 02, 2017, 09:16

Remained at max setpoints for ~18hrs.

IGP1 = 9.5e-7 Torr.

OMEGA =1914C

TGHT = 800A, 12.83V

TBHT = 230A, 3.22V

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Friday, February 03, 2017, 14:24

Vented in air and opened up this morning

Coating looks good.

See photos attached.


 

Attachment 1: 39530-10(1).JPG
39530-10(1).JPG
Attachment 2: 39530-10(2).JPG
39530-10(2).JPG
  342   Tuesday, December 20, 2016, 15:04 Laura Lambert   MaintenanceRETURN and SUPPLY valves CLOSED for xmas break

Tuesday, December 20, 2016, 15:05

confirmed ~full tank of Ar for glove box --> ~1600psi 

  341   Friday, December 16, 2016, 14:14 Laura LambertTa39530-3LP-FEBIADDoneConditioning Ta FEBIAD target for shutdown tests

 Friday, December 16, 2016, 14:08

Target consists of 470 discs.

Total packed length 3.4cm [exactly 7.8cm space on both sides]

Total mass 45.9091g [Incl foils + Ta wire on 6 packs]

Target consists of 350 single discs and 6x20 packs of Ta discs

Discs in target are arranged as follows: 1pack / 75singles / 1pack / 100singles / 2packs / 100singles / 1pack / 75singles / 1pack

3x Ta Heat shields.

LP-FEBIAD container with large center block.

No endcaps inserted, no Rh foil inserted.

Chamber currently pumping down.

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 350A at 2.0A/min.

Final desired temperature = 1900C


 Friday, December 16, 2016, 14:32

HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 2.1e-6 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

 Monday, December 19, 2016, 11:52

Tapped up manually to ~1900C [see attached excel for details on data collected - interesting temperature fluctuations]

 Will remain at max setpoints for min 4hrs then auto-cool


 Monday, December 19, 2016, 15:20

Target has remained at max setpoints for just over 4hrs

TGHT = 520A, 8.67V

OMEGA = 1820C

IGP1 = 5.2e-7 Torr

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Tuesday, December 20, 2016, 11:52

Vented in air and opened up this morning.

Looks like the windows was coated in evap2, unsure if this was missed and coated before conditioning target or if this is from materials coming out during conditioning process...

Target looks good.

Endcaps inserted but not expanded.


 

Attachment 1: Ta-FEBIAD.xlsx
Attachment 2: Evernote_Camera_Roll_20161220_145947.jpg
Evernote_Camera_Roll_20161220_145947.jpg
  340   Thursday, December 01, 2016, 16:08 Laura LambertEmpty42218-12LP-SISDonesintering TaC coating on UCx#19 container

 Thursday, December 01, 2016, 16:06

Container coated with TaC using 'flushing technique' and let dry overnight.

Cleaned ionizer tube with acetone, no coating inside ionizer tube

Wrapped with 3 x Ta heat shields, incl center block

Currently pumping down in evap2

OMEGA slope = 0.98


 Friday, December 02, 2016, 11:24

Opened up HS water valves, no leaks detected.

Tapped up manually to 35A.

Waited ~25min, vacuum stable.

IGP1 = 1.65e-6 Torr

Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT.

Max setpoints set for 350A and 230A for the TGHT and TBHT respectively.

Once max setpoints achieved, will tap up manually to final desired temperature of 1900C


 Monday, December 05, 2016, 09:38

TGHT = 350A, 5.38V

TBHT = 230A, 4.03V

OMEGA = 1550C

IGP1 = 3.2e-7 Torr

Tapping up to 1900C...


 Monday, December 05, 2016, 14:11

OMEGA = 1905C

TGHT = 475A, 7.63V

TBHT = 230A, 4.07V

IGP1 = 8.5e-7 Torr


 Tuesday, December 06, 2016, 08:41

TGHT = 475A, 7.76V

TBHT = 230A, 4.07V

IGP1 = 3.9e-7 Torr

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


Wednesday, December 07, 2016, 08:46 

Evap2 was vented in air and opened up yesterday afternoon.

