ID |
Date |
Author |
Target Material |
Target Oven W.O# |
Source |
Status |
Subject |
175
|
Thursday, November 23, 2017, 13:39 |
Marla Cervantes | UO2/C | 40282-2 | TARGET BOAT | Done | Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#3 | Thursday, November 23, 2017, 13:34
Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]
A 14mm punch was used to punch out circles from the cast.
35 circles were packed into a graphite sample container.
35 x UO2/C circles = 5.75 g
Graphite container = 5.38 g
Graphite container is placed inside a target boat.
Boat previously coated with TaC and sintered.
Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.
Chamber currently pumping down.
Friday, November 24, 2017, 12:48
IGP1=1.3e-6 Torr
TGHT = 520A, 4.98V
Vacuum went down indicating carbonization.
Will remain at max setpoint for the weekend.
Monday, November 27, 2017, 09:58
IG1 = 2.6e-6 Torr
TGHT = 520A, 5.1V
Carbonization complete in 3 hrs and 30 min.
Initiating auto-cool at 2.0A/min
Wednesday, November 27, 2017, 13:10
IEVAP was vented in argon and sample removed/transferred to glove box on Friday. |
Attachment 1: 171124_1e-1.jpg
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174
|
Wednesday, November 22, 2017, 14:20 |
Laura Lambert | | | | Maintenance | New eye wash for hot lab! | Wednesday, November 22, 2017, 11:05
Eye wash installed yesterday, simple attachment on sink spout.
Easy to use, simply twist attachment 180 degrees.
Water for tap can be turned on before or after twist.
Adjust pressure/ temperature accordingly.
Auto shut-off for eye-wash at ~38C [100F] - no accidental eye-burning when trying to wash eyes!
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173
|
Tuesday, November 14, 2017, 16:16 |
Laura Lambert | UO2/C | 40282-2 | TARGET BOAT | Done | Carbonizing UC2 discs for 1stepUCx in graphite sample container _#2 | Tuesday, November 14, 2017, 16:12
Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]
A 14mm punch was used to punch out circles from the cast.
35 circles were packed into a graphite sample container.
35 x UO2/C circles = 5.43g
Graphite tube is placed inside a target boat.
Boat previously coated with TaC and sintered.
Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.
Chamber currently pumping down.
Wednesday, November 15, 2017, 08:53
IGP1 = 1.6e-6 Torr
Tapping up manually...
Wednesday, November 15, 2017, 11:59
IGP1 = 5.0e-5 Torr
Tapped up entire process manually to 520A in 3hrs!!!
TGHT = 520A, 4.98V
Vacuum coming down nicely indicating carbonization process complete
Will remain at max setpoint for 4hrs to ensure full carbonization before cooling down later this afternoon.
Wednesday, November 15, 2017, 15:16
IG1 = 8.65e-6 Torr
TGHT = 520A, 4.92V
Carbonization complete.
Initiating auto-cool at 2.0A/min
Monday, November 20, 2017, 13:28
Evap1 was vented in argon and sample removed/ transfered to glove box on friday.
Discs look good, slightly lighter grayer compared to production UCx discs after second cast but before final carbonization.
Material seems to adhere to graphite backing foil well, no flakes coming off from just moving discs around.
Weight of 35 carbonized discs = 4.387g
Weight loss = 5.43g - 4.387g = 1.043g
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Attachment 1: striptool.JPG
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172
|
Tuesday, November 07, 2017, 14:38 |
Laura Lambert | Empty | | LP-FEBIAD | Done | TBHT test with LP-FEBIAD | Tuesday, November 07, 2017, 14:34
LP-FEBIAD used several years ago for temperature measurements is used for this test.
3xTa heat shields on container, incl center block - these heat shields have remained on there since the last round of tests in 2014?
Old version of LP container with larger center block.
Will heat TBHT to 290A and report data.
Loaded into evap1 and pumped down this a.m
IGP1 = 7.73e-6 Torr
Wednesday, November 08, 2017, 13:20
Tapped up to 290A manually.
TBHT epics controls = 287.7A, 2.45V
TBHT power supply = 290.4A, 2.46V
IGP1 epics = 2.51e-6 Toor
IGP1 direct readout = 3.18e-6 Torr
TP = 26.1C
Initiating auto-cool at 2.0A/min
Thursday, November 09, 2017, 11:41
Vented in air.
TBHT test went well.
See attachment for data collected.
