|
ID |
Date |
Author |
Target Material |
Target Oven W.O# |
Source |
Status |
Subject |
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350
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Tuesday, February 21, 2017, 15:21 |
Laura Lambert | Empty | 42218-1 | LP-IG-LIS | Done | sintering TaC coating on UCx#20 container | Tuesday, February 21, 2017, 15:19
Container coated with TaC using 'flushing technique' and let dry overnight.
Cleaned ionizer tube with acetone, no coating inside ionizer tube
Wrapped with 3 x Ta heat shields, incl center block
Currently pumping down in evap2
OMEGA slope = 0.98
Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.
Wednesday, February 22, 2017, 09:41
HS water valves opened, no leaks detected.
Tapped up manually to 35A
Waited ~45min
Vacuum stable.
IGP1 = 1.2e-6 Torr
Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 350A
Initiating auto ramp for TBHT @ 0.1A/min to a max setpoint of 230A
Once max setpoints achieved, will tap up manually to final desired temperature of 1900C
Friday, February 24, 2017 by Anders
Continue manually to 1900 C
Friday, February 24, 2017, 16:24: TGHT at 400 A 6.35V IG1 = 4.5e-7 Torr 1660 C
Friday, February 24, 2017, 16:57: TGHT at 410 A 6.6 V IG1 = 5.0e-7 Torr 1700 C
Sunday, February 26, 2017 by Anders
Sunday, February 26, 2017, 14:13: TGHT at 425 A 6.9 V IG1 = 2.5e-7 Torr
Lab closed for weekend. No access to temp reading.
Monday, February 27, 2017, 16:12
Tapped up manually to 1900C this morning.
TGHT = 490A, 8.14V
TBHT = 230A, 2.98V
MIKRON = 1911C
OMEGA = 1904C
evap2 has remained at max setpoints for ~6hrs
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Tuesday, February 28, 2017, 11:57
Container finished sintering.
Vented in air and opened up this morning.
Container looks good 
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Attachment 1: IMG_1562.JPG
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Attachment 2: IMG_1564.JPG
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349
|
Tuesday, February 14, 2017, 15:48 |
Laura Lambert | Endcaps | | TARGET BOAT | Done | Sintering TaC coating on Ta endcaps and springs |
Laura Lambert wrote: |
Laura Lambert wrote: |
Friday, February 03, 2017, 14:17
The endcaps are stacked together with a punched out disc of graphite foil placed in between each endcap for separation so endcaps won't fuse together.
The end caps are further wrapped in a larger piece of graphite foil to hold together as a tube [same method used in elogID # 158 and 235]
There are also 4 coated springs, 2 on each side of the endcaps tube, with the endcaps tube residing in the middle of the boat.
The boat is wrapped with 3-layers of Ta heatshields.
Chamber is currently being pumped down.
Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.
OMEGA slope = 0.98
Monday, February 06, 2017, 09:29
Power outage this weekend and evap2 tripped off.
Re-pumping down now...
Tuesday, February 07, 2017, 08:54
HS water valves opened, no leaks detected.
IGP1 = 1.9e-7 Torr
Tapped up manually to 35A
Vacuum stable.
IGP1 = 2.0e-7 Torr
Initiating auto-ramp at 0.2A/min with a final setpoint of 450A.
Final desired temperature = 1800C
Wednesday, February 08, 2017, 09:52
IGP1 = 2.98e-7 Torr
TGHT = 325A, 3.5V
Vacuum stable.
Increasing ramping rate to 1.0A/min
Wednesday, February 08, 2017, 11:46
IGP1 = 6.3e-7 Torr
TGHT = 433A, 4.89V
Increasing max setpoint to TGHT = 500A
OMEGA has still yet to show a temperature...should be reading points at this high in current
Will go down to the lab and follow up on OMEGA settings to confirm everything is set up ok before proceeding to a higher current...
Wednesday, February 08, 2017, 16:03
IGP1 = 4e-7 Torr
TGHT = 500A, 5.75V
OMEGA still not reading
Initiating auto-cool at -2A/min
Will update elog with more details tomorrow
Thursday, February 09, 2017, 10:52
Evap2 was cooled down and opened up this morning.
