Thursday, September 22, 2011, 20:21

Target oven was wrapped with 3 Ta-heat shields and has been pumping down.

IG currently @ 3.2e-6 Torr, BP @ 25mT. 

TGHT stepped up to 85A, 

Began auto-heating: TGHT to max 580A @ 0.5A/min. 

Monday, September 26, 2011, 10:23 

TGHT reached to 580A on last Friday and was held at that current for 3hrs then followed by the auto-cooling.

Chamber was vented.

Target oven looks great.

Thursday, September 29, 2011, 10:54

UO2/C mixture was made on Tuesday Sept 27, casted on a piece of glass and let dried in the fume hood for ~2days. 

Dried UO2/C mass = 61.72g

Target material is wrapped /w graphite sheet and put on a new heatboat coated/sintered /w TaC.

Heat boat is wrapped with 3-Ta heat shields. 

Evaporator chamber is currently being pumped down. 

Friday, September 30, 2011, 10:01

Evaporator has been pumped down over night, IG currently @ 2.92e-6 Torr, BP @ 27mT.

TGHT will be stepped up to 40A and allow the pressure to slowly increase.  

Friday, September 30, 2011, 10:30  

TGHT is holding at 40A/0.139V  (local @ 37A), and pressure is slowly increasing, expect pressure to stabilize at ~4.5e-5 Torr before being auto-heating.

See attachment#1: TGHT_40A. 

Friday, September 30, 2011, 13:39

TGHT has been at 40A for more than 3 hrs.  Pressure went as high as 6.9e-5 Torr and it's now coming down.  (See attachment#2:  TGHT@40A_3hrs)

Auto-heating is initiating.  TGHT rate @ 0.1A/min to reach to max current of 525A.  (see attachment#3: parameter.jpg) 

Sunday, October 09, 2011, 10:44  

Target heater reached to 520A and held for a few hours.  

Evaporator was cooled down last night and TGHT is now at 0A.

(For the overall process, see Attachment#4: UCx#3_batch1.jpg) 

IG1 @ 5.7e-7 Torr.  Chamber will be vented with Ar on Tuesday. 

TGHT is off and water valve is shut.  

 Tuesday, October 11, 2011, 13:10

Evaporator glovebox was purged with Ar prior to venting the chamber with Ar.  

Layers of burnout marks were coated all around the inside of the evaporator (see attachment#5. Evpr_afterprocess.jpg), 

Before cleaning, the evaporator chamber had ~200,000 cpm. 

The heating boat containing UCx was removed from the evaporator and stored in the "orange" case, then transferred to the Ar-glove box.

Weight of UCx flasks:  47.15g (See attachment#6: UCx#3_batch1_mass.jpg)

The evaporator was thoroughly cleaned; the burnout marks were removed, and it will be used for UCx#3:batch#2 - UO2/C process.

 Thursday, October 06, 2011, 12:19

UO2/C mixture was made on Oct 4 and casted on a piece of glass costed with WD40, and let dried in the fume hood for 2days. 

Dried UO2/C mass = 64.95g

The batch is wrapped with a piece of graphite sheet and waiting to be heated in the evaporator.  

Currently, batch#1 is in the evaporator.

 Wednesday, October 12, 2011, 10:52

UO2/C mixture was loaded on a heatboat and wrapped with 3-Ta heat shields. 

Evaporator has been pumped down overnight, IG currently at 1.57e-6 Torr.

TGHT will be stepped up to 40A. 

Wednesday, October 12, 2011, 11:00  

TGHT @ 40A/0.128V, local @ 37A. IG @ 1.7e-6 Torr.  

Wednesday, October 12, 2011, 12:35 

TGHT tripped off @ 40A due to high vacuum (>8E-5 Torr).  See attachment#1

Vacuum has come down to 8.5e-6 Torr. 

Stepped up TGHT to 35A.

Wednesday, October 12, 2011, 15:19  

TGHT was held at 35A for 2.5 hrs.  IG @ 4.5e-5 Torr.

Initiated auto heating @ 0.1A/min, Max current @ 525A. 

 Thursday, October 20, 2011, 16:15

Vacuum suddenly increased to ~ 7.7e-5 Torr when TGHT @ 317A (see attachment#2).  There could be a shift in the material during the thermal reduction,

and caused a sudden spike in vacuum.

Currently, IG @ 5.2e-5 Torr, TGHT @ 316.7A.

TGHT reached to 525A and held for >4hrs before cooling down (see attachment#3)

UCx was removed from the evaporator and transferred to the Ar-glove box.  

