The target was prepared and put under vacuum on 2020-08-10

2020-08-11 10:16am The pressure is 1e-6Torr. Leak checked performed, water on no problem. Starting to set target heating curve. 1A/10s up to 300A 

2020-08-11 11:23am target at 300A-1200degC Temperatures on exposed foil show to be higher than expected. 300degC already, 70degC on covered by foil thermocouple. Putting 50 more amps at 1A/10s 

2020-08-11 12:11pm target at 350A-1340degC. 350degC on exposed thermocouple. Ramping to 400A 1A/10s.

2020-08-11 12:28pm target at 400A-1420degC. 400degC on exposed thermocouple. Ramping to 450A 1A/10s.

 Thursday, July 30, 2015, 17:02

EVAP1 cooling system is now on the NALCW.  The city water has been removed from the system.  

Tested all the cooling system interlocks by shutting off each individual valve, and the main supply valve to the lab -  All Passed!  

Tuesday, November 26, 2019, 14:53

Total number of foils: 504

Total length packed 17.4 cm

container has 3 Ta heat shields.

No endcaps inserted to facilitate out-gassing

Two TaC coated Ta wire springs inserted at either end.

Initially to ramp TGHT and TBHT to 50A at 1A/min

Then heat manually to OMEGA ~1400 C , ramping TGHT manually and automatically  to reach 530A A (Omega slope set = 0.990)

Then temperature= (Correected to 1800C) 1900 C, Omega Slope set = 0.990, manually and automatically ramp to 700A, TGHT will be tapped up accordingly to reach desired Temp.

TBHT will be set fixed at 230 A (max).  TBHT heated manually and automatically to max.

Good vac at 3.00 e -5 Torr

Bad vac at 5.00 e-5 Torr

System experienced some vacuum issues due to cooling water leak in a heatshield line. 

Evaluation discs not included because no space.

Total Green disc mass measured = 58.250 g

Tuesday, November 26, 2019, 15:00

IGP1= 7.4e-06 Torr.  No leak issues found after last fix (Anders will add details).

Tuesday, November 26, 2019, 15:33

TGHT= 52.7A, .22V   TBHT= 49.3A, .52V

IGP1= 7.202 e-06 Torr (trending up so will allow to stabilize).

Wednesday, November 27, 2019, 06:09

left with autoramp waiting for vac to drop but no advance overnight.

Pressure did not seem to drop back below 3e-5 Torr magnitude, therefore not much advance in current ramp.

Thursday, November 28, 2019, 11:15

Continued ramping manually 

OMEGA = 1429 C  (0.99 slope), TGHT = 542A, 7.8V

With slope = 1.08 OMEGA = 1724 C, therefore staying at 0.99 slope

TaC coating sintering  plot suggests 753A to reach 1800C (See attachment 1)

Windows a little bit coated but not enough to disturb laser. 

Thursday, November 28, 2019, 12:17

TGHT =753A, 11.8V since 12:00 noon. 

TBHT= 233.4A, 3.3V

OMEGA= 1735 C (0.99 slope)

 Thursday, November 28, 2019, 13:01

OMEGA = 1860C (1.08 slope)

 Thursday, November 28, 2019, 14:38

OMEGA temperature began to creep up to ~1880.  Tapped TGHT current down to 733.5A, 11.4V

Thursday, November 28, 2019, 15:12

Checked windows and no significant additional buildup of obstructive material.

Temperature creeping up again.  Tap down TGHT current to 729 A, 11.2 V

OMEGA = 1870C at slope 1.08

 Thursday, November 28, 2019, 16:03

Temperature increase to 1880C

Tap down TGHT current to 715A, 10.9V

OMEGA= 1870 C (slope = 1.08)

Thursday, November 28, 2019, 16:22

Temperature creep to 1880 C

Tap down TGHT to 700A, 10.8V

OMEGA= 1845C

IGP1=2.2e-06 Torr

Thursday, November 28, 2019, 16:37

IGP1= 1.9e-06 Torr

OMEGA = 1850C (1.08 slope)

TGHT = 692A, 10.5V  TBHT= 233A, 3.2V

Initiating pressure ramp at -2A/min on TGHT and -1A/min on TBHT

Thursday, November 28, 2019, 16:45

IGP1= 1.28e-06 Torr

OMEGA= 1770 C (1.08 slope)

TGHT = 650A, 9.8V

ramp TGHT at -3.5A/min maintain TBHT at -1A/m in

 Thursday, November 28, 2019, 17:11

IGP1= 1.14e-06 Torr

OMEGA = 1730 C (1.08 slope)

ramp TGHT at -5A/min maintain TBHT at -1A/m

Thursday, November 28, 2019, 17:20

IGP1- 8.9e-07 Torr

OMEGA=1636C

ramp TGHT at -6A/min maintain TBHT at -1A/min

 Thursday, November 28, 2019, 17:34

IGP1= 7e-07 Torr

OMEGA= 1500 C (1.08 slope)

ramp TGHT at -8A/min maintain TBHT at -1A/min

TBHT = 183A

 OMEGA 1180C

TGHT =300 A

TBHT = 155A

Initiated -15A/min TGHT and -4A/min TBHT

IGP1= 5.2e-07 Torr

OMEGA below 1000C

begin manual tapdown

Thursday, November 28, 2019, 19:42

Target was dismounted after cooling.  Two graphite discs and end caps inserted.