Turns out both legs on the target boat were touching the new heatshield and therefore had been loosing power.
Normally a boat at 500A would read ~1800C, in this scenario at 500A the boat read ~1000C.
A lot of power was being lost into the heatshield.
See photos attached of target boat sitting at 500A.
The heatshield is currently being ground down in those two spots to accommodate the target boat.
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Tuesday, February 14, 2017, 15:43
Heatshield was ground back and target boat now fits nicely into heatshield without contact.
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Tuesday, February 14, 2017, 15:44
Boat with endcaps and springs reloaded today and pumped back down this afternoon.
HS water valves opened, no leaks detected.
Tapped up manually to 35A
Vacuum stable.
IGP1 = 3.5e-6 Torr
Initiating auto-ramp at 0.2A/min with a final setpoint of 400A.
Final desired temperature = 1800C
Wednesday, February 15, 2017, 10:24
IGP1 = 7.2e-7 Torr
TGHT = 260A, 3.95V
OMEGA = 1158C
Vacuum stable.
Increasing ramping rate to 1.0A/min.
Wednesday, February 15, 2017, 13:02
IGP1 = 2.0e-6 Torr
TGHT = 400A, 6.67V
OMEGA = 1530C
Increasing final setpoint to 450A
Wednesday, February 15, 2017, 13:55
IGP1 = 2.5e-6 Torr
TGHT =450A, 7.7V
OMEGA = 1640C
Increasing final setpoint to 500A
Wednesday, February 15, 2017, 15:13
IGP1 = 1.8e-6 Torr
TGHT = 500A, 8.59V
OMEGA = 1770C
MIKRON = 1740C
Tapping up manually to ~1800C...
Thursday, February 16, 2017, 09:09
IGP1 = 5.28e-7 Torr
TGHT = 520A, 9.1V
OMEGA = 1821C
Target boat has remained at max setpoints for 17.5hrs.
Initiating auto-cool at 1A/min
Thursday, February 16, 2017, 13:49
Increasing auto-cool to 2.0A/min
Friday, February 17, 2017, 16:00
Vented in air and opened up today.
Endcaps looks good see photos attached
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Attachment 1: IMG_1542.JPG
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Attachment 2: IMG_1545.JPG
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Attachment 3: IMG_1549.JPG
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Attachment 4: IMG_1552.JPG
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348
|
Tuesday, February 14, 2017, 15:44 |
Laura Lambert | Endcaps | | TARGET BOAT | Problems resolved | Sintering TaC coating on Ta endcaps and springs |
Laura Lambert wrote: |
Friday, February 03, 2017, 14:17
The endcaps are stacked together with a punched out disc of graphite foil placed in between each endcap for separation so endcaps won't fuse together.
The end caps are further wrapped in a larger piece of graphite foil to hold together as a tube [same method used in elogID # 158 and 235]
There are also 4 coated springs, 2 on each side of the endcaps tube, with the endcaps tube residing in the middle of the boat.
The boat is wrapped with 3-layers of Ta heatshields.
Chamber is currently being pumped down.
Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.
OMEGA slope = 0.98
Monday, February 06, 2017, 09:29
Power outage this weekend and evap2 tripped off.
Re-pumping down now...
Tuesday, February 07, 2017, 08:54
HS water valves opened, no leaks detected.
IGP1 = 1.9e-7 Torr
Tapped up manually to 35A
Vacuum stable.
IGP1 = 2.0e-7 Torr
Initiating auto-ramp at 0.2A/min with a final setpoint of 450A.
Final desired temperature = 1800C
Wednesday, February 08, 2017, 09:52
IGP1 = 2.98e-7 Torr
TGHT = 325A, 3.5V
Vacuum stable.
Increasing ramping rate to 1.0A/min
Wednesday, February 08, 2017, 11:46
IGP1 = 6.3e-7 Torr
TGHT = 433A, 4.89V
Increasing max setpoint to TGHT = 500A
OMEGA has still yet to show a temperature...should be reading points at this high in current
Will go down to the lab and follow up on OMEGA settings to confirm everything is set up ok before proceeding to a higher current...