Container looks good, coating fully sintered.


 

  339   Tuesday, November 22, 2016, 15:58 Laura LambertNb40282-3TARGET BOATDoneConditioning Nb samples for Doug

Tuesday, November 22, 2016, 15:53

Target boat has a layer of niobium foil on the bottom of the boat.

A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos

Niobium samples are placed in slots, holding in place, to avoid warping.

Smaller samples closest to MIKRON IR reading [left side]

Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.

Loaded into evap2 today.

Pumping down now...


 Wednesday, November 23, 2016, 11:45

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

IGP1 = 6.4e-7 Torr

Setting auto-ramp rate at 0.2A/min to max setpoint of 250A.

Will tap up manually to final desired temperature of 1400C.


 Wednesday, November 23, 2016, 13:17

IGP1 = 5.9e-7

TGHT = 66A, 0.51V

Vacuum stable.

Increasing ramping rate to 1.0A/min


 Thursday, November 24, 2016, 08:46

IGP1 = 3.9e-7 Torr

TGHT = 250A, 3.41V      *NOTE: the current set reads 243.8A but the readout is 250A

OMEGA = 1013C

MIKRON has no reading yet

Tapping up manually to 1400C


 Thursday, November 24, 2016, 15:42

Samples have remained at ~1400C for 5hrs.

IGP1 = 5.8e-7 Torr

TGHT = 420A, 6.5V

OMEGA = 1410C

MIKRON = 1420C

Initiating auto-cool at 2.0A/min


 Friday, November 25, 2016, 11:39

Vented in air and opened up this morning.

Samples look good!


 

Attachment 1: samples.jpg
samples.jpg
Attachment 2: evap2.jpg
evap2.jpg
Attachment 3: heating_up.xlsx
Attachment 4: visual_of_MIKRON_pointing_at_samples.JPG
visual_of_MIKRON_pointing_at_samples.JPG
  338   Friday, November 18, 2016, 17:28 John Wongnp-SiC TARGET BOATDoneHeat-treatment: Beta-SiC (1um) fiber mats - SAMPLE ID: A1

Laura Lambert wrote:

John Wong wrote:

Tuesday, November 15, 2016, 16:48

Three samples were prepared  (see my logbook#1 page 3, preparing for carbonization).

One layer of Ta foil was used to wrap around the target boat. 

Chamber is currently being pumped down


 Wednesday, November 16, 2016, 11:04

Ramping up TGHT at 2A/min, set at 350A.

Desired temperature, ~1530C (similar heating condition as raw npSiC heat treatment, elog ID335)


 Thursday, November 17, 2016, 10:09

TGHT reached to 350A/5.80V, stayed for over 20 hours.  Temp measured at 1276 C (Mikon) and 1270 (Omega), vac at 6.07e-7 Torr. 

Stepping up TGHT to reach the desired temp.


 

 Thursday, November 17, 2016, 11:13

TGHT = 400A, 6.73V

IGP1 = 8.2e-7 Torr

OMEGA = 1385C

MIKRON = 1389C

Tapping up manually to 1500C or a max setpoint of 450A


Thursday, November 17, 2016, 11:56

TGHT = 450A, 7.85V

IGP1 = 1.7e-6 Torr

OMEGA = 1502C

MIKRON = 1510C


 Friday, November 18, 2016, 10:08

IGP1 = 5.3e-7 Torr

TGHT = 450A, 7.9V

OMEGA = 1510C

MIKRON = 1515C

Evap2 has remained at max setpoints for 23hrs.

Initiating auto-cool at 2.0A/min


 

 Friday, November 18, 2016, 17:27

The heat treatment of the fiber mats is done. 

Analyzing steps...