Darwin Ortiz Rosales wrote:

Tuesday, November 26, 2019, 14:53 Total number of foils: 504 Total length packed 17.4 cm container has 3 Ta heat shields. No endcaps inserted to facilitate out-gassing Two TaC coated Ta wire springs inserted at either end. Initially to ramp TGHT and TBHT to 50A at 1A/min Then heat manually to OMEGA ~1400 C , ramping TGHT manually and automatically  to reach 530A A (Omega slope set = 0.990) Then temperature= 1900 C (Correction = 1800 C, NOT 1900 - JW), Omega Slope set = 0.990 (use 1.08, check temp, JW), manually and automatically ramp to 700A (check temp to see if it's matching with the 1.08 slope), TGHT will be tapped up accordingly to reach desired Temp. TBHT will be set fixed at 230 A (max).  TBHT heated manually and automatically to max. Good vac at 3.00 e -5 Torr Bad vac at 5.00 e-5 Torr System experienced some vacuum issues due to cooling water leak in a heatshield line.  Evaluation discs not included because no space. Total Green disc mass measured = 58.250 g   Tuesday, November 26, 2019, 15:00 IGP1= 7.4e-06 Torr.  No leak issues found after last fix (Anders will add details). Tuesday, November 26, 2019, 15:33 TGHT= 52.7A, .22V   TBHT= 49.3A, .52V IGP1= 7.202 e-06 Torr (trending up so will allow to stabilize).

 Wednesday, November 27, 2019, 17:44

I'll take over from here to step up the target heater, and I'll coordinate it with Darwin. 

 Wednesday, November 27, 2019, 20:36

Note: Sintering temp should be at 1800 C, NOT 1900.  Use Omega slope 1.08 and check temperature.  Correction made on elog #471.

Continue to step up TGHT and TBHT, keeping vacuum below 1.5 e-5 Torr. 

 Thursday, November 28, 2019, 03:06

TGHT reached to 400A/5.29V, TBHT at 230A/3.13V. 

Vacuum coming down from 1.3 e-5 Torr.

OMEGA = 1105 C (slope at 0.99).

Instructions for Darwin:

1.  Confirm temperature - check the temp plot from the TaC coating step. 

2.  Change OMEGA slop to 1.08 - check to see if this matches the temp plot.  If not, bring it back to 0.99.

3.  Continue to step up TGHT, check temp at 1400C (change slop 1.08 and check), 1500 C, 1600 C (check windows for coating - if any coating, then OMEGA is no longer useful hereon)

4.  Use the temp plot and continue to tap up TGHT to reach 1800 C and hold it for at least 4 hours or until the vacuum goes below 1 e-6 Torr then proceed with cooling down.

5.  Use the auto cooling program for TGHT (-2A/min) and TBHT (-1A/min)

Note:  For ramping up TGHT, keep vacuum below 1.5 e-4 Torr and keep tapping up to reach 1800 C.  Above 1100 C, this should be a quick step to get to 1800 C; should take < 2 hrs to get there.  

See the striptool or the attachment below to see how I did it. 

Once the chamber is cool down, take out a few samples for SEM analysis. 

Good luck!

Monday, June 24, 2019, 08:24

Total number of foils: 484

Total mass in  including container = 1495 grams

Total length packed 17.28 cm

container has 3 Ta heat shields.

No endcaps inserted to facilitate outgassing

Two TaC coated Ta wire springs inserted at either end.

Initially will heat via autoramp to OMEGA 1400 C , ramping TGHT at  0.1 A/min to reach 530A A (Omega slope set = 0.990)

Then temperature= (Correction to 1800C) 1900 C, Omega Slope set = 0.990, Auto TGHT at 0.2A/min to reach 700A, TGHT will be tapped up accordingly to reach desired Temp.

TBHT will be set fixed at 230 A (max).  TBHT at 0.1 A/min.

Good vac at 3.00 e -5 Torr

Bad vac at 5.00 e-5 Torr

System was pumped down on Friday June 24th, 2019.

IGP1= 3.3 e-07 Torr

(EPICS was down this morning and came back up around 930 a.m.)

Will proceed to manually tap up TGHT and TBHT to 40A as soon as EPICS stability confirmed

Mondayy, June 24, 2019, 15:30

TBHT = 39 A, 0.4V

TGHT=40 A, 0.1V

IGP1= 4.3 e-06 Torr and trending down

Autoramp increments to 0.1 A/min , to 400A on TGHT and 230A on TBHT

Tuesday, June 25, 2019, 08:40

Current has only increased to 53 A and pressure limit reached.  Lowered current back to 51 A on TGHT and TBHT.  Waiting for pressure to stabilize.

Tuesday, June 25, 2019, 12:16

TGHT 51.3 A, 0.39 V

TBHT 51.1 A, 0.58 V

IGP1 = 1.91 e-05 Torr

Starting autoramp with  increments to 0.1 A/min , to 400A on TGHT and 230A on TBHT

 Saturday, June 29, 2019, 22:45

Autoramp increments for TGHT set to 0.2 A/min

 IGP1=2.4 e-06 Torr

 Sunday, June 30, 2019, 07:46

Autoramp incrementsTGHT set to 0.1 A/min to prevent pressure spike. 