The material looks great! 

 Thursday, November 03, 2011, 08:59

Target was previously coated/sintered with TaC & wrapped with 3 Ta-heat shields, including the back-block. 

Target was loaded with 365 UC2 discs + 3 samples for analysis. 

One regular endcap and one D-cap on the other end where the 3 samples sit. 

Evaporator has been pumped down since last night.  Currently vac @ 2.0e-6 Torr.  

For this final conditioning, here are the instructions: 

1.  Slowly stepping up TGHT  to 100A to burn off the organic binder.  Vacuum is expected to rise to the limit and stay at the plateau for a few days.  

2.  Once the vacuum has come down, the target will be cooldown and the chamber will be vented with Ar.  The cup-holder may be filled with the organic binder and needed to be clean.

3.  Pump back down the evaporator; step up TGHT to 100A and wait for the reaction. 

4.  Initial TGHT auto ramping.  Set TGHT to 520A @ rate of 0.1A/min.  

5.  Allow TGHT to held at 520A for 4 hours, then cool down. 

6.  Remove target from the chamber and store in the air-tight box and transferred to the Ar-glove box. 

Thursday, November 03, 2011, 09:13 

TGHT reached to 55A, and vacuum slowly to rise. Vac @ 5.7e-6 Torr. 

Wil stay at 55A for now... 

 Thursday, November 03, 2011, 09:51

A spike in vacuum and triggered the alarm handler but didn't tripped the TGHT.

Brought TGHT back down to 50A.

Initiated Auto-heating.  Set TGHT to 100A @ 0.1A/min. 

Thursday, November 03, 2011, 18:25  

I just found out that the target heater did not reach to 100A.  The auto-heating was running to bring up TGHT to 100, but the readback stayed at 50A.  Peter K. was contacted.  We stopped the auto-heating program and instantly the target heating jumped to 100A.  Quickly, we brought down the heater to 50A.  (see attachment1 for the stiptool).  Not sure what was happening.  

I stepped up the TGHT manually to 61A, and the pressure is slowing increasing.  

Thursday, November 03, 2011, 19:26  

Something is wrong with the TGHT power supply.  I stepped it up from 55 to 63A, and found the readback stuck at 58 (local @ 56).  So, I tapped the TGHT down to 58A and then the readback followed the setpoint.

I tried again to bring it up to 63 and it stuck at 60A, and tapping down and up the slider triggered the readback to follow the setpoint.  This is a fault in the system. 

Peter was informed, and is taking over this for now.  We need to bring up the THGT up to 100A to burn off the organic binder.  I don't know what we should do from here.  I need a break! 

Friday, November 04, 2011, 15:46  

As per Jane,  there is a problem with the network issue that controls the target heater power supply.  The power supply current is not regulating proper.  (see attachment #2)

TGHT was ramped down from 85A to 0A for Control to work on the problem since this morning.  

See e-fault#5672, WP#2011-11-04-5. 

 Monday, November 07, 2011, 11:12

 Control has fixed the network issue.  

Stepped up to 10A, local read 8A.

 Initiated autoramping, setp TGHT to 20A at 1A/min.  TGHT did reach to 20A with no problem.  

Stepped up further to 30A, local at 28A.  

I conclude that the power supply is now regulating properly.  

Conditioning of UCx#3 continues... 

 Monday, November 07, 2011, 12:14

TGHT at 84.5A, locat @ 82A.  Vacuum hovering at 7.2e-5 Torr.  

Initiated auto-ramping: TGHT set to 100A, at 0.1A/min.  Incrementing current if vac < 5.0e-5 Torr and backing off if vac >6.0e-5 Torr. 

Monday, November 14, 2011, 11:03 

TGHT reached to 175A on Nov 11, 2011 to finish off the organics burnout process. 

Then TGHT was cool down @ 2A/min until TGHT reached to zero.

Evaporator was vented with Ar and the chamber was open.

The target was removed from the evaporator; the organic binder was condensed out from the D-endcap and some from the ionizer tube (See attachment 3 & 4).

One of the samples was retrieved for analysis, and the D-endcap was put back.

The target was installed back, and the chamber was pumped down. 

The sintering and thermal reduction processes continued with TGHT ramped up to 520A.  Heating rate @ 0.1/min. 

Target has been heated at 520A for ~5hrs, vac @ 5.35e-6 Torr. (see attachment 5). 

Wednesday, November 16, 2011, 13:42

 Target looks good.  It has been installed in the heatshield, and it's being stored in the Ar-golve box. 

Evaporator is now off.  