 

  337   Thursday, November 17, 2016, 11:15 Laura Lambertnp-SiC TARGET BOATIn progressHeat-treatment: Beta-SiC (1um) fiber mats - SAMPLE ID: A1

John Wong wrote:

Tuesday, November 15, 2016, 16:48

Three samples were prepared  (see my logbook#1 page 3, preparing for carbonization).

One layer of Ta foil was used to wrap around the target boat. 

Chamber is currently being pumped down


 Wednesday, November 16, 2016, 11:04

Ramping up TGHT at 2A/min, set at 350A.

Desired temperature, ~1530C (similar heating condition as raw npSiC heat treatment, elog ID335)


 Thursday, November 17, 2016, 10:09

TGHT reached to 350A/5.80V, stayed for over 20 hours.  Temp measured at 1276 C (Mikon) and 1270 (Omega), vac at 6.07e-7 Torr. 

Stepping up TGHT to reach the desired temp.


 

 Thursday, November 17, 2016, 11:13

TGHT = 400A, 6.73V

IGP1 = 8.2e-7 Torr

OMEGA = 1385C

MIKRON = 1389C

Tapping up manually to 1500C or a max setpoint of 450A


Thursday, November 17, 2016, 11:56

TGHT = 450A, 7.85V

IGP1 = 1.7e-6 Torr

OMEGA = 1502C

MIKRON = 1510C


 Friday, November 18, 2016, 10:08

IGP1 = 5.3e-7 Torr

TGHT = 450A, 7.9V

OMEGA = 1510C

MIKRON = 1515C

Evap2 has remained at max setpoints for 23hrs.

Initiating auto-cool at 2.0A/min


 

  336   Tuesday, November 15, 2016, 16:51 John Wongnp-SiC TARGET BOATIn progressHeat-treatment: Beta-SiC (1um) fiber mats - SAMPLE ID: A1

Tuesday, November 15, 2016, 16:48

Three samples were prepared  (see my logbook#1 page 3, preparing for carbonization).

One layer of Ta foil was used to wrap around the target boat. 

Chamber is currently being pumped down


 Wednesday, November 16, 2016, 11:04

Ramping up TGHT at 2A/min, set at 350A.

Desired temperature, ~1530C (similar heating condition as raw npSiC heat treatment, elog ID335)


 Thursday, November 17, 2016, 10:09

TGHT reached to 350A/5.80V, stayed for over 20 hours.  Temp measured at 1276 C (Mikon) and 1270 (Omega), vac at 6.07e-7 Torr. 

Stepping up TGHT to reach the desired temp.


 

  335   Monday, October 24, 2016, 17:52 John Wongnp-SiC TARGET BOATDoneThermo test of np-SiC raw powder

Monday, October 24, 2016, 17:43

Two samples were prepared and loaded into the target boat with 1 layer of heat-shied as shown in the attachment#1.

Ingredients used: np-SiC and very small about of 5% PVA to hold the powder together. 

Samples were dried in the oven at 110C before loaded in Evap#2. 

After dried:

Sample #1 (larger graphite boat, mass =0.3779) = 0.4259g (PVA mass unknown due to solution leaking out from the boat)

Sample #2 = 0.2306g (with 5% PVA of 0.4111g)

Test temperature at 1600C, expect TGHT to be around 400A. 


Monday, October 24, 2016, 17:50

Ramping up TGHT to 300A at 0.5A/min. Vac at 2.3e-6 Torr. 


 Tuesday, October 25, 2016, 12:59

TGHT reached to 300A and stabilized for 10 hours.  OMEGA temp reader at 1150C

Continue to ramp up TGHT


 Wednesday, October 26, 2016, 15:49

TGHT was ramped up to 450A/7.91V; the temp readers on MIKON and OMEGA were 1489 and 1535, respectively (see attachment).

The temperature was much lower than the previous two tests (see elog #296 and #335).  Not sure why... 

Will do composition analysis on the sample... 

Cooling down at 2A/min.