IGP1= 1.5 e-05 Torr

 Sunday, June 30, 2019, 08:26

Set autoramp increments on TGHT back to 0.2 A/min

Sunday, June 30, 2019, 15:47

Set autoramp max on TGHT to 500 A

Sunday, June 30, 2019, 21:15

OMEGA = 1240C

TGHT= 465A, 7.0V

TBHT = 233A, 3.2V

IGP1= 1.6 e-05 Torr

Set autoramp max on TGHT to 600A

Monday, July 01, 2019, 09:48

OMEGA = 1605 C

TGHT = 599A, 9.7V

TBHT = 233A, 3.2V

IGP1= 1.3 e-06 Torr

Set autoramp max on TGHT to 650A

Monday, July 01, 2019, 18:21

OMEGA = 1630 C

TGHT = 650 A, 10.6V

TBHT = 233A, 3.2V

IGP1 = 9.7 e-07 Torr

Set utoramp max on TGHT to 700A

Monday, July 01, 2019, 22:07

OMEGA = 1663 C

TGHT = 682A, 11.4V

TBHT = 233A, 3.2V

IGP1= 1.5 e-06 Torr

Set autoramp max on TGHT to 730A

Tuesday, July 02, 2019, 08:15

OMEGA =1700 C

TGHT = 730A, 12.0V

TBHT = 233A, 3.2V

IGP1= 1.1 e-06 Torr

Set autoramp max on TGHT to 750A and increments to 0.4A/min

Tuesday, July 02, 2019, 09:49

Temperature on OMEGA began dropping.  Changed OMEGA slope to 1.09 (Elog 371) and temperature reading = 1884 C.  Aborted autoramp and lowered TGHT current to 740A.

Tuesday, July 02, 2019, 12:14

Temperature and pressure have dropped at a consistent rate. 

IGP1= 9.6 e-07 Torr

OMEGA = 1715 C

Will tap up manually to 750A on TGHT

No appreciable increase in pressure will tap back down to 745A on TGHT

Tuesday, July 02, 2019, 13:11

OMEGA = 1675 C

TGHT = 745A, 12.4V

TBHT = 233A, 3.2V

IGP1 = 1.03 e-06Torr

 Will start to ramp- down TGHT @ -2.0A/min

OMEGA = 1354 C

TGHT = 495A, 7.01V

TBHT = 233.2A, 3.2V

IGP1= 2.2 e-07 Torr

Continue ramp-down TGHT @ -2.0A/min

Tuesday, July 02, 2019, 17:14

TGHT = 285.5A, 3.4V

TBHT = 232A, 3.1V

IGP1= 1.4 e-07 Torr

Start TBHT ramp-down at -1.0 A/min

Wednesday, July 03, 2019, 08:37

Turned off TGHT and TBHT

IGP1 = 7.8 e-08 Torr

Wednesday, July 03, 2019, 13:18

Final total weight of Target = 1489.5 g

Removed 18 discs after weighing.

 Monday, September 21, 2020, 16:50

450 graphite foils coated with graphite slurry were loaded in a tantalum tube, the tantalum tube was wrapped with 3 Ta heat shields and installed in the EVAP, to measure the temperature, a pack of 4 Ta foils were inserted in each side of the tube.

System is currently pumping down. 

 Tuesday, September 22, 2020, 07:54

IGP1 = 2e-6 Torr

 Good vacuum of 3e-2 Torr and Bad vacuum 5e-2 Torr

The autoramp is set to 50 A at 1 A each 10 s 

Tuesday, September 22, 2020, 08:18 

IGP1 = 3.7e-6 Torr

TGHT = .586 V, 50.06 A

Autoramp is set to 80 A same conditions.

 Tuesday, September 22, 2020, 08:26

IGP1 = 0.0006 Torr

TGHT = .97 V 80.3 A

Autoramp is set to to 100 A at 1 A each 20 s

Tuesday, September 22, 2020, 08:45

IGP1 = 0.003 Torr 

TGHT = 1.3 V, 100.5 A

Autoramp is set to 120 A at same conditions 

Tuesday, September 22, 2020, 09:36

IGP1 = 0.0001 torr

TGHT = 1.6 v, 122 A

Autoramp is set to 200 A at 2 A each 10 s 

Tuesday, September 22, 2020, 10:19

IGP1 = 5.4e-5 Torr

TGHT = 2.9 V, 200.5 A

Omega = 1123 °C

AP = 1164 °C 

Autoramp is set to 450 A,conditions:

2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

Tuesday, September 22, 2020, 11:24

TGHT = 447.8 A, 7.4 V

IGP1 =  3.7e-5 Torr

Omega = 1750 °C

AP = 1720.4 °C

Autoramp set to 520 A at same conditions

 Tuesday, September 22, 2020, 11:38

TGHT = 8.9 V, 525.8 A

IGP1 = 4.8e-5 Torr

Omega = 1914 °C

AP = 1835.6 °C

Autoramp set to 560 A at same conditions

Tuesday, September 22, 2020, 12:13

Omega 2038 °C 

Tuesday, September 22, 2020, 12:14

Current manually reduced to 555 A 

TGHT = 9.8 V, 560.8 A

IGP1 = 2.5e-5 Torr

Tuesday, September 22, 2020, 12:17 

Omega = 2030 °C

Tuesday, September 22, 2020, 12:19 

Current manually reduced to 550 A 

TGHT = 9.8 V, 547.8 A

IGP1 = 2.3e-5 Torr

Tuesday, September 22, 2020, 12:27 

Omega = 2027 °C

Tuesday, September 22, 2020, 12:27

Current manually reduced to 540 A 

TGHT = 9.6 V, 541.6 A

IGP1 = 2e-5 Torr

Tuesday, September 22, 2020, 12:34

Voltage suddenly increased!