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Attachment 1: evap1_data.xlsx
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171
|
Tuesday, November 07, 2017, 12:04 |
Laura Lambert | | | | Maintenance | Noise levels checked - ear protection not required. | Tuesday, November 07, 2017, 11:58
Noise levels were checked with monitor by Terry.
Max readings in lab reached ~83dB but sat between 70-78dB in most areas.
This is under limit for requirement to wear ear protection [85dB].
To reach limit - noise levels would need to increase drastically.
Conclusion: ear protection not required in lab.
Recommended if working in there for long periods of time for personal preference, but not a requirement.
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170
|
Tuesday, November 07, 2017, 11:57 |
Laura Lambert | | | | Maintenance | Interlocks limits changed to 100mTorr | Tuesday, November 07, 2017, 11:55
Interlocks limits updated/ changed to 100mTorr for both TGHT and TBHT by Ray
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169
|
Tuesday, October 10, 2017, 14:16 |
Laura Lambert | UO2/C | 40282-1 | TARGET BOAT | Done | Processing UC2Flk_19 | Tuesday, October 10, 2017, 14:11
UO2/C green was prepared Oct 4th, 2017
The cast peeled off the glass nicely Oct 6th, 2017
Initial UO2 powder used = 50.26g (Inventory R-01032A, UO2 + bottle = 676.34g before use)
Graphite powder used = 10.12g
Green cast dried UO2/C + organic mass = 61.30g
The green was rolled up and wrapped in a piece of graphite sheet.
The Ta-target boat was wrapped with 3-layers of heat shield [reused] and installed in evap1 this morning.
Chamber currently pumping down.
Target boat will be ramped up to 520A.
Vacuum limit stop at 3.0e-4 Torr, backing off at 6.0e-4 Torr.
Wednesday, October 11, 2017, 09:06
IGP1 = 1.74e-6 Torr
Tapped up to 35A, 0.29V
Waited ~70min, vacuum stable.
IGP1 = 6.9e-6 Torr
Initiating auto-ramp at 0.2A/min
Wednesday, October 11, 2017, 13:06
IGP1 = 3.1e-4 Torr
TGHT = 61A, 0.49V
Vacuum stable.
Changing vacuum limits.
Vacuum limit stop at 5.0e-4 Torr, backing off at 8.0e-4 Torr.
Thursday, October 12, 2017, 08:31
IGP1 = 1.06e-5 Torr
TGHT = 275A, 2.55V
Vacuum stable.
Increasing ramping rate to 0.5A/min.
Thursday, October 12, 2017, 09:03
IGP1 = 1.47e-5 Torr
TGHT = 290A, 2.70V
Vacuum stable.
Increasing ramping rate to 1.0A/ 30sec.
Friday, October 13, 2017, 08:30
IGP1 = 5.8e-6 Torr
TGHT = 520A, 4.98V
Vacuum stable.
Carbonization process complete!
Evap1 has remained at max setpoints for ~17hrs
Initiating auto-cool at 1.0A/min
Tuesday, October 17, 2017, 15:01
TGHT had sat at 0A for at least 24hrs.
At ~3:30-4am this morning everything tripped off. The only thing remained on was the roughing pump.
Power bump? Did someone accidentally turn it off? Will follow up on this...
Vacuum was sitting at ~3.5e-2Torr when I noticed today.
Most vacuum had been lost, but there was still a small vacuum - materials should be okay.
Purged and vented in Ar.
Transferred materials to glove box.
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168
|
Wednesday, September 27, 2017, 12:05 |
Laura Lambert | UO2/C | 40282-1 | TARGET BOAT | Done | Processing UC2Flk_18 | Wednesday, September 27, 2017, 09:25
UO2/C green was prepared Sept 20th, 2017.
The cast peeled off the glass Sept 22nd, 2017 - not quite enough 'special' ingredient.
UO2 stuck to glass around edges of cast - a lot of flakes produced while peeling off.
Initial UO2 powder used = 50.00g (Inventory R-01032A, UO2 + bottle = 726.38g before use)
Graphite powder used = 10.03g
Green cast dried UO2/C + organic mass = 60.38g
The green was rolled up and wrapped in a piece of graphite sheet.
The Ta-target boat was wrapped with 3-layers of heat shield [reused from last 1stepUCx] and installed in evap1 yesterday afternoon.
Chamber pumped down overnight.
Target boat will be ramped up to 520A.
Vacuum limit stop at 5.0e-5 Torr, backing off at 6.0e-5 Torr.
IG1 = 3.5e-6 Torr
Tapped up to 30A, 0.43V
Waited ~50min, vacuum stable.
