Logbooks Lab Maintenance Evaporator_1 Evaporator_2 Laser cutter Target Production Test-Stand RH-ISAC RH-Cyclotron RH-Meson Hall RH-Beamlines RH-ARIEL
  Evaporator_2, Page 31 of 34  Not logged in ELOG logo
  ID Date Author Target Materialdown Target Oven W.O# Source Status Subject
  295   Tuesday, May 10, 2016, 11:57 Laura Lambert 40282-3TARGET BOATDoneConditioning Nb samples for Tobias

John Wong wrote:

Laura Lambert wrote:

 Wednesday, May 04, 2016, 13:28

Target boat has a layer of niobium foil on the bottom of the boat.

A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos

Larger niobium samples are placed in the slots, holding in place, to avoid warping; smaller niobium sample sitting inside the boat by itself.

Smaller sample closest to OMEGA IR reading [right side]

Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.

Loaded into evap2 yesterday.

Vacuum pump bearings gone - pump replaced this morning by vacuum group.

Pumping down now...


 Friday, May 06, 2016, 13:36

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

IGP1 = 2.4e-7 Torr

Setting auto-ramp rate at 0.2A/min to 250A over the weekend.

Will tap up manually monday to final desired temperature of 1400C.


 Monday, May 09, 2016, 09:38

OMEGA = 1128C

IGP1 = 1.3e-7 Torr

TGHT = 250A, 3.7V

Tapping up manually to 1400C...


 Monday, May 09, 2016, 14:05

Evap2 has reached ~1405C

TGHT = 341A, 5.34V

IGP1 = 1.9e-7 Torr

Will remain at max setpoints for min 4hrs then initiate cool down.


 

 Monday, May 09, 2016, 18:18

TGHT at 341A/5.34V for over 4 hours.  Vac stables at 1.78e-7 Torr.

Cooling down at 2A/min


 

 Tuesday, May 10, 2016, 08:45

Vented in air and opened up this morning.

Samples look good!


 

  313   Friday, August 12, 2016, 11:08 Laura Lambert   MaintenanceNEW PUMP FOR GLOVE BOX

Wednesday, August 03, 2016, 16:16

Tues July 26th had some problems with the transfer chamber

Transfer chamber was not going below -20in pressure, when usually it will drop all the way to -30in

To by pass and put the uranium target into the glove box, the transfer chamber was flushed 10x - when opened, no change in H2O and O2 in glove box; therefore, 'bypass' worked.

Pump removed and tested by vacuum group - showed no reading on gauge when being tested, how was it even pumping?

New pump installed July 27th.

New pump = bigger/ faster/ quieter 


 

  315   Thursday, August 18, 2016, 10:37 Anders Mjos   MaintenanceNew cooling lines for Heat Shield

 Dan made a set of new cooling lines for the Source Tray Heat Shield cooling yesterday. No joints on the lines. Use same VCR fitting 3/8 -> 1/4" as for the Heat Shield. The old lines had worn threads on the male VCR nut.

  342   Tuesday, December 20, 2016, 15:04 Laura Lambert   MaintenanceRETURN and SUPPLY valves CLOSED for xmas break

Tuesday, December 20, 2016, 15:05

confirmed ~full tank of Ar for glove box --> ~1600psi 

  345   Monday, February 06, 2017, 11:17 Anders Mjos   Problems resolvedIOC restart after power outagae

 Dave Morris did a remote restart of the IOC after the outage. Turbo pump started.

  346   Thursday, February 09, 2017, 11:49 Laura Lambert   MaintenanceNew heatshield with flexible water lines

 Thursday, February 09, 2017, 11:47

A new heatshield with flexible water lines has been put into evap2 last Friday Feb3rd


 

  364   Monday, May 08, 2017, 10:05 Laura Lambert   MaintenanceTurbo pump control box replaced

 Monday, May 08, 2017, 10:05

Turbo pump control box died last week.

Replaced with a new one.


 

  369   Thursday, May 11, 2017, 11:30 Laura Lambert   MaintenanceNew Ion Gauge for IGP2

 Thursday, May 11, 2017, 11:25

IGP2 has been having problems where sometimes it turns off and requires simply unplugging and plugging back in.

Ion gauge has been replaced.

At first the vacuum box appeared red on epics and when attempting to reset everything nothing would work and the backing pump would try and turn on then timeout.

Apparently this new ion gauge draws slightly more than the old one and this blew a fuse in the PLC.

Old fuse was 2A, so a new 3A fuse has been replaced - seems to be working fine now. 


 

  379   Tuesday, July 18, 2017, 15:30 Laura Lambert   MaintenancePaddle wheel replacement for all evap2 water supplies

 Tuesday, July 18, 2017, 15:26

Problems occured with TGHT water supply paddle wheel stopped and therefore tripped off evap2 last week.