Evaporator was cleaned Nov 11 from after target was conditioned up to 175A. There was significant condensation of oily fluid on the left side where the target container was open (D-shaped end cap). There were also deposits in the hole for the ionizer, but the ionizer itself seemed to be clean.

 Tuesday, February 14, 2012, 20:58

Evaporator is setup for UO2/Nb sintering process.  

Target oven filled with 402 discs of UO2/Nb, 5.0cm in length with tot mass of 61.49g. 

The chamber has been pumped down for 7 hrs, vac is currently at 4.6e-6 Torr. 

Parament set as follow, see attachment 1. 

 TGHT ramped up to 57A.  Pressure is stabilizing at 3.8e-5 Torr.  

Auto heating initiated.  0.1A/min.  Max TGHT = 500A. 

Sunday, February 19, 2012, 11:41 

TGHT has stayed at 500A for >10hrs,  Vac levels at 2.9e-6 Torr.

Target cool down initiated @ 2A/min.

 Monday, February 20, 2012, 10:23

Target has been cooled down over the weekend.  Vac currently at 5.77e-7 Torr.  

See attachment#2: UO2_Nb_1_striptool.jpg 

Chamber  vented in atmosphere.   

Monday, February 20, 2012, 16:23 

Pumps/ power supplies off. 

Thursday, April 05, 2012, 16:43

Target oven is coated with TaC.  The oven is wrapped with 3 Ta-heat shields.

The chamber is currently being pumped down.  Vac @ high 10e-5 Torr.  Heater will be turned on once the pressure is gone down to low 10e-6. 

TGHT will be heated up to 820A.

**** Sintering is postponed until the situation with the ventilation in the lab06 is cleared. ****

 Friday, May 04, 2012, 16:59

The short-term solution  for improving the ventilation system and for the safety in operating the evaporators has been implement.  The test results was reviewed and approved by the committee.  The labs (06 and 07) are now back in operational. 

Friday, May 04, 2012, 17:03

Pumping down evaporator, currently a 2.4e-5 Torr.

Turned on TGHT, and stepped up to 85A.  Pressure remained at low e-5 Torr. 

Initiated Auto-heating at 0.5A/min to Max current 820A.  Parameter set:  Increasing current if Vac <4.0e-8 Torr, Backing current if Vac >5.0e-8 Torr.

 Monday, May 07, 2012, 10:38

At 820A, the TaC coating only seemed to have partially sinterred.  Raised TGHT up to 900A and heated for >6hrs.  The vacuum continued to increase as the target heater was raised; that indicated the sintering reaction was ongoing.  (See attachment #1: Targetoven_TaCsintered_acrchive.jpg).

The auto-cool down was initiated last night.  TGHT is now at 0A.  The chamber will be vented.

Tuesday, May 08, 2012, 07:32

Target oven is filled with 240 discs of SiC/C, and wrapped with 3 Ta-foils.

Tot mass= 31.95g (SiC + C foil + Org)

Tot length packed @ 8.2cm

Target was installed in the chamber yesterday and has been pumped down to low 10e-6 torr.

Increased TGHT to 70A and vacuum is starting to rise, currently at 2.6e-6 Torr.

Max target current = 820A or until there is no further reaction. 

 Tuesday, May 08, 2012, 08:55

Pressue is slowly coming down after heating for a while at 70A. 

Initiated auto heating at 0.5A/min. Parameter set for increasing current if <4.0e-5 torr, and backing off if >5.0e-5 torr.

Wednesday, May 09, 2012, 10:31

 There seems to be a pipe leakage in the ISAC-I B2 level, and the cooling water for the evaporator #1 is connected to the pipe.  

The TGHT was tapped down from 115A, and the p/s was turned off.  The water valve is now shut, and Curtis B. is looking into it.  

Wednesday, May 09, 2012, 13:44

As per Curtis, the drainage pipe was leaky, and it has been fixed. The evaporator is now turned back on.  TGHT was tabbed up to 115A, and has remained at that current for an hour.  The pressure is slowly raising, current at 4.6e-6 Torr.

Wednesday, May 09, 2012, 14:24

Initiated TGHT...

Saturday, May 12, 2012, 23:38 

TGHT is ramping up very slowly (currently at 270A) due to pressure restriction.  It has already taken over 4 days.  (see attachment 1: TGHT 0_270A)

Changed the parameter to <5.0e05 Torr for stepping up in current and >6.0e-5 Torr for backing off current.

 Sunday, May 13, 2012, 20:44

Pressure has started to come down to 3e-6 Torr.  Increased heating rate from 0.5A/min to 1.0A/min.