IGP1 = 8.6e-6 Torr
Initiating auto-ramp at 0.1A/min
Wednesday, September 27, 2017, 13:28
IGP1 = 1.4e-5 Torr
TGHT = 38.5A, 0.48V
Vacuum stable.
Changing vacuum limits and ramping rate.
Vacuum limit stop at 2.0e-4 Torr, backing off at 5.0e-4 Torr.
Increasing ramping rate to 0.2A/min.
Thursday, September 28, 2017, 08:41
IGP1 = 3.26e-5 Torr
TGHT = 174A, 1.71V
Vacuum stable.
Increasing ramping rate to 0.5A/min.
Thursday, September 28, 2017, 09:56
IGP1 = 4.85e-5 Torr
TGHT = 195A, 1.92V
Vacuum initially climbed a small amount with last increase, has started to decrease - vacuum stable.
Increasing ramping rate to 1.0A/min.
Thursday, September 28, 2017, 10:30
IGP1 = 5.3e-5 Torr
TGHT = 220A, 2.18V
Vacuum increased slightly again with faster ramping rate.
Vacuum now dropping - stable.
Increasing ramping rate to 2.0A/min.
Thursday, September 28, 2017, 11:07
IGP1 = 6.35e-5 Torr
TGHT = 302A, 3.09V
Vacuum increased slightly again with faster ramping rate.
Vacuum now dropping - stable.
Increasing ramping rate to 2.5A/min.
Thursday, September 28, 2017, 11:45
IGP1 = 1.67e-4 Torr
TGHT = 380A, 4.04V
Vacuum increased normally at slow rate for first half hour.
~30min into the 2.5A/min rate increase, vacuum started to climb much faster.
Paused auto-ramp for few min to allow vacuum to stabilize.
Vacuum decreasing - stable.
IGP1 = 1.4e-4 Torr
Decreasing ramping rate to 0.5A/min for next hour while unable to watch.
Thursday, September 28, 2017, 13:20
IGP1 = 1.93e-4 Torr
TGHT = 425A, 4.58V
Vacuum stable.
Changing vacuum limits and ramping rate.
Increasing ramping rate 1.0A/min.
Vacuum limit stop at 3.0e-4 Torr, backing off at 6.0e-4 Torr.
Thursday, September 28, 2017, 14:06
IGP1 = 3.1e-4 Torr
TGHT = 456A, 4.93V
Vacuum stable.
Changing vacuum limits and ramping rate.
Changing ramping rate to 0.5A/ 30sec.
Vacuum limit stop at 4.0e-4 Torr, backing off at 7.0e-4 Torr.
Thursday, September 28, 2017, 14:44
IGP1 = 4.0e-4 Torr
TGHT = 468A, 5.07V
Vacuum stable.
Changing vacuum limits.
Vacuum limit stop at 5.0e-4 Torr, backing off at 8.0e-4 Torr.
Thursday, September 28, 2017, 15:49
TP thermocouple = 28.1C
IGP1 = 5.0e-4 Torr
TGHT = 485A, 5.25V
Vacuum stable.
Changing ramping rate for overnight heating.
Decreasing ramping rate to 0.5A/min.
Friday, September 29, 2017, 09:11
TP thermocouple = 26.1C
IGP1 = 5.0e-6 Torr
TGHT = 520A, 5.60V
Vacuum stable.
Carbonization process complete!
Evap1 has remained at max setpoints for ~13hrs
Initiating auto-cool at 1.0A/min
Tuesday, October 03, 2017, 10:09
Vented in Ar and transferred from evap1 to glove box yesterday.
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167
|
Thursday, September 21, 2017, 11:35 |
Laura Lambert | Empty | | | Done | Testing TBHT [1st run!], RP [new oil] and IG [new gauge] | Thursday, September 21, 2017, 11:32
Copper plate attached to TBHT to allow current to be applied.
Started pumping down this a.m.
Roughing pump sounds normal.
Currently Ion Gauge times out before turning on, will attempt again later when lower vacuum achieved...
Monday, September 25, 2017, 13:30
Ion Gauge hadn't been fully hooked up via eipcs yet.
Ramped down last week/ vented/ hooked up ion gauge in epics/ restarted IOC - now updated and good to go.
Started pumping down again this a.m.
Roughing pump sounds normal.
Ion gauge working well!
IGP1 = 2.7e-5 Torr
Wednesday, September 27, 2017, 09:20
Cooled down, vented in air and opened up yesterday.
TBHT ran well - readout on power supply and readout on striptool were very close.