TGHT = 10.3 V, 533.8 A

IGP1 = 2.9e-5 Torr

Omega = 2129 °C

Current reduced manually to 520 A to compensate the voltage increment 

Tuesday, September 22, 2020, 12:52

Another voltage increment 

TGHT = 9.9 V, 519.75 A

IGP1 = 1.9 e-5 Torr

Omega 2108 °C

Current reduced manually to 500 A to compensate the voltage increment 

Omega = 2070 °C

Tuesday, September 22, 2020, 13:05 

TGHT = 9.4 V, 492.4 A

Omega = 2063 °C

Tuesday, September 22, 2020, 13:08

Another voltage increment! this time it was an spike 

Tuesday, September 22, 2020, 16:13

After 5 hours

IGP1 = 6e-6 Torr

TGHT = 9.5 V, 488 A

Autoramp was set to 0 A at 2 A/min 

Omega = 2044 °C

AP = 2003.7 °C

Wednesday, September 23, 2020, 16:18

EVAP2 vented with air, target removed. 

 Wednesday, May 27, 2020, 10:22

IGP1 = 3.2e-7 Torr

TGHT = 0.186 V, 0.028 A

The autoramp is set to 50A:

1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

Wednesday, May 27, 2020, 10:40

 TGHT = 1.17 V, 50.9 A

PS = 1.21 V, 50 A

IGP1 = 8e-4 Torr and going down

Autoramp is set to 80 A same conditions

1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr

Wednesday, May 27, 2020, 12:29

TGHT = 1.59 V, 80.04 A

PS = 1.58 V, 80 A

IGP1 =  2e-4 Torr and going down

Autoramp is set to 100 A,conditions:

1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

Wednesday, May 27, 2020, 12:38

TGHT = 1.97 V, 100.35 A

IGP1 = 4e-4 Torr

Autoramp is set to 120 A,conditions:

1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

 Wednesday, May 27, 2020, 12:48

TGHT = 2.27 V, 119.1 A

IGP1 = 4e-4 Torr

Autoramp is set to 190 A,conditions:

1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

Wednesday, May 27, 2020, 13:03

TGHT = 3.4 V, 191.25 A

IGP1 = 3e-4 Torr

Autoramp is set to 190 A,conditions:

2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

Wednesday, May 27, 2020, 13:36 

TGHT = 7.8 V, 423 A

IGP1 = 3e-4 Torr

Autoramp is set to 450 A,conditions:

2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

Wednesday, May 27, 2020, 13:43

TGHT = 8.5 V, 451.6 A

IGP1 = 2e-4 Torr

Autoramp is set to 520 A,conditions:

2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr  

Wednesday, May 27, 2020, 14:02 

TGHT = 10.3 V, 508.16 A

Power supply = 10.39 V, 506 A

Omega = 2000 degC

AP = 2046.4 degC

After 3 hours at 2000 degC, the autoramp was set to 0 A,

conditions: -2 A each 10 s.

Note: There was a voltage drop of 0.6 V (fig. elog-484-fig2)

Friday, March 20, 2020, 19:39

The target material is loaded in a graphite cartridge.

The graphite cartridge is placed in a new tantalum boat previously without TaC,

the Ta boat was wrapped with three new Ta heat shields.

The system is currently pumping down. 

Monday, March 23, 2020, 07:49

IGP1 = 2.2e-7 Torr

Good vacuum= 3.00 e-5 Torr

Bad vacuum = 5.00 e-5 Torr

Ramping TGHT to 40A at 0.5A/min 

Monday, March 23, 2020, 10:35

Due to the COVID-19, non-essential activities are wrapped up,

the conditioning of the carbon target will be postponed until further notice 

Marla Cervantes wrote:

Friday, March 20, 2020, 19:39 The target material is loaded in a graphite cartridge. The graphite cartridge is placed in a new tantalum boat previously without TaC, the Ta boat was wrapped with three new Ta heat shields. The system is currently pumping down.  Monday, March 23, 2020, 07:49 IGP1 = 2.2e-7 Torr Good vacuum= 3.00 e-5 Torr Bad vacuum = 5.00 e-5 Torr Ramping TGHT to 40A at 0.5A/min  Monday, March 23, 2020, 10:35 Due to the COVID-19, non-essential activities are wrapped up, the conditioning of the carbon target will be postponed until further notice

 Wednesday, May 20, 2020, 12:50

On May 19 the pumps of EVAP2 were turned on to purge the system

Today Aaron made a leak check, for details, visit elog-481

Currently IGP1 = 8.17e-7 Torr

 Thursday, May 21, 2020, 09:41

IGP1 = 4.5e-7 Torr

TGHT = 0.03 V, 0.028 A

Current will be increased manually to 10 A, and then it will be autoramp to 500 A

Whit this power supply the current increments are register since the beging 

TGHT = 0.145 V, 10.35 A

During the input of the 10 A there was no anomaly with the pressure and the autoramp was set to 50A:

1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

Thursday, May 21, 2020, 10:39

The autoramp reached the 50 A set

TGHT = 0.65 V, 49.05 A

Power supply = 0.64 V, 50 A

IGP1 = 4.7e-7 Torr

Everything looks good, autoramp is set to 80 A same conditions

1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

 Monday, March 16, 2020, 13:47

Target material characteristics: Graphite cast of 0.965g/cm3, 287 D-shaped discs, disc area 0.969cm2, total mass of 9.972g, length 10.657cm.

The target material is loaded in a graphite cartridge.

The graphite cartridge is placed in a tantalum boat previously coated with TaC,

the Ta boat was wrapped with two used Ta heat shields.

The system is currently pumping down.

 Tuesday, March 17, 2020, 08:11

IGP1 = 3.18e-7 Torr

Current will be increased manually to 10 A, and then it will be autoramp to 500 A

During the input of the 10 A there was no anomaly with the pressure and the autoramp was set to:

1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

 Tuesday, March 17, 2020, 09:03

After 30 min:

TGHT: 98.1 A, 1.48 V (the voltage is increasing)

IGP1 = 3e-4 Torr

The autoramp is set to 2 A each 10 s to 500 A

Tuesday, March 17, 2020, 09:52

At 500 A the temperature was ~1243 C

So, the autoramp was re started  2 A each 10 s to 520 A

TGHT= 510 A, 9.18 V

IGP1= 8.2e-5 Torr

Pressure decreasing.