 Monday, May 14, 2012, 01:09

TGHT has reached to 820A and been holding at that current for about 3hr.  The pressure is coming down steadily, currently at 1.6e-5 Torr.

Asked ISAC OPS (Ed P.) to initial the auto-cool down at 03:00h, at 2A/min.

The target should be ready by 10:00h.

 Monday, May 14, 2012, 10:56

TGHT is now at 0A (see attachment 2).  The chamber is now being vented.  The target will be inspected.

Thursday, May 17, 2012, 12:51 

The target looks good and was tested in the teststand, see https://elog.triumf.ca/TIS/Test-Stand/97

It will be used as SiC#27.  

Wednesday, June 06, 2012, 16:55

The UO2/C green was prepared on June 04, 2012. 

UO2 powder used = 50.26g

C-grv used = 10.14g. 

Dry UO2/C green mass = 61.71g.

The green was rolled and wrapped in a piece of graphite sheet.

The target boat was wrapped with 3 Ta-heat shield and installed in the Evap#1. 

The chamber is currently being pumped down.

 Tuesday, June 12, 2012, 11:42

Currently, IEVAPIG1= 1.83e-6 Torr, IEVAP:CG2= 48 mTorr.

Backing line pressure is slightly high.  Will get Edi to look into this.

 Tuesday, June 12, 2012, 14:38

The backing pump oil was changed (ISAC WP#2012-06-12-1).  IEVAP:CG2 is currently reading 27mTorr and IEVAPIG1 at 1.66e-6 Torr.

 Tuesday, June 12, 2012, 16:06

TGHT was tabbed up to 50A and stayed for 1.5 hrs.  Not much change in the pressure, currently at 1.8e-6 Torr, BP @ 25mTorr.  

Keep stepping up TGHT current...

 Tuesday, June 12, 2012, 16:37

TGHT at 65A.  Pressure is starting to rise.

 Tuesday, June 12, 2012, 16:46

Pressure at  6.8e-6 Torr and going up slowly. 

Initiated TGHT auto-ramping:

Max current = 525A,  rate @ 0.1A/min (see attachment #1)

 Wednesday, June 13, 2012, 13:22

TGHT has almost reached to 80A.  Pressure is limiting at 4.5e-6 Torr. (see attachment#2)

Thursday, June 14, 2012, 17:11

TGHT has reached to 95.40A, local @ 92A & 0.48V.  Pressure is still limiting at 4e-6 Torr.  (see attachment #3)

The TGHT current can not go up above 232A because it's voltage limiting at 1.953V (see attachment#4).  The carbon thermal-reduction process stops and the vacuum is going down to low 10e-6 Torr. 

The voltage can not be increased on EPICS; it has to be adjusted locally.  

Auto-ramping aborted.  

The TGHT current setpoint was lowered down to 228A.

Sunday, June 17, 2012, 12:03  

Asked ISAC Ops (Ed Parton) to help me increase the voltage locally.  The voltage nob was turned 1/4 clockwise, and the current was tapped up from 228 to 231A, and it was responding.  The voltage nob was further turned to 3/4 clockwise. 

Initiated auto-ramping. 

Currently, TGHT setpoint at 234.90A, local 231A/1.95V.  

Vacuum is responding and it's slowly going up (currently at 2.8e-6 Torr) - The carbon thermal reduction process continues... 

Monday, June 18, 2012, 00:20  

TGHT is going up slowly, currently at  285A.  The pressure is limiting as the carbonization process is under way (see attachment 5).

 Monday, June 25, 2012, 16:00

The EPICS control was down on Sunday night. So the auto-ramping was aborted.  

Control group fixed the problem, and the network is back online.

The auto-ramping has been re-initiated. 

TGHT is currently at 314.70A, local at 311/3.04V.  IG at 4.21e-5 Torr, BP at 15mTorr.

 Saturday, June 30, 2012, 23:08

The carbonization process has finished.

TGHT has reached to 520A and maintained at that current for about 5hrs. (see attachment #6).

Initiated auto-cool down.

Tuesday, July 03, 2012, 13:05 

TGHT is now at 0A.  The carbonization process is done.  

It took over 20 days for this process (see attachment #7), due to some control issues & power supply problem. Also the vacuum limit was set to 4.0e-5 Torrr; that might increase the pumping time.  

Next time, try setting the pressure limit to 5.0e-5 Torr.  

The chamber will be vented with Ar, and the UC2 flakes will be transferred to the Ar-glove box.  