Roughing pump ran smoothly - nothing other than usual problems.
Sometimes when roughing pump is 1st turned on it chokes up and sounds TERRIBLE. At this point if you turn it off and leave it for a few seconds then try turning it on again it usually works fine.
Ion gauge ran well - direct readout vs striptool readout are slightly off because the direct readout is in mBar and the striptool in Torr.
One minor thing noticed with the new ion gauge - when water is turned on the vacuum increases very minorly by ~5e-8 Torr.
This wouldn't show up with the old Ion Gauge - maybe the new one is slightly more sensitive?
Otherwise everything ran great
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166
|
Wednesday, September 20, 2017, 08:07 |
Aaron Schmidt | | | | Maintenance | Ion gauge & RP status | Wednesday, September 20, 2017, 08:00:
-A new ion gauge was installed yesterday afternoon and the old one removed. The old IG was found to be contaminated (300 cpm) and as of 20/09/2017, it is double bagged and stashed underneath the evaporator for the time being.
Completed under work permit: I2017-09-19-9
-The roughing pump was reconnected this morning without issue. |
165
|
Thursday, September 07, 2017, 14:26 |
Aaron Schmidt | | | | Maintenance | roughing pump oil replaced | Thursday, September 07, 2017, 11:00 -12:00
The roughing pump was disconnected from Evaporator 1, along with the exhaust/ventilation. No contamination was found on swipes.
The oil was refilled.
The roughing pump was then moved away from the PLC to allow access for Dave Morris. The RP can be reconnected and tested after the PLC work is complete.
Work permit # I2017-09-07-1
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164
|
Wednesday, August 23, 2017, 15:54 |
Laura Lambert | UO2/C | 40282-2 | TARGET BOAT | Done | Carbonizing UC2 discs for 1stepUCx in graphite sample container _#1 | Wednesday, August 23, 2017, 15:41
2 rounds of UO2/C were cast onto a graphite sheet in the fume hood and let dry.
For this round of samples, circles from cast 1 were used
Graphite powder used = 5.16g
A 14mm punch was used to punch out circles from a 16mm wide strip.
35 circles were packed into a graphite sample container.
graphite container [no endcap] = 3.37g
35 x UO2/C circles = 4.76g
graphite container+smpls = 8.13g
container+smpls+endcap = 10.08g
Graphite tube is placed inside a target boat.
Boat previously coated with TaC and sintered - 1st use of newly sintered boat.
Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.
Chamber currently pumping down.
Friday, August 25, 2017, 09:59
IG1 = 3.45e-6 Torr.
Stepped up manually to 80A.
Vacuum stable.
IG1 = 3.0e-5 Torr.
Initiating auto-ramp.
Target boat will be ramped up to 520A at the rate of 0.1A/min.
Vacuum limit stop at 1.0e-4 Torr, backing off at 5.0e-4 Torr.
Monday, August 28, 2017, 08:09
IG1 = 6.3e-6 Torr
TGHT = 455A, 4.65V
Vacuum stable.
Increasing ramping rate to 0.2A/min.
Monday, August 28, 2017, 08:53
IG1 = 7.3e-6 Torr
TGHT = 465A, 4.75V
Vacuum stable.
Increasing ramping rate to 0.5A/min.
Monday, August 28, 2017, 13:17
IG1 = 1.32e-5 Torr
TGHT = 520A, 5.44V
Vacuum still fairly high and not dropping very fast indicating carbonization incomplete.
Increasing max setpoint to 530A and restarting auto-ramp.
Monday, August 28, 2017, 15:13
IG1 = 1.32e-5 Torr
TGHT = 530A, 5.58V
Vacuum still high, wavering up and down/ not dropping - carbonization remains incomplete.
Increasing max setpoint to 540A and restarting auto-ramp.
Tuesday, August 29, 2017, 09:28
IG1 = 3.72e-6 Torr
TGHT = 540A, 5.66V
Carbonization complete.
Initiating auto-cool at 2.0A/min
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Attachment 1: IMG_1768.JPG
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Attachment 2: IMG_1774.JPG
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163
|
Thursday, July 27, 2017, 09:08 |
Laura Lambert | | | | Problems resolved | *hot lab is HOT* |
Laura Lambert wrote: |
Thursday, July 13, 2017, 12:48
NOTE: hot lab reached 27degrees every day this week and went up to 28C today!
This is with the small portable fan running.
27C was reached even with both evaporators off.
When at 28C: evap2 = ~1500C and evap1 = 35A
Thursday, July 20, 2017, 15:58
Hot lab reached 30C today.