Wednesday, February 08, 2017, 16:03
IGP1 = 4e-7 Torr
TGHT = 500A, 5.75V
OMEGA still not reading
Initiating auto-cool at -2A/min
Will update elog with more details tomorrow
Thursday, February 09, 2017, 10:52
Evap2 was cooled down and opened up this morning.
Turns out both legs on the target boat were touching the new heatshield and therefore had been loosing power.
Normally a boat at 500A would read ~1800C, in this scenario at 500A the boat read ~1000C.
A lot of power was being lost into the heatshield.
See photos attached of target boat sitting at 500A.
The heatshield is currently being ground down in those two spots to accommodate the target boat.
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Tuesday, February 14, 2017, 15:43
Heatshield was ground back and target boat now fits nicely into heatshield without contact.
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347
|
Thursday, February 09, 2017, 23:28 |
John Wong | np-SiC | | TARGET BOAT | Done | Thermotest: SiC-SiO2-Lys and SiC pellets | Thursday, February 09, 2017, 23:26
There are two types of samples being test for thermal stability:
1. SiC-SiO2-Lys nanofiber mats
2. SiC pellets
(see Lab Book for more info)
Desired temperature: ~1500C
One-Ta heat shield is used, est. TGHT 450A.
Thursday, February 09, 2017, 23:38
TGHT currently at 322A/5.28V, OMEGA 1204C.
Vac 2.9e-6 Torr.
Friday, February 10, 2017, 08:58
TGHT at 400A, temp at 1425C for 8 hours.
Decided to cool down for analysis. Check for carboreduction for SiO2 at 1400C. Then continue to ramp up to 1500C.
Ramping down at 2A/min
Friday, February 10, 2017, 10:47
Rapid out-gas (2.7e-6 to 3.8e-6 Torr) from TGHT 330A until current stopped at 400A (see attachment). Could be the evolution of O2 from SiO2...
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Attachment 1: striptool_01.JPG
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346
|
Thursday, February 09, 2017, 11:49 |
Laura Lambert | | | | Maintenance | New heatshield with flexible water lines | Thursday, February 09, 2017, 11:47
A new heatshield with flexible water lines has been put into evap2 last Friday Feb3rd
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345
|
Monday, February 06, 2017, 11:17 |
Anders Mjos | | | | Problems resolved | IOC restart after power outagae | Dave Morris did a remote restart of the IOC after the outage. Turbo pump started. |
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344
|
Friday, February 03, 2017, 14:18 |
Laura Lambert | Endcaps | | TARGET BOAT | Problems | Sintering TaC coating on Ta endcaps and springs | Friday, February 03, 2017, 14:17
The endcaps are stacked together with a punched out disc of graphite foil placed in between each endcap for separation so endcaps won't fuse together.
The end caps are further wrapped in a larger piece of graphite foil to hold together as a tube [same method used in elogID # 158 and 235]
There are also 4 coated springs, 2 on each side of the endcaps tube, with the endcaps tube residing in the middle of the boat.
The boat is wrapped with 3-layers of Ta heatshields.
Chamber is currently being pumped down.
Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.
OMEGA slope = 0.98
Monday, February 06, 2017, 09:29
Power outage this weekend and evap2 tripped off.
Re-pumping down now...
Tuesday, February 07, 2017, 08:54
HS water valves opened, no leaks detected.
IGP1 = 1.9e-7 Torr
Tapped up manually to 35A
Vacuum stable.
IGP1 = 2.0e-7 Torr
Initiating auto-ramp at 0.2A/min with a final setpoint of 450A.
Final desired temperature = 1800C
Wednesday, February 08, 2017, 09:52
IGP1 = 2.98e-7 Torr
TGHT = 325A, 3.5V
Vacuum stable.