Tuesday, July 10, 2012, 12:44

Target contains 230 discs of UCx (material from UC2 flakes, batch#01-04062012). 

Total UCx mass (UC2 + C-grv extra + C-foil + Org.) = 38.564g

Total length = 8.0 cm

Target was previously contained with TaC and sintered;  it's wrapped with 3 layers of Ta-heat shield, including the back-block.

A regular TaC-coated endcap is inserted on one end and the other is inserted with a D-cap with two samples  (Marked sample #1 & #2).

The chamber is currently being pumped down.

 Tuesday, July 10, 2012, 19:06

IG currently at 9.1e-6 Torr, BP @ 22mTorr.  

Set TGHT auto-ramping parameters:  

Vacuum limit 5.0 e-6 Torr, (max 6.0 e-6 Torr)

rate = 0.25A/min

TGHT = 55A  

Initiated auto-ramping...

 Tuesday, July 10, 2012, 23:20

TGHT reached to 55A and stayed for about 55min.  The pressure was at 2.5e-5 Torr.

Increases TGHT auto-ramping to 175A to allow burning off most of the organic binder, and the chamber will be vented and cleaned before ramping 

up the heater to 520A.

Ramping rate set to 0.1A/min.

Monday, July 16, 2012, 09:44 

TGHT reached to 175A.  It has taken almost 6 days to burn off the organic binder. (see attachment #1).  

Auto-cool down has initiated.  The chamber will be vented with Ar gas and it will be opened for cleaning of the burn-off binder. 

 Monday, July 16, 2012, 14:20

The chamber was vented with Ar, and the target was removed for cleaning.  There was quite a bit of organic gunge filled the ionizer holder-base plate and condensation out the D-cap (as usual).

The chamber was cleaned and the target was installed back.  It's currently being pumped down.

Once the vacuum reached to 10e- Torr.  The heater will be ramped up to max 520A to finish the sintering process.

 Monday, July 16, 2012, 17:01

Pressure has reached to 9.1e-6 Torr. 

Initiated auto-heating at 1A/min.  Set TGHT = 175A.

 Monday, July 16, 2012, 20:00

TGHt reached to 175A.  Pressure stable at 2.2e-5 Torr.  

Increase target heater to 520A; autoramping at 0.1A/min. 

 Thursday, July 19, 2012, 10:27

TGHT reached to 520A, 5.47V (local 516A, 5.36V) and has stayed for about 4 hours.  IG1 = 9.58e-6 Torr and coming down.  BP=29mTorr.

Thursday, July 19, 2012, 10:29

Auto-cooling down in process...  2A/min for TGHT --> 0A.

 Thursday, July 19, 2012, 16:52

The chamber was vented with Ar gas, and the target was transported to the Ar-glove box. 

The samples were removed from the target.

A new TaC-sintered end-cap was inserted.

The target looks good!

Total time for the conditioning process = 9 days.

See attachment#2 for the overall heating/pressure curves.

Thursday, July 19, 2012, 17:09

UO2/C green was prepared on June 13, 2012. 

UO2 powder used = 50.32g (Inventory R-00835A UO2 + bottle = 946.48g left)

Graphite powder used = 10.00g

The green was rolled and wrapped in a piece of graphite sheet.

The target boat was wrapped with 3 Ta-heat shield and installed in the Evap#1. 

The chamber is currently being pumped down.

 Friday, July 20, 2012, 09:50

IG1 currently at 6.2e-6 Torr, BP @ 31mTorr. 

The target will be ramped up to 520A at 0.1A/min. 

Vacuum limit stop at 5.0e-5 Torr, backing off at 6.0e-5 Torr.

TGHT tabbed up to 50A.  Not much of change in the vacuum.

Initiated autoramping..

Friday, July 20, 2012, 10:18  

TGHT tripped up at 51A due to high vacuum.  

Lowered TGHT to 30A and begin auto ramping.  Pressure is holding at 7e-5 Torr. 

 Wednesday, July 25, 2012, 11:57

TGHT has reached to 100A, and the vacuum is starting to come down from the high limit, 5e-5 Torr. (see attachment#1).  

The organic burn-off is almost to complete and the carbonization process will begin soon. 

Tuesday, August 07, 2012, 12:18

The carbonization process is completed.  The target heater reached to 520A (local 515A,5.17V), vacuum at 4.0 e-6 Torr. (see attachment #2)

Cooling down is in process at 2A/min.

 Tuesday, August 07, 2012, 17:44

TGHT has reached to 0A.  IG currently @ 1.3e-6 Torr, BP @ 34mTorr. 