Small fan off - unsure if able to run due to contamination spread...
Both evap1 and evap2 were under vacuum but had not initiated ramping up yet.
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Thursday, July 27, 2017, 09:06
There was a broken valve motor affecting all ISAC rooms - temporary fix in place.
Ventilation in ISAC hot lab has been increased.
Temperature back to a reasonable level - currently sitting at 22C!
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162
|
Thursday, July 20, 2017, 15:57 |
Laura Lambert | UC2 | 42218-15 | LP-SIS | Done | Conditioning UCx#21 |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Wednesday, July 12, 2017, 17:06
Target container was previously coated with TaC and sintered.
Container is wrapped with 3 layers of Ta-heat shield, including the center block
The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].
Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack
A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.
The right side is open with a TaC coated spring to help hold materials in.
The chamber is currently pumping down.
TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]
Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.
Thursday, July 13, 2017, 12:49
Tapped up manually to 35A.
Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr
Initiating auto-ramp.
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Thursday, July 13, 2017, 14:48
Update: auto-ramp not started.
With recent updates to evap1 epics, not everything was uploaded correctly.
TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.
No parameters can be inputed and therefore unable to start auto-ramp.
Friday, July 14, 2017, 15:56
Problems still not fixed.
Have tapped up manually to 50A, 0.59V
Vacuum stable; IG1 = 5.26e-6 Torr.
Will remain at setpoints over weekend before continuing to ramp up manually...
Monday, July 17, 2017, 15:10
New problems:
Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]
In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.
Evap2 needs to be fixed asap and cannot wait for this process to be complete.
Evap1 had been tapped up manually to 60A.
Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.
Tuesday, July 18, 2017, 15:31
Paddle wheels for evap2 replaced and up and running again.
IG1 = 1.2e-6 Torr.
Starting to tap back-up manually...
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Wednesday, July 19, 2017, 14:12
TGHT auto-ramp fixed.
Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.
Currently during auto-ramp, every time steps up: states TBHT tripped off.
This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.
Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...
Note: Might be a few spikes on striptool from past hour when IOC was rebooted.
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Wednesday, July 19, 2017, 14:16
Tapped up manually to 30A yesterday.
Continued manual tap up today and reached 60A.
Initiated auto-ramp.
IG1 = 4.4e-6 Torr
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Thursday, July 20, 2017, 14:48
TGHT tripped off yesterday evening
Auto-ramping was fixed but a few more glitches in the system caused the TGHT to trip.
Please refer to photos.
When auto-ramp is running and vacuum reaches the parameter set for 'Good Vacuum', the auto-ramp should stop until the vacuum drops below the good vacuum at which point it can then continue to auto-ramp.
When auto-ramp is running and vacuum reaches the parameter set for 'Bad Vacuum', the auto-ramp should initiate auto-cool/ramp-down until the vacuum drops to the good vacuum parameter at which point it can then proceed with the 'Good Vacuum' requirement.
With this scenario, the auto-ramp system ignored the parameters set for good and bad vacuum, proceeded past both points and continued to ramp until the vacuum eventually reached it's trip off vacuum causing the TGHT to trip.
The TGHT current was at ~90A when it tripped off, so the target should be OK.
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Thursday, July 20, 2017, 15:14
Turns out the auto-ramp was reading the vacuum of 'IGP1' which is what the old ion gauge used to be called for evap1 and is currently one on evap2
AKA attempting to take a vacuum reading from one that doesn't exist for evap1
This ion gauge is now labelled 'IGP' and the auto-ramp system now uses 'IGP' for the vacuum parameter confirmations.
Changed a few things in the auto-ramp system:
-Updated messages.
-Auto-ramp aborts when TGHT/TBHT trips off.
-Displays setpoint it is ramping up to for next step
-Confirms which ion gauge it is reading
-Displays final setpoint and increment on message board
-No longer displays TBHT as 'tripped off' when not running.
System updated.
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Thursday, July 20, 2017, 15:57
Tapped up manually to 35A, 0.45V
IG1 = 5.26e-6 Torr
Re-initiated auto-ramp at 0.1A/min.
Friday, July 21, 2017, 13:50
TGHT = 81A, 0.92V
IG1 = 5.2e-5 Torr
Vacuum currently yo-yo-ing, but stable.
Changing vacuum limits.
Vacuum limit stop at 1.0e-4 Torr, backing off at 5.0e-4 Torr.
