Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Note: This is the "old" design boat.  The new design boat was able to heat up to 900A/16.88 - the temperature was measured at about 1500C.  (see elog: https://elog.triumf.ca/TIS/Evaporator_2/15)

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.

John Wong wrote:

John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.

 Thursday, January 23, 2014, 16:18

Chamber vented overnight and was opened up this morning.

Target boat not fully sintered [see attached photos].

Chamber currently being pumped down again in order to continue with sintering TaC coating.

HS cooling water valves were opened, no leaks detected.

Will ramp up to 700A again over the weekend.

Laura Lambert wrote:

John Wong wrote: John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.     Thursday, January 23, 2014, 16:18 Chamber vented overnight and was opened up this morning. Target boat not fully sintered [see attached photos]. Chamber currently being pumped down again in order to continue with sintering TaC coating. HS cooling water valves were opened, no leaks detected. Will ramp up to 700A again over the weekend.

 Friday, January 24, 2014, 14:21

Chamber was pumped down to 1.7e-7 Torr.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A.

Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.

Laura Lambert wrote:

Laura Lambert wrote: John Wong wrote: John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.     Thursday, January 23, 2014, 16:18 Chamber vented overnight and was opened up this morning. Target boat not fully sintered [see attached photos]. Chamber currently being pumped down again in order to continue with sintering TaC coating. HS cooling water valves were opened, no leaks detected. Will ramp up to 700A again over the weekend.  Friday, January 24, 2014, 14:21 Chamber was pumped down to 1.7e-7 Torr. TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A. Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.

 Monday, January 27, 2014, 10:05

TGHT reached 700A over the weekend. Measured temp @ 2000C.

TGHT auto-cool inititated at 2.0A/min.

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote: John Wong wrote: John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.     Thursday, January 23, 2014, 16:18 Chamber vented overnight and was opened up this morning. Target boat not fully sintered [see attached photos]. Chamber currently being pumped down again in order to continue with sintering TaC coating. HS cooling water valves were opened, no leaks detected. Will ramp up to 700A again over the weekend.  Friday, January 24, 2014, 14:21 Chamber was pumped down to 1.7e-7 Torr. TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A. Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.    Monday, January 27, 2014, 10:05 TGHT reached 700A over the weekend. Measured temp @ 2000C. TGHT auto-cool inititated at 2.0A/min.

 Tuesday, January 28, 2014, 11:53

Chamber cooled down overnight, vented and opened up this morning.

Target boat still has a strip of green, still not fully sintered! [see attached photos].

Chamber currently being pumped down again to attempt sintering - round 3.

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: John Wong wrote: John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.     Thursday, January 23, 2014, 16:18 Chamber vented overnight and was opened up this morning. Target boat not fully sintered [see attached photos]. Chamber currently being pumped down again in order to continue with sintering TaC coating. HS cooling water valves were opened, no leaks detected. Will ramp up to 700A again over the weekend.  Friday, January 24, 2014, 14:21 Chamber was pumped down to 1.7e-7 Torr. TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A. Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.    Monday, January 27, 2014, 10:05 TGHT reached 700A over the weekend. Measured temp @ 2000C. TGHT auto-cool inititated at 2.0A/min.    Tuesday, January 28, 2014, 11:53 Chamber cooled down overnight, vented and opened up this morning. Target boat still has a strip of green, still not fully sintered! [see attached photos]. Chamber currently being pumped down again to attempt sintering - round 3.

 Tuesday, January 28, 2014, 13:06

Discussed with Peter. Instead of re-sintering the whole boat by itself, end caps will be inserted for sintering and will be placed further down the boat where the sintering process appears complete.

 Tuesday, February 18, 2014, 12:12

A new target boat was sprayed with TaC coating and let dry.
The target boat is NOT wrapped with Ta-heat shield.

Thermocouples have been attached to the target boat in order to monitor the internal temperature of the new target boat design. 

The boat was installed in Evap#2, chamber is currently being pumped down.

 Tuesday, February 18, 2014, 14:20

Chamber was pumped down this morning to 2.9e-6 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently at 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr; Bad vacuum: 4.00e-5 Torr.

Temperature reading on left: thermocouple touching edge of target boat; temperature reading on right: thermocouple floating in center of target boat.

 Wednesday, February 19, 2014, 09:11

TGHT has been slowly ramping up overnight at a rate of 0.2A/min

IGP1 = 3.9e-7 Torr, TGHT = 260A; stepping ramping rate up to 2.0A/min

 Wednesday, February 19, 2014, 15:25

IGP1 = 9.4e-7 Torr

Thermocouple T2 = 1267.8C

Internal temp measured with Mikron = 1600C

Increasing max setpoint to 720A due to previous not fully sintered new design of target boat.

 Thursday, February 20, 2014, 09:17

Thermocouple T2 = 1254.5C

Internal temp measured with Mikron = 1811C

IGP1 = 2.6e-7 Torr

Reached max setpoint yesterday evening.

