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Message ID: 63     Entry time: Tuesday, April 02, 2013, 17:46
Author: John Wong 
Target Material: UO2/C 
Target Oven W.O#: Target boat #2 
Source:  
Status: Done 
Subject: Processing UC2 flakes for UCx#6 (batch#03 - 02042013) 

Tuesday, April 02, 2013, 17:25

UO2/C green was prepared on Mar 11, 2013.

UO2 powder used = 50.32g (Inventory R-00835A UO2 + bottle = 896.16

Graphite powder used = 10.00g

The green was rolled and wrapped in a piece of graphite sheet

The target boat was wrapped with 3 -Ta heat shields and installed in the Evap#1.

The chamber is currently being pumped down.

The target will be ramped up to 520A at the rate of 0.1A/min. 

Vacuum limit stop at 5.0e-5 Torr, backing off at 6.0e-5 Torr.


 Wednesday, April 03, 2013, 11:28

IG1 currently at 3.56e-6 Torr, BP at 28mTorr.

Tabbing up TGHT to 50A.

After 20 mins, IG got up to 7.5e-5 torr (tripping at 8e-5 Torr).  Lower TGHT to 20A. 

Initiated autoramping...


 Monday, April 15, 2013, 14:33

The domestic water will be shut off tomorrow, April 16 at 07:00 for ARIEL work.  The evaporator cooling water will be shut off; therefore the process must stop for now.

TGHT is current at 315.5A, IG1 at 5.2e-5 Torr. 

Cooling down at 1A/min.


 Tuesday, April 16, 2013, 16:28

The cooling water is back online.  The carbonization process will continue...

TGHT will be ramped up to 300A at 2A/min.  Then the ramping rate will changed to 0.1A/min to have TGHT reach to 520A.

IG is currently at 1.2e-6 Torr.


 Wednesday, April 17, 2013, 10:53

TGHT continues to ramp at 0.1A/min.


 Sunday, April 21, 2013, 22:11

The synthesis of UC2 is complete. 

Auto cooling is initiated.  Ramping down at 1A/min.

The chamber will be vented with Ar tomorrow.


 

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