Temperature register in iR2C: 1272 C

The temperature stayed at 1270 C, 

The autoramp is re started: 2 A each 10 s to 600 A

Tuesday, March 17, 2020, 10:24

TGHT: 10.693 V, 588.5 A

IGP1 max 7.4e-5 Torr

Temperature after 3 min at 588.5 A: 1368 C

Tuesday, March 17, 2020, 10:34 

The autoramp is re started: 2 A each 10 s to 650 A

Tuesday, March 17, 2020, 10:46

TGHT=11.99 V, 637.6 A

IGP1=5.5e-5 Torr (8e-5 Torr max)

Temperature 1459 C

The current and voltage drop 10 A and 0.3 V respectively when the autoramp is stopped

Tuesday, March 17, 2020, 10:53

The autoramp is re started: 2 A each 10 s to 700A 

Tuesday, March 17, 2020, 11:04

TGHT: 13 V, 686.59 A

IGP1: 6.2e-5 Torr (Max 8.7e-5Torr) 

Temperature: 1507 C

Tuesday, March 17, 2020, 11:05

 The autoramp is re started: 2 A each 10 s to 800A 

Tuesday, March 17, 2020, 11:16

TGHT=14.29 V, 759 A

IGP1: 8.6e-5 Torr (Max 1e-4 Torr)

Temperature 1527 C

There is a current discrepancy in EPICs (see current discrepancy picture),

the autoramp stopped at 761 A because EPICS? reads 800 A

Increasing current manually. 

Increasing the current manually did not work, because set current is at fake maximum 

 Tuesday, March 17, 2020, 13:43

The temperature stabilized to 1567 C. The current however was not stable ( look at the CarbonTarget - Max current)

an autoramp is set to -2 A  each 10 s to 0A

The set current is going down but not the epics reading current neither the temperature. I assume the current will star going down when the set and the reading current from epics are the same.

Tuesday, March 17, 2020, 13:50

Autoramp was stopped, and current was reduced manually, at around 652 A (set current) the reading current started going down (639.5 A) 

Autoramp is set to -2 A each 10s to 0 A

The tantalum boat deformed and the graphite cartridge rim broke 

 Wednesday, February 11, 2015, 16:10

Container loaded into EVAP2.

3xTa heat shields.

Chamber currently being pumped down.

TGHT/ TBHT will be ramped up to 580A/ 230A or 1800C tapped up manually.

 Thursday, February 12, 2015, 09:39

HS water valves opened, no leaks detected.
Tapping up manually.

 Thursday, February 12, 2015, 12:07

OMEGA reached 1805C; TGHT = 415A, TBHT = 205A

Will continue to tap up manually to 2000C

 Thursday, February 12, 2015, 15:19

Reached TGHT = 500A, TBHT = 230A, OMEGA = 2035C.

Sat for ~2hrs.

Tapping up a further 25A on the TGHT.

 Thursday, February 12, 2015, 16:05

Tapped up manually to:

OMEGA = 2250C

DV = 5.65V

TGHT = 580A

TBHT = 230A

Friday, February 13, 2015, 10:05

Reached max setpoint last night.

Voltage starting to increase at contant TGHT @ 580A.  Lower TGHT to 525A, temp at 2150C (time 6:30pm) 

Initiating manual cool down.

Friday, February 13, 2015, 15:31

vented and opened up this afternoon.

everything looked good, container not broken! graphite insert looked good! the container was slightly bent, but nothing of significance.

however, the graphite insert bonded to the container so it was not taken out in one piece...

 Tuesday, February 10, 2015, 14:00

Container loaded into EVAP2 at noon.

no heat shields.

Chamber currently being pumped down.

TGHT/ TBHT will be ramped up to 580A/ 230A, tapped up manually.

 Tuesday, February 10, 2015, 14:39

HS water valves opened, no leaks detected.

Tapping up manually / recording data in excel

 Wednesday, February 11, 2015, 11:24

Reached max set points yesterday early evening.

Tapped down manually this a.m.

Will vent and open this afternoon.

 Wednesday, February 11, 2015, 15:54

Took out this afternoon.

container looks good.

graphite insert removed/ inspected - not much change, slightly lighter in colour.

[see attachments for graphs/ table]

 Wednesday, December 16, 2015, 10:09

Target consists of 505 discs.

Total packed length 3.4cm.

*same parameters at Ta#46*

Total mass of target materials 53.9381g [4 packs of 20 with Ta wire + 425 single discs].

3 x Ta Heat shields.

No Re foil inserted.

No endcaps inserted.

Chamber pumped down overnight.

IGP1 = 5.1e-7 Torr.

Tapped up manually to 35A.

IGP1 = 5.2e-7 Torr.

Vacuum stable, initiating auto-ramp.

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 1800C, auto ramp to 600A at 2.0A/min [estimated final value of 720A according to elog ID 239]

 Wednesday, December 16, 2015, 15:08

TBHT reached max setpoint of 230A, 3.3V

TGHT = 600A, 8.9V

IGP1 = 1.1e-6 Torr.

OMEGA = 1543C

Increasing final setpoint of TGHT to 700A and re-initiating auto-ramp.

 Wednesday, December 16, 2015, 16:02

TGHT = 700A, 10.6V

IGP1 = 2.1e-6 Torr.

OMEGA = 1740C

Tapping up manually to 1800C.