Increasing ramping rate to 1.0A/min
Wednesday, February 08, 2017, 11:46
IGP1 = 6.3e-7 Torr
TGHT = 433A, 4.89V
Increasing max setpoint to TGHT = 500A
OMEGA has still yet to show a temperature...should be reading points at this high in current
Will go down to the lab and follow up on OMEGA settings to confirm everything is set up ok before proceeding to a higher current...
Wednesday, February 08, 2017, 16:03
IGP1 = 4e-7 Torr
TGHT = 500A, 5.75V
OMEGA still not reading
Initiating auto-cool at -2A/min
Will update elog with more details tomorrow
Thursday, February 09, 2017, 10:52
Evap2 was cooled down and opened up this morning.
Turns out both legs on the target boat were touching the new heatshield and therefore had been loosing power.
Normally a boat at 500A would read ~1800C, in this scenario at 500A the boat read ~1000C.
A lot of power was being lost into the heatshield.
See photos attached of target boat sitting at 500A.
The heatshield is currently being ground down in those two spots to accommodate the target boat.
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Attachment 1: IMG_1526.JPG
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Attachment 2: IMG_1527.JPG
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343
|
Tuesday, January 31, 2017, 16:03 |
Laura Lambert | Empty | 39530-10 | HP-FEBIAD | Done | Sintering TaC coated container for backup | Tuesday, January 31, 2017, 13:43
Container coated with TaC using new method: Ends taped off, with liquid poured in and swirled around entire container, then poured back out - 'flushing technique'
Container is wrapped with 3 x Ta heat shields, not incl center block.
Loaded into EVAP2 and currently pumping down.
Tuesday, January 31, 2017, 16:02
IGP1 = 3.9e-6 Torr.
HS water valves opened.
No leaks detected.
Tapped up manually to 35A.
Vacuum stable.
Initiated auto ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.
Final setpoints for TGHT = 450A and TBHT = 230A, with final desired temp of 1900C
OMEGA slope = 0.98
Wednesday, February 01, 2017, 10:01
IGP1 = 5.7e-7 Torr.
TGHT = 254A, 3.0V
TBHT = 142A, 1.8V
Increasing ramping rate to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Wednesday, February 01, 2017, 11:48
IGP1 = 1.7e-6 Torr.
TGHT = 450A, 6.27V
TBHT = 230A, 3.14V
OMEGA = 1176C
Increasing max setpoint of TGHT = 600A
Wednesday, February 01, 2017, 13:09
IGP1 = 3.7e-6 Torr.
TGHT = 600A, 9.0V
TBHT = 230A, 3.18V
OMEGA = 1480C
Increasing max setpoint of TGHT = 700A
Wednesday, February 01, 2017, 14:08
IGP1 = 3.8e-6 Torr.
TGHT = 700A, 10.96V
TBHT = 230A, 3.2V
OMEGA = 1705C
Increasing max setpoint of TGHT = 750A
Wednesday, February 01, 2017, 15:02
IGP1 = 5.1e-6 Torr.
TGHT = 750A, 11.87V
TBHT = 230A, 3.2V
OMEGA = 1808C
Increasing max setpoint of TGHT = 800A
Wednesday, February 01, 2017, 15:30
IGP1 = 6.6e-6 Torr.
TGHT = 800A, 12.86V
TBHT = 230A, 3.2V
OMEGA = 1903C
Will remain at max setpoints overnight.
Thursday, February 02, 2017, 09:16
Remained at max setpoints for ~18hrs.
IGP1 = 9.5e-7 Torr.
OMEGA =1914C
TGHT = 800A, 12.83V
TBHT = 230A, 3.22V
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Friday, February 03, 2017, 14:24
Vented in air and opened up this morning
Coating looks good.
See photos attached.
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Attachment 1: 39530-10(1).JPG
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Attachment 2: 39530-10(2).JPG
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342
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Tuesday, December 20, 2016, 15:04 |
Laura Lambert | | | | Maintenance | RETURN and SUPPLY valves CLOSED for xmas break | Tuesday, December 20, 2016, 15:05
confirmed ~full tank of Ar for glove box --> ~1600psi |
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341
|
Friday, December 16, 2016, 14:14 |
Laura Lambert | Ta | 39530-3 | LP-FEBIAD | Done | Conditioning Ta FEBIAD target for shutdown tests | Friday, December 16, 2016, 14:08
Target consists of 470 discs.