All paddle wheels were replaced today for evap2 [other than the chiller].

A build up of dirt was found on all wheels replaced.

Evap2 good to go.

Will test flow meters before heating up to higher setpoints to confirm everything is working.


 

  380   Wednesday, July 19, 2017, 13:55 Marla Cervantes 40282-5TARGET BOATDoneSintering La(OH)3/C discs

 Wednesday, July 19, 2017, 13:44

Discs previously casted by Marla and Pauline and weighed. 

Discs are placed inside a small graphite container.

Graphite container with discs loaded with 30 discs was loaded into Ta-boat previously coated with TaC.

Ta-boat is wrapped with 3 Ta heat shields.

Loaded in evaporator 2.

Chamber currently pumping down.


Thursday, July 20, 2017, 16:07

 HS water valves were opened in the morning, no leaks were detected.

Perform water test to confirm paddle wheels are working well.

Current was tapped manually to 40 A.

Read out on meter confirmed paddle wheels are registering 

Tap back down to 20 A, tripped off system on purpose by closing HS water valves.

TGHT tripped off as expected.

Water flow test was good, initiating ramp up of samples.

Taped manually to 40 A.

After the stabilization of the vacuum auto ramping was set up to 0.2 A/min.

Up to a final set up point of 250 A.

Final desired temperature ~1800 C.


 Friday, July 21, 2017, 10:20

Final set up from July 20 was reached.

Current reading: 244.6 A.

Voltage reading: 3.82 V.

Temperature reached: 1105 C.

Final set up was change to 1500 A.

The temperature reached at 6 pm was 1936 C so the current  was decreased  to 488 A.

The final temperature after 30 min was 1800 C.

The set up stayed the same for the weekend.


 Monday, July 24, 2017, 13:06

Temperature reading in the morning was 1856 C.

TGHT: 487.87 A, 9.07 V

TGHT power supply: 

IGP1: 3.75e-7 Torr

IGP2: 3.51e-7 Torr

Started to ramp down at 1 A/min rate.

Initiating auto cooling at 1.0A/min for TGHT.170724-LaC2-CarbothermalReduction-EPICS-PLOTS.PNG


 Tuesday, July 25, 2017, 09:27

LaC2/C discs were taken off of evap2.

LaC2/C discs were brought in to glove box.

IMG-20170725-WA0018.jpg

 

  381   Tuesday, August 01, 2017, 15:34 Laura Lambert   ProblemsIGP1 mis-communicating with EPICS - PLC problem?

Monday, July 31, 2017, 15:24

Turned on BV and TP this afternoon.

Started ramping down, ~1min after turned on both tripped off.

Vacuum box turned red.

IGP1 appears yellow but still registering a vacuum.

TP interlocks: requires IEVAP2:IGP1 < 500mTorr but IGP1 = 6mTorr when tripped off.

Should have been satisfied and therefore not tripped but IGP1 not communicating?

Nothing wrong with ion gauge in person, vacuum good on direct read out.

When attempting 'Global Reset', nothing would reset - vacuum box remained red etc.

See screenshot attached of errors.


 Tuesday, August 01, 2017, 15:31

Had kept BP, PV and RV overnight.

This morning vacuum fine, everything had reset except "IEVAP2:TP on" under device notes for IEVAP2:TP remained red.

Turned on BV and TP, once turbo pump registered on, red wording went away.

Currently pumping down - everything looks fine now.

Still unsure of reason for these errors...


 Friday, August 04, 2017, 10:55

Happened again last night at ~5:45 while evaps at ~420A - see elog i.d. 383 for photos and details.


 

Attachment 1: evap2_trip_7.31.2017.JPG
evap2_trip_7.31.2017.JPG
  382   Wednesday, August 02, 2017, 16:12 Marla Cervantes 40282-5 DoneSintering La(OH)3/C pellets

 Monday, July 31, 2017,  

Pellets previously pressed by Marla and Pauline. 

Pellets are placed inside a small graphite container.

Graphite container loaded with 5 pellets was loaded into Ta-boat previously coated with TaC.

Ta-boat is wrapped with 3 Ta heat shields.

Loaded in evaporator 2.


 Tuesday, August 01, 2017,

Chamber pumping down.


 Wednesday, August 02, 2017, 16:03

HS water valves were opened, no leaks were detected.

Current was tapped manually to 40 A.

After the stabilization of the vacuum auto ramping was set up to 0.5 A/min.

Up to a final set up point of 300 A.

Final desired temperature ~1700 C.