TP = 28.4C, RT = 27.3C
Thursday, July 27, 2017, 09:02
TGHT = 431A, 4.37V
IG1 = 1.32e-5 Torr
Vacuum stable.
Increasing ramping rate to 0.2A/min
TP = 26.7C, RT = 22.0C
Friday, July 28, 2017, 09:35
TGHT = 450A, 4.59V
IG1 = 5.4e-6 Torr
Target has remained at max setpoint for 23hrs.
TP = 25.9C, RT = 19.5C
Initiating auto-cool at 1.0A/min
Friday, August 04, 2017, 13:59
Evap1 was vented in Ar and transferred to the glove box on monday.
A few discs on opened end had slightly shifted [see photo], discs moved back in place - can see down into target.
Discoloration of Ta container to gold in some spots - this is normal as seen with most UCx targets
Target looks good.
Still requires 2nd endcap to be inserted.
Monday, August 21, 2017, 11:13
Both endcaps in.
No Rh foil inserted.
Endcaps require expanding.
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Attachment 1: IMG_3249.JPG
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Attachment 2: IMG_3251.JPG
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Attachment 3: IMG_3257.JPG
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Attachment 4: IMG_3258.JPG
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Attachment 5: IMG_3260.JPG
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161
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Thursday, July 20, 2017, 15:35 |
Laura Lambert | UC2 | 42218-15 | LP-SIS | Problems resolved | Conditioning UCx#21 |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Wednesday, July 12, 2017, 17:06
Target container was previously coated with TaC and sintered.
Container is wrapped with 3 layers of Ta-heat shield, including the center block
The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].
Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack
A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.
The right side is open with a TaC coated spring to help hold materials in.
The chamber is currently pumping down.
TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]
Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.
Thursday, July 13, 2017, 12:49
Tapped up manually to 35A.
Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr
Initiating auto-ramp.
|
Thursday, July 13, 2017, 14:48
Update: auto-ramp not started.
With recent updates to evap1 epics, not everything was uploaded correctly.
TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.
No parameters can be inputed and therefore unable to start auto-ramp.
Friday, July 14, 2017, 15:56
Problems still not fixed.
Have tapped up manually to 50A, 0.59V
Vacuum stable; IG1 = 5.26e-6 Torr.
Will remain at setpoints over weekend before continuing to ramp up manually...
Monday, July 17, 2017, 15:10
New problems:
Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]
In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.
Evap2 needs to be fixed asap and cannot wait for this process to be complete.
Evap1 had been tapped up manually to 60A.
Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.
Tuesday, July 18, 2017, 15:31
Paddle wheels for evap2 replaced and up and running again.
IG1 = 1.2e-6 Torr.
Starting to tap back-up manually...
|
Wednesday, July 19, 2017, 14:12
TGHT auto-ramp fixed.
Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.
Currently during auto-ramp, every time steps up: states TBHT tripped off.
This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.
Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...
Note: Might be a few spikes on striptool from past hour when IOC was rebooted.
|
Wednesday, July 19, 2017, 14:16
Tapped up manually to 30A yesterday.
Continued manual tap up today and reached 60A.
Initiated auto-ramp.
IG1 = 4.4e-6 Torr
|
Thursday, July 20, 2017, 14:48
TGHT tripped off yesterday evening
Auto-ramping was fixed but a few more glitches in the system caused the TGHT to trip.
Please refer to photos.
When auto-ramp is running and vacuum reaches the parameter set for 'Good Vacuum', the auto-ramp should stop until the vacuum drops below the good vacuum at which point it can then continue to auto-ramp.
When auto-ramp is running and vacuum reaches the parameter set for 'Bad Vacuum', the auto-ramp should initiate auto-cool/ramp-down until the vacuum drops to the good vacuum parameter at which point it can then proceed with the 'Good Vacuum' requirement.
With this scenario, the auto-ramp system ignored the parameters set for good and bad vacuum, proceeded past both points and continued to ramp until the vacuum eventually reached it's trip off vacuum causing the TGHT to trip.
The TGHT current was at ~90A when it tripped off, so the target should be OK.
|
Thursday, July 20, 2017, 15:14
Turns out the auto-ramp was reading the vacuum of 'IGP1' which is what the old ion gauge used to be called for evap1 and is currently one on evap2
AKA attempting to take a vacuum reading from one that doesn't exist for evap1
This ion gauge is now labelled 'IGP' and the auto-ramp system now uses 'IGP' for the vacuum parameter confirmations.
Changed a few things in the auto-ramp system:
-Updated messages.
-Auto-ramp aborts when TGHT/TBHT trips off.