 Wednesday, December 16, 2015, 16:28

TGHT = 730A, 11.2V

Vacuum is coming down from IGP1 = 2.6e-6 Torr.

OMEGA = 1800C

Will condition the target at 1800C overnight and ramp down in the morning.

 Thursday, December 17, 2015, 09:31

OMEGA = 1802C on right side

Temp on leg of left side = 2150C, the hottest point - measured with the Mikron pyrometer.

 Friday, December 18, 2015, 08:53

Evap2 remained at 1800C for ~26.5hrs

Auto-ramped down to TGHT = 300A and TBHT = 90A at a rate of 2.0A/min and 1.0A/min respectively.

Conditioning complete.

TGHT will be ramped up later today for emissivity measurements.

 Monday, January 04, 2016, 11:21

the following was performed by aurelia.

emissivity measurements were taken late december.

evap2 was cooled down and left under vacuum over the xmas break.

currently ramping back up for more emissivity measurements.

 Friday, January 08, 2016, 10:47

Aurelia done measurements.

vented and opened this morning.

 Friday, May 29, 2015, 11:21

Total number of foils: 425 discs

Total mass of materials [incl graphite foils]: 44.41g

Total length packed: 12.3cm

Container has no heat shields.

No endcaps inserted to allow outgassing.

Currently being pumped down.

 Friday, May 29, 2015, 14:13

HS water valves opened, no leaks detected.

IGP1 = 5.4e-6 Torr.

Tapping up manually.

Friday, May 29, 2015, 16:48

Tapped up manually to 20A.

IGP1 = 5.9e-6 Torr.

Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT.

Max setpoints set to 580A and 230A for the TGHT and TBHT respectively.

Good Vacuum = 3.0e-5 Torr. Bad Vacuum = 4.0e-5 Torr.

 Monday, June 01, 2015, 09:17

IGP1 = 3.8e-6 Torr.

TGHT = 478A.

TBHT reached max setpoint of 230A.

Increasing ramping rate to 0.5A/min.

 Monday, June 01, 2015, 13:15

Checked window for temperature readings, good visibility, no coating on window. 

IGP1 = 9.1e-6 Torr.

TGHT reached max setpoint of 580A 30min ago.

Stepping up manually to a target temperature of 2000C...

 Monday, June 01, 2015, 16:25

IGP1 = 6.5e-6 Torr.

TGHT = 870A, 17.90V

OMEGA = 1948C

Laura Lambert wrote:

Friday, May 29, 2015, 11:21 Total number of foils: 425 discs Total mass of materials [incl graphite foils]: 44.41g Total length packed: 12.3cm Container has no heat shields. No endcaps inserted to allow outgassing. Currently being pumped down.  Friday, May 29, 2015, 14:13 HS water valves opened, no leaks detected. IGP1 = 5.4e-6 Torr. Tapping up manually. Friday, May 29, 2015, 16:48 Tapped up manually to 20A. IGP1 = 5.9e-6 Torr. Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT. Max setpoints set to 580A and 230A for the TGHT and TBHT respectively. Good Vacuum = 3.0e-5 Torr. Bad Vacuum = 4.0e-5 Torr.  Monday, June 01, 2015, 09:17 IGP1 = 3.8e-6 Torr. TGHT = 478A. TBHT reached max setpoint of 230A. Increasing ramping rate to 0.5A/min.  Monday, June 01, 2015, 13:15 Checked window for temperature readings, good visibility, no coating on window.  IGP1 = 9.1e-6 Torr. TGHT reached max setpoint of 580A 30min ago. Stepping up manually to a target temperature of 2000C...  Monday, June 01, 2015, 16:25 IGP1 = 6.5e-6 Torr. TGHT = 870A, 17.90V OMEGA = 1948C

 Monday, June 01, 2015, 17:59

After almost an hour at 870A, the temperature went up from 1948C to 1980C; however temperature around the target container/legs are >2000C.  The voltage on the power supply also went up slightly. 

There is a film coated on the window port and that could affect the temp reading.

To be safe, I lowered the TGHT to 830A/17.38V, temp at 1930C. 

Will keep at 830A for 4 hours and cool down this evening. 

Recommend: Using Ta-heat shields for sintering next time.

 Monday, June 01, 2015, 22:55

TGHT at 830A for almost 5 hours.  

TEMP has gone up to 1994C.  Voltage has also gone up to 19V.  

Cooling down at 2A/min for TGHT and 1A/min for TBHT. 

John Wong wrote:

Laura Lambert wrote:  Friday, May 29, 2015, 11:21 Total number of foils: 425 discs Total mass of materials [incl graphite foils]: 44.41g Total length packed: 12.3cm Container has no heat shields. No endcaps inserted to allow outgassing. Currently being pumped down.  Friday, May 29, 2015, 14:13 HS water valves opened, no leaks detected. IGP1 = 5.4e-6 Torr. Tapping up manually. Friday, May 29, 2015, 16:48 Tapped up manually to 20A. IGP1 = 5.9e-6 Torr. Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT. Max setpoints set to 580A and 230A for the TGHT and TBHT respectively. Good Vacuum = 3.0e-5 Torr. Bad Vacuum = 4.0e-5 Torr.  Monday, June 01, 2015, 09:17 IGP1 = 3.8e-6 Torr. TGHT = 478A. TBHT reached max setpoint of 230A. Increasing ramping rate to 0.5A/min.  Monday, June 01, 2015, 13:15 Checked window for temperature readings, good visibility, no coating on window.  IGP1 = 9.1e-6 Torr. TGHT reached max setpoint of 580A 30min ago. Stepping up manually to a target temperature of 2000C...  Monday, June 01, 2015, 16:25 IGP1 = 6.5e-6 Torr. TGHT = 870A, 17.90V OMEGA = 1948C    Monday, June 01, 2015, 17:59 After almost an hour at 870A, the temperature went up from 1948C to 1980C; however temperature around the target container/legs are >2000C.  The voltage on the power supply also went up slightly.  There is a film coated on the window port and that could affect the temp reading. To be safe, I lowered the TGHT to 830A/17.38V, temp at 1930C.  Will keep at 830A for 4 hours and cool down this evening.  Recommend: Using Ta-heat shields for sintering next time.  Monday, June 01, 2015, 22:55 TGHT at 830A for almost 5 hours.   TEMP has gone up to 1994C.  Voltage has also gone up to 19V.   Cooling down at 2A/min for TGHT and 1A/min for TBHT.