 

  383   Friday, August 04, 2017, 10:52 Laura Lambert 40282-5TARGET BOATProblemsSintering La(OH)3/C pellets

Marla Cervantes wrote:

 Monday, July 31, 2017,  

Pellets previously pressed by Marla and Pauline. 

Pellets are placed inside a small graphite container.

Graphite container loaded with 5 pellets was loaded into Ta-boat previously coated with TaC.

Ta-boat is wrapped with 3 Ta heat shields.

Loaded in evaporator 2.


 Tuesday, August 01, 2017,

Chamber pumping down.


 Wednesday, August 02, 2017, 16:03

HS water valves were opened, no leaks were detected.

Current was tapped manually to 40 A.

After the stabilization of the vacuum auto ramping was set up to 0.5 A/min.

Up to a final set up point of 300 A.

Final desired temperature ~1700 C.


 

 Friday, August 04, 2017, 10:20

evap2 tripped twice yesterday.

1st trip) there was a power bump which caused a trip at ~4:20pm, this can be seen in the striptool image attached.

-TGHT spiked to zero, but immediately went back to the ~420A it was sitting at at the time.

-This did not initiate a full trip of everything, but a visual spike in the system can be seen

-Oddly this was not picked up in archives - happened so fast and must have been in the small time frame it was not picking up information

-Did TGHT actually drop to zero followed by then applying an immediate 420A?

-Or did it simple not register a reading due to power bump?

2nd trip) IGP1 stopped communicating at ~5:45pm, this can be seen in both the archives, striptool and evap2 control screenshot images attached

-IGP1 was fine, vacuum was good

-Registering good vacuum in epics - can see in screen shot vacuum was still good but IGP1 turned yellow as if turned off

-This resulted in TP followed by BV tripping off due to no longer getting a vacuum reading making the TP think there was a bad vacuum.

-Possible miscommunication with PLC?

-This is the same scenario that happened on mon - see elog i.d. 381

Will follow up when more information acquired...


 

Attachment 1: evap2_trip_8.4.2017.JPG
evap2_trip_8.4.2017.JPG
Attachment 2: evap2_trip_8.4.2017[2].JPG
evap2_trip_8.4.2017[2].JPG
Attachment 3: evap2_trip_8.4.2017[3].JPG
evap2_trip_8.4.2017[3].JPG
Attachment 4: evap2_trip_8.4.2017[4].JPG
evap2_trip_8.4.2017[4].JPG
  384   Friday, August 04, 2017, 14:09 Laura Lambert 40282-5TARGET BOATDoneSintering La(OH)3/C pellets

Laura Lambert wrote:

Marla Cervantes wrote:

 Monday, July 31, 2017,  

Pellets previously pressed by Marla and Pauline. 

Pellets are placed inside a small graphite container.

Graphite container loaded with 5 pellets was loaded into Ta-boat previously coated with TaC.

Ta-boat is wrapped with 3 Ta heat shields.

Loaded in evaporator 2.


 Tuesday, August 01, 2017,

Chamber pumping down.


 Wednesday, August 02, 2017, 16:03

HS water valves were opened, no leaks were detected.

Current was tapped manually to 40 A.

After the stabilization of the vacuum auto ramping was set up to 0.5 A/min.

Up to a final set up point of 300 A.

Final desired temperature ~1700 C.


 

 Friday, August 04, 2017, 10:20

evap2 tripped twice yesterday.

1st trip) there was a power bump which caused a trip at ~4:20pm, this can be seen in the striptool image attached.

-TGHT spiked to zero, but immediately went back to the ~420A it was sitting at at the time.

-This did not initiate a full trip of everything, but a visual spike in the system can be seen

-Oddly this was not picked up in archives - happened so fast and must have been in the small time frame it was not picking up information

-Did TGHT actually drop to zero followed by then applying an immediate 420A?

-Or did it simple not register a reading due to power bump?

2nd trip) IGP1 stopped communicating at ~5:45pm, this can be seen in both the archives, striptool and evap2 control screenshot images attached

-IGP1 was fine, vacuum was good

-Registering good vacuum in epics - can see in screen shot vacuum was still good but IGP1 turned yellow as if turned off

-This resulted in TP followed by BV tripping off due to no longer getting a vacuum reading making the TP think there was a bad vacuum.

-Possible miscommunication with PLC?

-This is the same scenario that happened on mon - see elog i.d. 381

Will follow up when more information acquired...


 

 Friday, August 04, 2017, 14:05

Vented in air and transferred to glove box today.

Container did not break.

Some wires in PLC were not creating a good contact - could be problem re: IGP1 tripping off.

Wires replaced by Gelo.

Put back under vacuum with nothing loaded over weekend to see how things run...