-Displays setpoint it is ramping up to for next step
-Confirms which ion gauge it is reading
-Displays final setpoint and increment on message board
-No longer displays TBHT as 'tripped off' when not running.
System updated.
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160
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Thursday, July 20, 2017, 15:00 |
Laura Lambert | UC2 | 42218-15 | LP-SIS | Problems | Conditioning UCx#21 |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Wednesday, July 12, 2017, 17:06
Target container was previously coated with TaC and sintered.
Container is wrapped with 3 layers of Ta-heat shield, including the center block
The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].
Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack
A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.
The right side is open with a TaC coated spring to help hold materials in.
The chamber is currently pumping down.
TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]
Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.
Thursday, July 13, 2017, 12:49
Tapped up manually to 35A.
Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr
Initiating auto-ramp.
|
Thursday, July 13, 2017, 14:48
Update: auto-ramp not started.
With recent updates to evap1 epics, not everything was uploaded correctly.
TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.
No parameters can be inputed and therefore unable to start auto-ramp.
Friday, July 14, 2017, 15:56
Problems still not fixed.
Have tapped up manually to 50A, 0.59V
Vacuum stable; IG1 = 5.26e-6 Torr.
Will remain at setpoints over weekend before continuing to ramp up manually...
Monday, July 17, 2017, 15:10
New problems:
Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]
In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.
Evap2 needs to be fixed asap and cannot wait for this process to be complete.
Evap1 had been tapped up manually to 60A.
Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.
Tuesday, July 18, 2017, 15:31
Paddle wheels for evap2 replaced and up and running again.
IG1 = 1.2e-6 Torr.
Starting to tap back-up manually...
|
Wednesday, July 19, 2017, 14:12
TGHT auto-ramp fixed.
Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.
Currently during auto-ramp, every time steps up: states TBHT tripped off.
This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.
Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...
Note: Might be a few spikes on striptool from past hour when IOC was rebooted.
|
Wednesday, July 19, 2017, 14:16
Tapped up manually to 30A yesterday.
Continued manual tap up today and reached 60A.
Initiated auto-ramp.
IG1 = 4.4e-6 Torr
|
Thursday, July 20, 2017, 14:48
TGHT tripped off yesterday evening
Auto-ramping was fixed but a few more glitches in the system caused the TGHT to trip.
Please refer to photos.
When auto-ramp is running and vacuum reaches the parameter set for 'Good Vacuum', the auto-ramp should stop until the vacuum drops below the good vacuum at which point it can then continue to auto-ramp.
When auto-ramp is running and vacuum reaches the parameter set for 'Bad Vacuum', the auto-ramp should initiate auto-cool/ramp-down until the vacuum drops to the good vacuum parameter at which point it can then proceed with the 'Good Vacuum' requirement.
With this scenario, the auto-ramp system ignored the parameters set for good and bad vacuum, proceeded past both points and continued to ramp until the vacuum eventually reached it's trip off vacuum causing the TGHT to trip.
The TGHT current was at ~90A when it tripped off, so the target should be OK.
|
Attachment 1: Capture.JPG
|
|
Attachment 2: Capture3.JPG
|
|
159
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Wednesday, July 19, 2017, 14:17 |
Laura Lambert | UC2 | 42218-15 | LP-SIS | In progress | Conditioning UCx#21 |
Laura Lambert wrote: |
Laura Lambert wrote: |
Laura Lambert wrote: |
Wednesday, July 12, 2017, 17:06
Target container was previously coated with TaC and sintered.
Container is wrapped with 3 layers of Ta-heat shield, including the center block
The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].
Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack
A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.
The right side is open with a TaC coated spring to help hold materials in.
The chamber is currently pumping down.
TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]
Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.
Thursday, July 13, 2017, 12:49
Tapped up manually to 35A.
Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr
Initiating auto-ramp.
|
Thursday, July 13, 2017, 14:48
Update: auto-ramp not started.
With recent updates to evap1 epics, not everything was uploaded correctly.
TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.
No parameters can be inputed and therefore unable to start auto-ramp.
Friday, July 14, 2017, 15:56
Problems still not fixed.
Have tapped up manually to 50A, 0.59V
Vacuum stable; IG1 = 5.26e-6 Torr.
Will remain at setpoints over weekend before continuing to ramp up manually...
Monday, July 17, 2017, 15:10
New problems:
Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]
In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.
Evap2 needs to be fixed asap and cannot wait for this process to be complete.
Evap1 had been tapped up manually to 60A.
Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.