Total packed length 3.4cm [exactly 7.8cm space on both sides]
Total mass 45.9091g [Incl foils + Ta wire on 6 packs]
Target consists of 350 single discs and 6x20 packs of Ta discs
Discs in target are arranged as follows: 1pack / 75singles / 1pack / 100singles / 2packs / 100singles / 1pack / 75singles / 1pack
3x Ta Heat shields.
LP-FEBIAD container with large center block.
No endcaps inserted, no Rh foil inserted.
Chamber currently pumping down.
TBHT will be ramped up to 230A at 1.0A/min.
TGHT will be ramped up to 350A at 2.0A/min.
Final desired temperature = 1900C
Friday, December 16, 2016, 14:32
HS water valves opened, no leaks detected
Tapped up manually to 35A
Vacuum stable, IGP1 = 2.1e-6 Torr
Initiating auto-ramp.
OMEGA slope = 0.98
Monday, December 19, 2016, 11:52
Tapped up manually to ~1900C [see attached excel for details on data collected - interesting temperature fluctuations]
Will remain at max setpoints for min 4hrs then auto-cool
Monday, December 19, 2016, 15:20
Target has remained at max setpoints for just over 4hrs
TGHT = 520A, 8.67V
OMEGA = 1820C
IGP1 = 5.2e-7 Torr
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Tuesday, December 20, 2016, 11:52
Vented in air and opened up this morning.
Looks like the windows was coated in evap2, unsure if this was missed and coated before conditioning target or if this is from materials coming out during conditioning process...
Target looks good.
Endcaps inserted but not expanded.
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Attachment 1: Ta-FEBIAD.xlsx
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Attachment 2: Evernote_Camera_Roll_20161220_145947.jpg
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340
|
Thursday, December 01, 2016, 16:08 |
Laura Lambert | Empty | 42218-12 | LP-SIS | Done | sintering TaC coating on UCx#19 container | Thursday, December 01, 2016, 16:06
Container coated with TaC using 'flushing technique' and let dry overnight.
Cleaned ionizer tube with acetone, no coating inside ionizer tube
Wrapped with 3 x Ta heat shields, incl center block
Currently pumping down in evap2
OMEGA slope = 0.98
Friday, December 02, 2016, 11:24
Opened up HS water valves, no leaks detected.
Tapped up manually to 35A.
Waited ~25min, vacuum stable.
IGP1 = 1.65e-6 Torr
Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT.
Max setpoints set for 350A and 230A for the TGHT and TBHT respectively.
Once max setpoints achieved, will tap up manually to final desired temperature of 1900C
Monday, December 05, 2016, 09:38
TGHT = 350A, 5.38V
TBHT = 230A, 4.03V
OMEGA = 1550C
IGP1 = 3.2e-7 Torr
Tapping up to 1900C...
Monday, December 05, 2016, 14:11
OMEGA = 1905C
TGHT = 475A, 7.63V
TBHT = 230A, 4.07V
IGP1 = 8.5e-7 Torr
Tuesday, December 06, 2016, 08:41
TGHT = 475A, 7.76V
TBHT = 230A, 4.07V
IGP1 = 3.9e-7 Torr
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Wednesday, December 07, 2016, 08:46
Evap2 was vented in air and opened up yesterday afternoon.
Container looks good, coating fully sintered.
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339
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Tuesday, November 22, 2016, 15:58 |
Laura Lambert | Nb | 40282-3 | TARGET BOAT | Done | Conditioning Nb samples for Doug | Tuesday, November 22, 2016, 15:53
Target boat has a layer of niobium foil on the bottom of the boat.
A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos
Niobium samples are placed in slots, holding in place, to avoid warping.
Smaller samples closest to MIKRON IR reading [left side]
Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.
Loaded into evap2 today.
Pumping down now...
Wednesday, November 23, 2016, 11:45
HS water valves opened, no leaks detected.
Tapped up manually to 35A.