The chamber will be vented with Ar gas tomorrow and the UC2 flakes will be transfer to the Ar-glove box.

Tuesday, April 02, 2013, 17:25

UO2/C green was prepared on Mar 11, 2013.

UO2 powder used = 50.32g (Inventory R-00835A UO2 + bottle = 896.16

Graphite powder used = 10.00g

The green was rolled and wrapped in a piece of graphite sheet

The target boat was wrapped with 3 -Ta heat shields and installed in the Evap#1.

The chamber is currently being pumped down.

The target will be ramped up to 520A at the rate of 0.1A/min. 

Vacuum limit stop at 5.0e-5 Torr, backing off at 6.0e-5 Torr.

 Wednesday, April 03, 2013, 11:28

IG1 currently at 3.56e-6 Torr, BP at 28mTorr.

Tabbing up TGHT to 50A.

After 20 mins, IG got up to 7.5e-5 torr (tripping at 8e-5 Torr).  Lower TGHT to 20A. 

Initiated autoramping...

 Monday, April 15, 2013, 14:33

The domestic water will be shut off tomorrow, April 16 at 07:00 for ARIEL work.  The evaporator cooling water will be shut off; therefore the process must stop for now.

TGHT is current at 315.5A, IG1 at 5.2e-5 Torr. 

Cooling down at 1A/min.

 Tuesday, April 16, 2013, 16:28

The cooling water is back online.  The carbonization process will continue...

TGHT will be ramped up to 300A at 2A/min.  Then the ramping rate will changed to 0.1A/min to have TGHT reach to 520A.

IG is currently at 1.2e-6 Torr.

 Wednesday, April 17, 2013, 10:53

TGHT continues to ramp at 0.1A/min.

 Sunday, April 21, 2013, 22:11

The synthesis of UC2 is complete. 

Auto cooling is initiated.  Ramping down at 1A/min.

The chamber will be vented with Ar tomorrow.

Monday, May 06, 2013, 14:29

UO2/C green was prepared on May 2, 2013 and let dry over the weekend.

UO2 powder used = 50.36g   (Inventory R-00835A UO2 + bottle = 896.30)

Graphite powder used = 10g

The green was rolled up and wrapped in a piece of graphite sheet.

The Ta-target boat was wrapped with 3-Ta heat shields and installed in the Evap#1

The chamber is currently being down down.

The target will be ramped up to 520A at the rate of 0.1A/min.

Vacuum limit stop at 5.0e-5 Torr, backing off at 6.0e-5 Torr.

 Tuesday, May 07, 2013, 11:12

Currently, IG @ 5.6e-6 Torr; BP @ 25mTorr.  Vacuum spikes intermittently...

Stepping up TGHT to 50A.  After about 15 min, vacuum climbed up to 5.5e-5 Torr. 

Lowered TGHT to 25A, and continue heating at that current...

 Tuesday, May 07, 2013, 12:18

Vacuum is coming down to 2.6e-5 Torr.

Auto-heating initiated...

 Friday, May 24, 2013, 14:19

The carbonization process has come the end.

TGHT has reached to 520A for ~14hrs. 

IG1 @ 6.34e-6 Torr, BP @ 25mTorr.

Autocooling is initiated; ramping rate @ 1A/min.

The chamber will be remained under vacuum, and will be vented in Ar next week.

 Monday, May 27, 2013, 14:11

The chamber was vented with Ar. 

UC2 was transfered to the Ar glovebox. 

Evap#1 is off.

 Wednesday, May 29, 2013, 17:14

See attachment#1 for TGHT vs IG1 data retrieval.

Thursday, May 30, 2013, 16:16

The target container was previously coated with TaC and sintered in Evap 2.

The target is loaded with 250 discs of UCx (material from batch#03_02042013)

Total length = 8.9cm

The container is wrapped with 3 layers of Ta-heat shield, including the back block.

A regular TaC coated/sintered endcap is inserted on left, wrt to the ionizer tube pointing out of the page.  The right end is open with no cap. 

(Did not use a D-cap... trying out this method.  Need to be careful when handling the target!)

The chamber is dumping down.

 Instructions for conditioning the UCx target:

1.  TGHT will need to heat up to ~175A to burn off the organics. 

      Parameter setup:  5.0e-5 good vac, 6.0-5 bad vac.  The auto-ramping rate is set to 0.1A/min.