 

  387   Tuesday, September 12, 2017, 13:08 Aaron Schmidt    Window shutter added

 Tuesday, September 12, 2017, 12:00:

The coated back window was changed to a shuttered window.

On star-point flange bolt interfered with the shutter, however it was removed, shortened, and re-installed.

The installation is complete. Awaiting roughing pump to leak check.

  393   Thursday, November 23, 2017, 15:10 Laura Lambert 41882-4TARGET BOATDoneGraphite insert test

 Thursday, November 23, 2017, 14:54

Graphite insert loaded into previously TaC coated target boat.

One endcap removed to allow for outgassing: left side out, right side in.

Weight of graphite tube + single endcap = 10.2012g

Same Ta heats shields remain on container from sintering TaC coating.

Currently pumping down in evap2.


Friday, November 24, 2017, 11:31

IGP1 = 4.52e-7 Torr

IGP2 = 3.43e-7 Torr

OMEGA slope = 0.98

Good vac at 3.0e-4, bad vac at 8.0e-4 Torr.

HS water valves have remained open since the last time evap2 was used.

No leak check done.

Tapped up manually to 50A.

Vacuum stable.

IGP1 = 5.34e-7 Torr

IGP2 = 5.54e-7 Torr

Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 300A

Once max setpoints achieved, will tap up manually to final desired temperature of 2000C

Uranium targets go to a max temperature of 1950C online, so graphite insert should be tested to 2000C


 Monday, November 27, 2017, 10:15

IGP1 = 2.5e-7 Torr

IGP2 = 1.9e-7 Torr

Reached 300A, 4.61V

OMEGA = 1298C

Tapped up manually to 485A, 8.46V

OMEGA = 1808C

Remained at this setpoint for a day


Tuesday, November 28, 2017, 15:41 

IGP1 = 3.88e-7 Torr

IGP2 = 3.58e-7 Torr

Tapping up to 2000C...


Tuesday, November 28, 2017, 16:10 

TGHT = 570A, 10.20V

OMEGA = 2005C

IGP1 = 9.64e-7 Torr

IGP2 = 1.05e-6 Torr

There was a minor drop in voltage at 540A, 9.58V - dropped to ~9.4V then slowly went back up to 9.58V [see photo]

Will remain at this setpoint overnight and cool down in the a.m.


 Wednesday, November 29, 2017, 08:48

Voltage increased slowly while sitting at max setpoint of 570A [see photo]

TGHT = 570A, 11.20V --> voltage increased by 1.0V over ~16.5hrs

OMEGA = 2114C

IGP1 = 6.6e-7 Torr

IGP2 = 6.5e-7 Torr

Initiating auto-cool at 2.0A/min


 Wednesday, November 29, 2017, 16:15

Vented in air and removed today.

Will update tomorrow with results and photos.


 

Attachment 1: IMG_0018.JPG
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Attachment 6: voltage_increase_11.29.2017.JPG
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  399   Monday, December 11, 2017, 14:22 Laura Lambert   MaintenanceInterlock limits updated to 500mTorr

 Monday, December 11, 2017, 14:21

Dave updated evap2 interlock limits to 500mTorr for TGHT and TBHT on friday


 

  406   Wednesday, April 25, 2018, 07:21 Aaron Schmidt   DoneHS swap evap 2

Wednesday, April 25, 2018, 07:05: TGHT & TBHT off

Wednesday, April 25, 2018, 07:15: BV1 & TP1 off

Wednesday, April 25, 2018, 07:17: PV1 & BP1off

Wednesday, April 25, 2018, 07:19: Begin venting

Wednesday, April 25, 2018, 07:22: Full venting.

Wednesday, April 25, 2018, 07:29: HS waterlines purged.

Wednesday, April 25, 2018, 07:48: Aurelia's test ta target assembly was removed. The blank target heating heat shield for evap 2 was reinstalled. shields in but empty.

Evap 2 Doors closed.

  411   Friday, June 08, 2018, 08:33 Aaron Schmidt   Problems resolvedChiller tripped / Alarm

Alarm noted on passing Hot Lab. RPG notified, no radiological hazards. ISAC ops contacted, drop in DI water last night.

Entered w/ PPE. Chiller alarming. Evap 1 running ok

Friday, June 08, 2018, 08:30: Chiller turned on/off. Reset. No alarm.

  419   Tuesday, September 11, 2018, 10:47 Aaron Schmidt    Evap 2 step discrepancy

 Tuesday, September 11, 2018, 10:45:

TGHT: 53.4 A   TBHT: 57.75

Actual

TGHT: 60.0A  TBHT: 59.0A

Uploaded the rest to Word doc. Screenshots included.

Attachment 1: PS_Check.docx
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