IGP1 = 6.4e-7 Torr
Setting auto-ramp rate at 0.2A/min to max setpoint of 250A.
Will tap up manually to final desired temperature of 1400C.
Wednesday, November 23, 2016, 13:17
IGP1 = 5.9e-7
TGHT = 66A, 0.51V
Vacuum stable.
Increasing ramping rate to 1.0A/min
Thursday, November 24, 2016, 08:46
IGP1 = 3.9e-7 Torr
TGHT = 250A, 3.41V *NOTE: the current set reads 243.8A but the readout is 250A
OMEGA = 1013C
MIKRON has no reading yet
Tapping up manually to 1400C
Thursday, November 24, 2016, 15:42
Samples have remained at ~1400C for 5hrs.
IGP1 = 5.8e-7 Torr
TGHT = 420A, 6.5V
OMEGA = 1410C
MIKRON = 1420C
Initiating auto-cool at 2.0A/min
Friday, November 25, 2016, 11:39
Vented in air and opened up this morning.
Samples look good!
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Attachment 1: samples.jpg
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Attachment 2: evap2.jpg
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Attachment 3: heating_up.xlsx
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Attachment 4: visual_of_MIKRON_pointing_at_samples.JPG
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338
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Friday, November 18, 2016, 17:28 |
John Wong | np-SiC | | TARGET BOAT | Done | Heat-treatment: Beta-SiC (1um) fiber mats - SAMPLE ID: A1 |
Laura Lambert wrote: |
John Wong wrote: |
Tuesday, November 15, 2016, 16:48
Three samples were prepared (see my logbook#1 page 3, preparing for carbonization).
One layer of Ta foil was used to wrap around the target boat.
Chamber is currently being pumped down
Wednesday, November 16, 2016, 11:04
Ramping up TGHT at 2A/min, set at 350A.
Desired temperature, ~1530C (similar heating condition as raw npSiC heat treatment, elog ID335)
Thursday, November 17, 2016, 10:09
TGHT reached to 350A/5.80V, stayed for over 20 hours. Temp measured at 1276 C (Mikon) and 1270 (Omega), vac at 6.07e-7 Torr.
Stepping up TGHT to reach the desired temp.
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Thursday, November 17, 2016, 11:13
TGHT = 400A, 6.73V
IGP1 = 8.2e-7 Torr
OMEGA = 1385C
MIKRON = 1389C
Tapping up manually to 1500C or a max setpoint of 450A
Thursday, November 17, 2016, 11:56
TGHT = 450A, 7.85V
IGP1 = 1.7e-6 Torr
OMEGA = 1502C
MIKRON = 1510C
Friday, November 18, 2016, 10:08
IGP1 = 5.3e-7 Torr
TGHT = 450A, 7.9V
OMEGA = 1510C
MIKRON = 1515C
Evap2 has remained at max setpoints for 23hrs.
Initiating auto-cool at 2.0A/min
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Friday, November 18, 2016, 17:27
The heat treatment of the fiber mats is done.
Analyzing steps...
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337
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Thursday, November 17, 2016, 11:15 |
Laura Lambert | np-SiC | | TARGET BOAT | In progress | Heat-treatment: Beta-SiC (1um) fiber mats - SAMPLE ID: A1 |
John Wong wrote: |
Tuesday, November 15, 2016, 16:48
Three samples were prepared (see my logbook#1 page 3, preparing for carbonization).
One layer of Ta foil was used to wrap around the target boat.
Chamber is currently being pumped down
Wednesday, November 16, 2016, 11:04
Ramping up TGHT at 2A/min, set at 350A.
Desired temperature, ~1530C (similar heating condition as raw npSiC heat treatment, elog ID335)
Thursday, November 17, 2016, 10:09
TGHT reached to 350A/5.80V, stayed for over 20 hours. Temp measured at 1276 C (Mikon) and 1270 (Omega), vac at 6.07e-7 Torr.
Stepping up TGHT to reach the desired temp.