2.  Once the organics have burnt off, ramp down the TGHT to 0A at 2A/min.

3.  Purge the glovebox with argon gas. 

4.  Vent the chamber with Ar gas.  Close the valve when it is completely vented.

5.  Remove the target.  Be careful the left end (view from the top) is open with the D-cap. 

6.  Clean the chamber with TCE and remove all the gunge.

7.  Install the target back

8.  Pump down the chamber to at least low 10e-6 Torr before begin the final carbonization process.

9.  Auto-ramp the TGHT current to 175A at 1A/min.

10.  Once the TGHT reach to 175A.  Auto-ramp TGHT to 520A at 0.1A/min.

11.  At 520A, keep heating the target for at least 4-5 hours.

12.  Auto ramp TGHT to 0A at 2A/min.

13.  Purge the glovebox with argon for at least 5 min

14.  Vent the chamber with argon gas.  Close the vavle when it is completely vented.

15.  Remove the target from the chamber and put in the "orange box" and transport to the Ar-glove box.

Done!

 Friday, May 31, 2013, 18:17

Chamber has pumped down to 6.7e-6 Torr. 

Ramping up TGHT to 175A.

 Wednesday, June 05, 2013, 11:14

TGHT reached to 227A/1.99V. (see attachment#1)

TGHT is ramping down to 0A  to clean up the chamber before continue with the conditioning.

John Wong wrote:

Thursday, May 30, 2013, 16:16 The target container was previously coated with TaC and sintered in Evap 2. The target is loaded with 250 discs of UCx (material from batch#03_02042013) Total length = 8.9cm The container is wrapped with 3 layers of Ta-heat shield, including the back block. A regular TaC coated/sintered endcap is inserted on left, wrt to the ionizer tube pointing out of the page.  The right end is open with no cap.  (Did not use a D-cap... trying out this method.  Need to be careful when handling the target!) The chamber is dumping down.  Instructions for conditioning the UCx target: 1.  TGHT will need to heat up to ~175A to burn off the organics.        Parameter setup:  5.0e-5 good vac, 6.0-5 bad vac.  The auto-ramping rate is set to 0.1A/min. 2.  Once the organics have burnt off, ramp down the TGHT to 0A at 2A/min. 3.  Purge the glovebox with argon gas.  4.  Vent the chamber with Ar gas.  Close the valve when it is completely vented. 5.  Remove the target.  Be careful the left end (view from the top) is open with the D-cap.  6.  Clean the chamber with TCE and remove all the gunge. 7.  Install the target back 8.  Pump down the chamber to at least low 10e-6 Torr before begin the final carbonization process. 9.  Auto-ramp the TGHT current to 175A at 1A/min. 10.  Once the TGHT reach to 175A.  Auto-ramp TGHT to 520A at 0.1A/min. 11.  At 520A, keep heating the target for at least 4-5 hours. 12.  Auto ramp TGHT to 0A at 2A/min. 13.  Purge the glovebox with argon for at least 5 min 14.  Vent the chamber with argon gas.  Close the vavle when it is completely vented. 15.  Remove the target from the chamber and put in the "orange box" and transport to the Ar-glove box. Done!  Friday, May 31, 2013, 18:17 Chamber has pumped down to 6.7e-6 Torr.  Ramping up TGHT to 175A.  Wednesday, June 05, 2013, 11:14 TGHT reached to 227A/1.99V. (see attachment#1) TGHT is ramping down to 0A  to clean up the chamber before continue with the conditioning.

 Wednesday, June 05, 2013, 16:45

Glove box purged with Ar, ~30min

Chamber vented with Ar

Target removed. chamber cleaned with TCE.

Chamber pumped back down

IG1 currently at 1.4E-4 torr

See attachment 1 before chamber was cleaned

Thursday, June 06, 2013, 11:38

Chamber has been pumped down overnight

IG1 currently at 4.7E-06 Torr, BP at 30 mTorr

TGHT will be ramped up to 220A at 1A/min

Laura Lambert wrote:

John Wong wrote: Thursday, May 30, 2013, 16:16 The target container was previously coated with TaC and sintered in Evap 2. The target is loaded with 250 discs of UCx (material from batch#03_02042013) Total length = 8.9cm The container is wrapped with 3 layers of Ta-heat shield, including the back block. A regular TaC coated/sintered endcap is inserted on left, wrt to the ionizer tube pointing out of the page.  The right end is open with no cap.  (Did not use a D-cap... trying out this method.  Need to be careful when handling the target!) The chamber is dumping down.  Instructions for conditioning the UCx target: 1.  TGHT will need to heat up to ~175A to burn off the organics.        Parameter setup:  5.0e-5 good vac, 6.0-5 bad vac.  The auto-ramping rate is set to 0.1A/min. 2.  Once the organics have burnt off, ramp down the TGHT to 0A at 2A/min. 3.  Purge the glovebox with argon gas.  4.  Vent the chamber with Ar gas.  Close the valve when it is completely vented. 5.  Remove the target.  Be careful the left end (view from the top) is open with the D-cap.  6.  Clean the chamber with TCE and remove all the gunge. 7.  Install the target back 8.  Pump down the chamber to at least low 10e-6 Torr before begin the final carbonization process. 9.  Auto-ramp the TGHT current to 175A at 1A/min. 10.  Once the TGHT reach to 175A.  Auto-ramp TGHT to 520A at 0.1A/min. 11.  At 520A, keep heating the target for at least 4-5 hours. 12.  Auto ramp TGHT to 0A at 2A/min. 13.  Purge the glovebox with argon for at least 5 min 14.  Vent the chamber with argon gas.  Close the vavle when it is completely vented. 15.  Remove the target from the chamber and put in the "orange box" and transport to the Ar-glove box. Done!  Friday, May 31, 2013, 18:17 Chamber has pumped down to 6.7e-6 Torr.  Ramping up TGHT to 175A.  Wednesday, June 05, 2013, 11:14 TGHT reached to 227A/1.99V. (see attachment#1) TGHT is ramping down to 0A  to clean up the chamber before continue with the conditioning.      Wednesday, June 05, 2013, 16:45 Glove box purged with Ar, ~30min Chamber vented with Ar Target removed. chamber cleaned with TCE. Chamber pumped back down IG1 currently at 1.4E-4 torr See attachment 1 before chamber was cleaned     Thursday, June 06, 2013, 11:38 Chamber has been pumped down overnight IG1 currently at 4.7E-06 Torr, BP at 30 mTorr TGHT will be ramped up to 220A at 1A/min

 Thursday, June 06, 2013, 16:53

TGHT has reached to 220A; continue ramping up to 520A at 0.1A/min rate.

 Monday, June 10, 2013, 12:28

TGHT has reached to 520A; target has been heated at the current over the weekend.

IG is stabilizing at 3.7e-6 Torr. 

Initiating auto-cooling to 0A at 2A/min.

Chamber will be vented in Ar tomorrow.

 Monday, June 10, 2013, 17:50

TGHT reached to 0A. See attachment #1 for the overall process. 

 Tuesday, June 25, 2013, 14:35

UO2/C green was prepared on June 18, 2013 and let dry over the weekend.

UO2 powder used = 50.25g (Inventory R-00835A UO2 + bottle = 845.94g - before use)

Graphite powder used = 10.0g

The green was rolled up and wrapped in a piece of graphite sheet.

The Ta-target boat was wrapped with a 3-Ta heat shields and installed in the Evap#1 on June 24, 2013

The chamber has been pumped down

IG1 currently at 4.6E-06 torr

Target will be ramped up to 520A at the rate of 0.1A/min

Vacuum limit stop at 5.0E-05 torr, backing off at 6.0E-05 torr

Laura Lambert wrote:

Tuesday, June 25, 2013, 14:35 UO2/C green was prepared on June 18, 2013 and let dry over the weekend. UO2 powder used = 50.25g (Inventory R-00835A UO2 + bottle = 845.94g - before use) Graphite powder used = 10.0g The green was rolled up and wrapped in a piece of graphite sheet. The Ta-target boat was wrapped with a 3-Ta heat shields and installed in the Evap#1 on June 24, 2013 The chamber has been pumped down IG1 currently at 4.6E-06 torr     Target will be ramped up to 520A at the rate of 0.1A/min Vacuum limit stop at 5.0E-05 torr, backing off at 6.0E-05 torr

 Tuesday, June 25, 2013, 16:26

TGHT was stepped up to 30A for about 1hr and lowered to 20A before the pressure went up t0 ~ 1.5e-5 Torr.

Auto ramping initiated...

1. stage - burning off organics complete

2. stage - carbonization began 1-8 am 2013/07/02

Peter Kunz wrote:

1. stage - burning off organics complete 2. stage - carbonization began 1-8 am 2013/07/02

 Thursday, July 11, 2013, 16:11

EPICS was down and wiped out all the strip tools, but Evap stayed on.  Data archivers showed the system was down at around mid-night on July 10 - no data was archived for 12 hours. 

TGHT has stayed at 520A (max) for at least 4 hours since I started the Evap EPICS back.

Vacuum is currently at 7.7e-6 Torr. 

The carbonization process is complete.

Auto-cool down in process - at 1A/min.