 Tuesday, June 02, 2015, 12:37

Chamber was vented and the target was inspected. 

Some stressed marks on the target container can be observed.

The container is also slightly curved but otherwise it's fine. 

The materials packed length has expended outward so 3 discs were removed in order to insert the end caps. 

The packed length is now 16cm.

Two extra graphite foils were inserted on both ends, and previously coated/sintered TaC-end caps are inserted and expended. 

Rn foil is inserted & Std solutions are added. 

Ready for test-stand.

Link to photos for more details:

https://www.dropbox.com/sh/0cra7viqs9ro8q3/AADEGk8goGI4c-uzRQSGwWmxa?dl=0

John Wong wrote:

John Wong wrote: Laura Lambert wrote:  Friday, May 29, 2015, 11:21 Total number of foils: 425 discs Total mass of materials [incl graphite foils]: 44.41g Total length packed: 12.3cm Container has no heat shields. No endcaps inserted to allow outgassing. Currently being pumped down.  Friday, May 29, 2015, 14:13 HS water valves opened, no leaks detected. IGP1 = 5.4e-6 Torr. Tapping up manually. Friday, May 29, 2015, 16:48 Tapped up manually to 20A. IGP1 = 5.9e-6 Torr. Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT. Max setpoints set to 580A and 230A for the TGHT and TBHT respectively. Good Vacuum = 3.0e-5 Torr. Bad Vacuum = 4.0e-5 Torr.  Monday, June 01, 2015, 09:17 IGP1 = 3.8e-6 Torr. TGHT = 478A. TBHT reached max setpoint of 230A. Increasing ramping rate to 0.5A/min.  Monday, June 01, 2015, 13:15 Checked window for temperature readings, good visibility, no coating on window.  IGP1 = 9.1e-6 Torr. TGHT reached max setpoint of 580A 30min ago. Stepping up manually to a target temperature of 2000C...  Monday, June 01, 2015, 16:25 IGP1 = 6.5e-6 Torr. TGHT = 870A, 17.90V OMEGA = 1948C    Monday, June 01, 2015, 17:59 After almost an hour at 870A, the temperature went up from 1948C to 1980C; however temperature around the target container/legs are >2000C.  The voltage on the power supply also went up slightly.  There is a film coated on the window port and that could affect the temp reading. To be safe, I lowered the TGHT to 830A/17.38V, temp at 1930C.  Will keep at 830A for 4 hours and cool down this evening.  Recommend: Using Ta-heat shields for sintering next time.  Monday, June 01, 2015, 22:55 TGHT at 830A for almost 5 hours.   TEMP has gone up to 1994C.  Voltage has also gone up to 19V.   Cooling down at 2A/min for TGHT and 1A/min for TBHT.     Tuesday, June 02, 2015, 12:37 Chamber was vented and the target was inspected.  Some stressed marks on the target container can be observed. The container is also slightly curved but otherwise it's fine.  The materials packed length has expended outward so 3 discs were removed in order to insert the end caps.  The packed length is now 16cm. Two extra graphite foils were inserted on both ends, and previously coated/sintered TaC-end caps are inserted and expended.  Rn foil is inserted & Std solutions are added.  Ready for test-stand. Link to photos for more details: https://www.dropbox.com/sh/0cra7viqs9ro8q3/AADEGk8goGI4c-uzRQSGwWmxa?dl=0

 see attachment for data recorded during ZrC conditioning 

Ta#(Spare) LP-SIS target description: 

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.033mm (0.0013") avg Measured. 

Target material batch: Ta 2023-1  Mt'l PO# TR-2022-03028

Target density = 12.515 g/cm3

Target length = 4.97 cm

Total Mass = 62.202 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven =  461g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

Dimpling direction on foils/ Packs.                                                               --> Center <--

End caps installed (Not expanded). No Ta foil heat shield added

Was labelled Ta#67 until the Thin foil target 45447-14 became so.

Thursday, October 05, 2023, 12:44: Roughing. 

Thursday, October 05, 2023, 13:10; TP1 on.  

Thursday, October 05, 2023, 13:11: TGHT / TBHT test. Tap up to 5 / 5 A & back to 0 A. Ok.

Thursday, October 05, 2023, 13:13: Slope Set @ 0.98 

Friday, October 06, 2023, 05:54: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min. 

Friday, October 06, 2023, 11:50: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (640 A w/ offset). Temperature @ 1716 C. Vacuum @ 2.76e-06T.

Friday, October 06, 2023, 12:20: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1809 C. Vacuum @ 3.77e-06T.

Friday, October 06, 2023, 12:37: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 665 A @ 2 A per min (650 A w/ offset). Temperature @ 1844 C. 