 

Attachment 1: Capture.JPG
Capture.JPG
Attachment 2: 450A_1500C.JPG
450A_1500C.JPG
  334   Tuesday, October 18, 2016, 09:23 Laura LambertTa41790-5LP-SISDoneTemperature measurements for Ta#50

Aurelia Laxdal wrote:

Aurelia Laxdal wrote:

Laura Lambert wrote:

Thursday, October 13, 2016, 18:04

Target loaded into evap2

No heat shields.

Both endcaps inserted and expanded.

Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]

Chamber pumped down.

HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 5e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


Friday, October 14, 2016, 13:28

TGHT and TBHT had reached 300A/ 230A respectively.

Power bump ~10min ago caused evap2 to trip off.

Tapped back up manually to 35A.

Re-initiating auto ramp now.


 

Friday October 14: the target was ramp up to 300A/230A after Laura started it. Then, I cooled down at 6pm before leaving TRIUMF. <br>

Saturday October 15: restated the auto-ramp for Ta#50 in EVAP2. It's currently set to go to 300A/230A.

 Sunday October 16: the target temperature measurements up to 620A/230A were performed today not on October 15 (yesterday, it was cooled down before reaching 300A/230A). Currently the target is cooling down, to be ready tomorrow morning for the Test Stand. 

 Monday, October 17, 2016, 09:21

Vented in air and taken out this morning.

Target looks good!


 

  333   Sunday, October 16, 2016, 17:55 Aurelia LaxdalTa41790-5LP-SISIn progressTemperature measurements for Ta#50

Aurelia Laxdal wrote:

Laura Lambert wrote:

Thursday, October 13, 2016, 18:04

Target loaded into evap2

No heat shields.

Both endcaps inserted and expanded.

Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]

Chamber pumped down.

HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 5e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


Friday, October 14, 2016, 13:28

TGHT and TBHT had reached 300A/ 230A respectively.

Power bump ~10min ago caused evap2 to trip off.

Tapped back up manually to 35A.

Re-initiating auto ramp now.


 

Friday October 14: the target was ramp up to 300A/230A after Laura started it. Then, I cooled down at 6pm before leaving TRIUMF. <br>

Saturday October 15: restated the auto-ramp for Ta#50 in EVAP2. It's currently set to go to 300A/230A.

 Sunday October 16: the target temperature measurements up to 620A/230A were performed today not on October 15 (yesterday, it was cooled down before reaching 300A/230A). Currently the target is cooling down, to be ready tomorrow morning for the Test Stand. 

  332   Saturday, October 15, 2016, 12:42 Aurelia LaxdalTa41790-5LP-SISIn progressTemperature measurements for Ta#50

Laura Lambert wrote:

Thursday, October 13, 2016, 18:04

Target loaded into evap2

No heat shields.

Both endcaps inserted and expanded.

Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]

Chamber pumped down.

HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 5e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


Friday, October 14, 2016, 13:28

TGHT and TBHT had reached 300A/ 230A respectively.

Power bump ~10min ago caused evap2 to trip off.

Tapped back up manually to 35A.

Re-initiating auto ramp now.


 

Friday October 14: the target was ramp up to 300A/230A after Laura started it. Then, I cooled down at 6pm before leaving TRIUMF. <br>

Saturday October 15: restated the auto-ramp for Ta#50 in EVAP2. It's currently set to go to 300A/230A.

  331   Thursday, October 13, 2016, 18:05 Laura LambertTa41790-5LP-SISIn progressTemperature measurements for Ta#50

Thursday, October 13, 2016, 18:04

Target loaded into evap2

No heat shields.

Both endcaps inserted and expanded.

Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]

Chamber pumped down.

HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 5e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


Friday, October 14, 2016, 13:28

TGHT and TBHT had reached 300A/ 230A respectively.

Power bump ~10min ago caused evap2 to trip off.

Tapped back up manually to 35A.

Re-initiating auto ramp now.


 

ELOG V2.9.2-2455