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Thursday, November 17, 2016, 11:13
TGHT = 400A, 6.73V
IGP1 = 8.2e-7 Torr
OMEGA = 1385C
MIKRON = 1389C
Tapping up manually to 1500C or a max setpoint of 450A
Thursday, November 17, 2016, 11:56
TGHT = 450A, 7.85V
IGP1 = 1.7e-6 Torr
OMEGA = 1502C
MIKRON = 1510C
Friday, November 18, 2016, 10:08
IGP1 = 5.3e-7 Torr
TGHT = 450A, 7.9V
OMEGA = 1510C
MIKRON = 1515C
Evap2 has remained at max setpoints for 23hrs.
Initiating auto-cool at 2.0A/min
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336
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Tuesday, November 15, 2016, 16:51 |
John Wong | np-SiC | | TARGET BOAT | In progress | Heat-treatment: Beta-SiC (1um) fiber mats - SAMPLE ID: A1 | Tuesday, November 15, 2016, 16:48
Three samples were prepared (see my logbook#1 page 3, preparing for carbonization).
One layer of Ta foil was used to wrap around the target boat.
Chamber is currently being pumped down
Wednesday, November 16, 2016, 11:04
Ramping up TGHT at 2A/min, set at 350A.
Desired temperature, ~1530C (similar heating condition as raw npSiC heat treatment, elog ID335)
Thursday, November 17, 2016, 10:09
TGHT reached to 350A/5.80V, stayed for over 20 hours. Temp measured at 1276 C (Mikon) and 1270 (Omega), vac at 6.07e-7 Torr.
Stepping up TGHT to reach the desired temp.
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335
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Monday, October 24, 2016, 17:52 |
John Wong | np-SiC | | TARGET BOAT | Done | Thermo test of np-SiC raw powder | Monday, October 24, 2016, 17:43
Two samples were prepared and loaded into the target boat with 1 layer of heat-shied as shown in the attachment#1.
Ingredients used: np-SiC and very small about of 5% PVA to hold the powder together.
Samples were dried in the oven at 110C before loaded in Evap#2.
After dried:
Sample #1 (larger graphite boat, mass =0.3779) = 0.4259g (PVA mass unknown due to solution leaking out from the boat)
Sample #2 = 0.2306g (with 5% PVA of 0.4111g)
Test temperature at 1600C, expect TGHT to be around 400A.
Monday, October 24, 2016, 17:50
Ramping up TGHT to 300A at 0.5A/min. Vac at 2.3e-6 Torr.
Tuesday, October 25, 2016, 12:59
TGHT reached to 300A and stabilized for 10 hours. OMEGA temp reader at 1150C
Continue to ramp up TGHT
Wednesday, October 26, 2016, 15:49
TGHT was ramped up to 450A/7.91V; the temp readers on MIKON and OMEGA were 1489 and 1535, respectively (see attachment).
The temperature was much lower than the previous two tests (see elog #296 and #335). Not sure why...
Will do composition analysis on the sample...
Cooling down at 2A/min.
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Attachment 1: Capture.JPG
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Attachment 2: 450A_1500C.JPG
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334
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Tuesday, October 18, 2016, 09:23 |
Laura Lambert | Ta | 41790-5 | LP-SIS | Done | Temperature measurements for Ta#50 |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Laura Lambert wrote: |
Thursday, October 13, 2016, 18:04
Target loaded into evap2
No heat shields.
Both endcaps inserted and expanded.
Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]
Chamber pumped down.
HS water valves opened, no leaks detected
Tapped up manually to 35A
Vacuum stable, IGP1 = 5e-7 Torr
Initiating auto-ramp.
OMEGA slope = 0.98
TBHT will be ramped up to 230A at 1.0A/min.
TGHT will be ramped up to 300A at 2.0A/min.
Final desired temperature = 1900C
Friday, October 14, 2016, 13:28
TGHT and TBHT had reached 300A/ 230A respectively.
Power bump ~10min ago caused evap2 to trip off.
Tapped back up manually to 35A.
Re-initiating auto ramp now.
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Friday October 14: the target was ramp up to 300A/230A after Laura started it. Then, I cooled down at 6pm before leaving TRIUMF. <br>
Saturday October 15: restated the auto-ramp for Ta#50 in EVAP2. It's currently set to go to 300A/230A.