Friday, October 06, 2023, 12:53: Tapped up to TGHT / TBHT @ 670/ 230 A (657 / 233 A). Temperature @ 1880 C. Vacuum @ 4.94e-06T. 

Friday, October 06, 2023, 12:57: Tapped TGHT to 675.  TGHT / TBHT @ 675 / 230 A (662 / 233 A). Temperature @ 1889 C. Vacuum @ 5.03e-06T. 

Friday, October 06, 2023, 13:00: Tapped TGHT to 682.  TGHT / TBHT @ 682 / 230 A (669 / 233 A). Temperature @ 1901 C. Vacuum @ 5.46e-06T. Desired Temperature reached.

Friday, October 06, 2023, 13:01: Auto-cooling @ 2 A per min.

Tuesday, October 10, 2023, 08:37: PS & TP off. 

 Ta#67 Thin foil LP-SIS target description: 

Total Ta foils = 470 loaded into 2 packs of 235 foils each.

Foil Thickness = 0.010mm (0.0004") avg Measured. 

Target material batch:  https://elog.triumf.ca/TIS/Target+Production/143

Target density = 4.498 g/cm3

Target length = 3.7465 cm

Total Mass = 16.8509 g [Incl foils + Ta wire on 2 packs]

Total mass w/ Target oven =  415g (No end caps)

Discs in target are arranged as follows: 2packs

Dimpling direction on foils/ Packs.                                                               --> Center <--

No Ta foil heat shield added

Monday, July 22, 2024, 14:53: Roughing. 

Halt roughing. Install heat plates.

Monday, July 22, 2024, 15:06: Roughing.

Monday, July 22, 2024, 15:26: TP On.

Monday, July 22, 2024, 15:34: TP Timeout. Restart. 

Monday, July 22, 2024, 15:35: TP at speed (Green) 

Monday, July 22, 2024, 15:36: PS On. TGHT / TBHT to 5/5 A manually. OK. Tap down. 

Tuesday, July 23, 2024, 07:03: Auto-ramping TGHT / TBHT to 120 / 60 A @ 2 A per min. Desired temperature 1900 C.

Tuesday, July 23, 2024, 08:02: OMEGA IR2C Laser off. Slope set to 0.98. 

Tuesday, July 23, 2024, 08:06: Auto-ramping TGHT / TBHT to 300 / 150 A @ 2 A per min. 

Tuesday, July 23, 2024, 09:57: Auto-ramping TGHT / TBHT to 500 / 200 A @ 2 A per min. Temperature @ 1022 C. 

Tuesday, July 23, 2024, 11:59: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min. Temperature @ 1538 C.

Tuesday, July 23, 2024, 12:46: TGHT / TBHT @ 580 / 230 A (569 / 233 A). Temperature @ 1710 C. Vacuum @ 7.44e-06T. 

Tuesday, July 23, 2024, 14:23: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 620 A @ 2 A per min. Temperature @ 1721 C. Vacuum @ 5.06e-06T. 

Tuesday, July 23, 2024, 14:48: TGHT / TBHT @ 620 / 230 A 609 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min. Temperature @ 1799 C. Vacuum @ 6.76e-06T.  

Tuesday, July 23, 2024, 14:56:  TGHT / TBHT @ 630 / 230 A 618 / 233 A). Temperature @ 1816 C. Vacuum @ 7.14e-06T. Tapping up manually TGHT to get to 1900degC 

Tuesday, July 23, 2024, 15:23:  TGHT / TBHT @ 670 / 230 A 657 / 233 A).  Temperature @ 1890 C. Vacuum @ 9.94e-06T.  Stopping and waiting for 5min.

Tuesday, July 23, 2024, 15:39: Target ramp down 2A/min to 0 both TGHT and TBHT. 

Wednesday, July 24, 2024, 08:50: TP off.

Wednesday, July 24, 2024, 09:18: Venting.

Wednesday, July 24, 2024, 10:28: Target removed. EVAP2 clear. 

 Ta#66 LP-SIS target description: 

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.033mm (0.0013") avg Measured. 

Target material batch: Ta 2023-1  Mt'l PO# TR-2022-03028

Target density = 12.446 g/cm3

Target length = 5.0 cm

Total Mass = 62.230 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven=  g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

Dimpling direction on foils/ Packs.                                                               --> Center <--

End caps installed (Not expanded). No Ta foil heat shield added

Desired temperature 1900C

Wednesday, September 20, 2023, 14:18: Roughing. 

Wednesday, September 20, 2023, 14:35: TP Started. 

Wednesday, September 20, 2023, 14:43: TP on. 

Wednesday, September 20, 2023, 14:45: TGHT / TBHT raised to 5 / 5 A & lowered. Quick check ok. 

Thursday, September 21, 2023, 07:47: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min. Vacuum @ 8.30e-07T.

Thursday, September 21, 2023, 09:54: Slope set to 0.98 

Thursday, September 21, 2023, 13:42: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (640 A w/ offset). Temperature @ 1748 C. Vacuum @ 2.47e-06T.

Thursday, September 21, 2023, 14:10: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1843 C. Vacuum @ 3.30e-06T.

Thursday, September 21, 2023, 14:23: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 660 A @ 2 A per min (648 A w/ offset). Temperature @ 1879 C. Vacuum @ 3.77e-06T.

Thursday, September 21, 2023, 14:29: Tapped TGHT to 662.  TGHT / TBHT @ 662 / 230 A (649 / 233 A). Temperature @ 1903 C. Vacuum @ 4.08e-06T. Desired Temperature reached.

Thursday, September 21, 2023, 14:33: Auto-cooling started @ 1 A per min.

Monday, September 25, 2023, 08:09: Turbo pump off.