Tuesday, July 18, 2017, 15:31
Paddle wheels for evap2 replaced and up and running again.
IG1 = 1.2e-6 Torr.
Starting to tap back-up manually...
|
Wednesday, July 19, 2017, 14:12
TGHT auto-ramp fixed.
Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.
Currently during auto-ramp, every time steps up: states TBHT tripped off.
This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.
Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...
Note: Might be a few spikes on striptool from past hour when IOC was rebooted.
|
Wednesday, July 19, 2017, 14:16
Tapped up manually to 30A yesterday.
Continued manual tap up today and reached 60A.
Initiated auto-ramp.
IG1 = 4.4e-6 Torr
|
158
|
Wednesday, July 19, 2017, 14:15 |
Laura Lambert | UC2 | 42218-15 | LP-SIS | Problems resolved | Conditioning UCx#21 |
Laura Lambert wrote: |
Laura Lambert wrote: |
Wednesday, July 12, 2017, 17:06
Target container was previously coated with TaC and sintered.
Container is wrapped with 3 layers of Ta-heat shield, including the center block
The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].
Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack
A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.
The right side is open with a TaC coated spring to help hold materials in.
The chamber is currently pumping down.
TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]
Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.
Thursday, July 13, 2017, 12:49
Tapped up manually to 35A.
Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr
Initiating auto-ramp.
|
Thursday, July 13, 2017, 14:48
Update: auto-ramp not started.
With recent updates to evap1 epics, not everything was uploaded correctly.
TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.
No parameters can be inputed and therefore unable to start auto-ramp.
Friday, July 14, 2017, 15:56
Problems still not fixed.
Have tapped up manually to 50A, 0.59V
Vacuum stable; IG1 = 5.26e-6 Torr.
Will remain at setpoints over weekend before continuing to ramp up manually...
Monday, July 17, 2017, 15:10
New problems:
Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]
In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.
Evap2 needs to be fixed asap and cannot wait for this process to be complete.
Evap1 had been tapped up manually to 60A.
Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.
Tuesday, July 18, 2017, 15:31
Paddle wheels for evap2 replaced and up and running again.
IG1 = 1.2e-6 Torr.
Starting to tap back-up manually...
|
Wednesday, July 19, 2017, 14:12
TGHT auto-ramp fixed.
Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.
Currently during auto-ramp, every time steps up: states TBHT tripped off.
This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.
Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...
Note: Might be a few spikes on striptool from past hour when IOC was rebooted.
|
157
|
Thursday, July 13, 2017, 14:50 |
Laura Lambert | UC2 | 42218-15 | LP-SIS | Problems | Conditioning UCx#21 |
Laura Lambert wrote: |
Wednesday, July 12, 2017, 17:06
Target container was previously coated with TaC and sintered.
Container is wrapped with 3 layers of Ta-heat shield, including the center block
The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].
Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack
A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.
The right side is open with a TaC coated spring to help hold materials in.
The chamber is currently pumping down.
TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]
Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.
Thursday, July 13, 2017, 12:49
Tapped up manually to 35A.
Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr
Initiating auto-ramp.
|
Thursday, July 13, 2017, 14:48
Update: auto-ramp not started.
With recent updates to evap1 epics, not everything was uploaded correctly.
TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.
No parameters can be inputed and therefore unable to start auto-ramp.
Friday, July 14, 2017, 15:56
Problems still not fixed.
Have tapped up manually to 50A, 0.59V
Vacuum stable; IG1 = 5.26e-6 Torr.
Will remain at setpoints over weekend before continuing to ramp up manually...
Monday, July 17, 2017, 15:10
New problems:
Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]
In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.
Evap2 needs to be fixed asap and cannot wait for this process to be complete.
Evap1 had been tapped up manually to 60A.
Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.
Tuesday, July 18, 2017, 15:31
Paddle wheels for evap2 replaced and up and running again.
IG1 = 1.2e-6 Torr.
Starting to tap back-up manually...
|
156
|
Thursday, July 13, 2017, 12:49 |
Laura Lambert | | | | Problems | *hot lab is HOT* | Thursday, July 13, 2017, 12:48
NOTE: hot lab reached 27degrees every day this week and went up to 28C today!
This is with the small portable fan running.
27C was reached even with both evaporators off.
When at 28C: evap2 = ~1500C and evap1 = 35A
Thursday, July 20, 2017, 15:58
Hot lab reached 30C today.
Small fan off - unsure if able to run due to contamination spread...
Both evap1 and evap2 were under vacuum but had not initiated ramping up yet.
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Attachment 1: Capture.JPG
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