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Sunday October 16: the target temperature measurements up to 620A/230A were performed today not on October 15 (yesterday, it was cooled down before reaching 300A/230A). Currently the target is cooling down, to be ready tomorrow morning for the Test Stand.
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Monday, October 17, 2016, 09:21
Vented in air and taken out this morning.
Target looks good!
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333
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Sunday, October 16, 2016, 17:55 |
Aurelia Laxdal | Ta | 41790-5 | LP-SIS | In progress | Temperature measurements for Ta#50 |
Aurelia Laxdal wrote: |
Laura Lambert wrote: |
Thursday, October 13, 2016, 18:04
Target loaded into evap2
No heat shields.
Both endcaps inserted and expanded.
Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]
Chamber pumped down.
HS water valves opened, no leaks detected
Tapped up manually to 35A
Vacuum stable, IGP1 = 5e-7 Torr
Initiating auto-ramp.
OMEGA slope = 0.98
TBHT will be ramped up to 230A at 1.0A/min.
TGHT will be ramped up to 300A at 2.0A/min.
Final desired temperature = 1900C
Friday, October 14, 2016, 13:28
TGHT and TBHT had reached 300A/ 230A respectively.
Power bump ~10min ago caused evap2 to trip off.
Tapped back up manually to 35A.
Re-initiating auto ramp now.
|
Friday October 14: the target was ramp up to 300A/230A after Laura started it. Then, I cooled down at 6pm before leaving TRIUMF. <br>
Saturday October 15: restated the auto-ramp for Ta#50 in EVAP2. It's currently set to go to 300A/230A.
|
Sunday October 16: the target temperature measurements up to 620A/230A were performed today not on October 15 (yesterday, it was cooled down before reaching 300A/230A). Currently the target is cooling down, to be ready tomorrow morning for the Test Stand. |
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332
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Saturday, October 15, 2016, 12:42 |
Aurelia Laxdal | Ta | 41790-5 | LP-SIS | In progress | Temperature measurements for Ta#50 |
Laura Lambert wrote: |
Thursday, October 13, 2016, 18:04
Target loaded into evap2
No heat shields.
Both endcaps inserted and expanded.
Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]
Chamber pumped down.
HS water valves opened, no leaks detected
Tapped up manually to 35A
Vacuum stable, IGP1 = 5e-7 Torr
Initiating auto-ramp.
OMEGA slope = 0.98
TBHT will be ramped up to 230A at 1.0A/min.
TGHT will be ramped up to 300A at 2.0A/min.
Final desired temperature = 1900C
Friday, October 14, 2016, 13:28
TGHT and TBHT had reached 300A/ 230A respectively.
Power bump ~10min ago caused evap2 to trip off.
Tapped back up manually to 35A.
Re-initiating auto ramp now.
|
Friday October 14: the target was ramp up to 300A/230A after Laura started it. Then, I cooled down at 6pm before leaving TRIUMF. <br>
Saturday October 15: restated the auto-ramp for Ta#50 in EVAP2. It's currently set to go to 300A/230A. |
|
331
|
Thursday, October 13, 2016, 18:05 |
Laura Lambert | Ta | 41790-5 | LP-SIS | In progress | Temperature measurements for Ta#50 | Thursday, October 13, 2016, 18:04
Target loaded into evap2
No heat shields.
Both endcaps inserted and expanded.
Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]
Chamber pumped down.
HS water valves opened, no leaks detected
Tapped up manually to 35A
Vacuum stable, IGP1 = 5e-7 Torr
Initiating auto-ramp.
OMEGA slope = 0.98
TBHT will be ramped up to 230A at 1.0A/min.
TGHT will be ramped up to 300A at 2.0A/min.
Final desired temperature = 1900C
Friday, October 14, 2016, 13:28
TGHT and TBHT had reached 300A/ 230A respectively.
Power bump ~10min ago caused evap2 to trip off.
Tapped back up manually to 35A.
Re-initiating auto ramp now.
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