Initiating auto-cooling at 2.0A/min.

 Friday, February 21, 2014, 10:47

Vented and opened chamber this morning.

Target boat not fully sintered. [see attached photos]

Close to a full sinter, and will re-sinter next week with endcaps, so will not re-sinter by itself.

 Tuesday, September 23, 2014, 15:00

A new target boat [new design with no end caps] was sprayed with TaC coating and let dry.

The target boat is wrapped with 3-layers of Ta-heat shield.

The boat was installed in EVAP2, chamber is currently being pumped down.

 Friday, August 10, 2012, 19:54

Target boat with TaC coating, inside covered with a 0.002 inches thick Ta foil, wrapped with a 0.002 inches thick Ta foil, contains a Ta foil with TaO coating.

See John's Ipad for their recipes.

Evaporator #2 is now auto-ramping overnight at 0.2 A/min, up to 830 A, with the maximum voltage limited at 14 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum).

Nikita Bernier wrote:

Friday, August 10, 2012, 19:54   Target boat with TaC coating, inside covered with a 0.002 inches thick Ta foil, wrapped with a 0.002 inches thick Ta foil, contains a Ta foil with TaO coating. See John's Ipad for their recipes. Evaporator #2 is now auto-ramping overnight at 0.2 A/min, up to 830 A, with the maximum voltage limited at 14 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum).

 Saturday, August 11, 2012, 19:15

Heating process was going smoothly up to 400 A. See Attachment 1.

Around 420 A, vacuum went up again and the voltage increased more quickly. It seems like resistance is building up. After reaching 530 A, the current was tapped down to 420 A in an effort to save the Ta boat. See Attachment 2.

The current will stay at 420 A for the weekend until John takes a look at this.

Nikita Bernier wrote:

Nikita Bernier wrote:  Friday, August 10, 2012, 19:54   Target boat with TaC coating, inside covered with a 0.002 inches thick Ta foil, wrapped with a 0.002 inches thick Ta foil, contains a Ta foil with TaO coating. See John's Ipad for their recipes. Evaporator #2 is now auto-ramping overnight at 0.2 A/min, up to 830 A, with the maximum voltage limited at 14 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum).    Saturday, August 11, 2012, 19:15 Heating process was going smoothly up to 400 A. See Attachment 1. Around 420 A, vacuum went up again and the voltage increased more quickly. It seems like resistance is building up. After reaching 530 A, the current was tapped down to 420 A in an effort to save the Ta boat. See Attachment 2. The current will stay at 420 A for the weekend until John takes a look at this.

 Monday, August 13, 2012, 13:46

 TGHT was ramped down at 2 A/min and then tapped down to 0A. See Attachment 1.  The target boat will be cooled down for about an hour before turning off the chiller.

 Monday, September 24, 2012, 15:01

The target boat with TaC coating is being used again. The inside of the boat is covered with a 0.002 inches thick Ta foil with TaC coating, wrapped with a 0.002 inches thick Ta foil.

Chamber was pumped down to 6e-6 Torr before the Heat Shield cooling water valve was opened. A small vacuum bump was detected (See attachment #1). It is not clear if it was caused by a water leak or not.

After consulting with Peter, I will wait for the vacuum to be below e-07 Torr before turning the target heater on.

Nikita Bernier wrote:

Monday, September 24, 2012, 15:01 The target boat with TaC coating is being used again. The inside of the boat is covered with a 0.002 inches thick Ta foil with TaC coating, wrapped with a 0.002 inches thick Ta foil. Chamber was pumped down to 6e-6 Torr before the Heat Shield cooling water valve was opened. A small vacuum bump was detected (See attachment #1). It is not clear if it was caused by a water leak or not. After consulting with Peter, I will wait for the vacuum to be below e-07 Torr before turning the target heater on.

 Monday, September 24, 2012, 18:02

The vacuum was stable until 1e-06 Torr. The target heater was turned on and tapped up to 60 A (0.8 V). 

Evaporator #2 is now auto-ramping overnight at 0.2 A/min, up to 800-850 A, with the maximum voltage limited at 14 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum). 

 Tuesday, September 25, 2012, 15:11

Sintering process is going smoothly. See Attachment 1. The auto-ramping was increased to 1 A/min up to 800-850 A.

Tuesday, September 25, 2012, 16:11 

And the voltage limit was increased to 18 V ! See Attachment 2.

 Tuesday, September 25, 2012, 19:13

Around 806 A (readback), voltage increased more quickly than the current. It seems like resistance is building up. After reaching 836 A (readback), the current was tapped down to 800 A (readback)/ 816 A (setting) in an effort to save the Ta boat. See Attachment 3. The current will stay at 800 A for ~4 hours before ramping down.

Nikita Bernier wrote:

Nikita Bernier wrote:  Monday, September 24, 2012, 15:01 The target boat with TaC coating is being used again. The inside of the boat is covered with a 0.002 inches thick Ta foil with TaC coating, wrapped with a 0.002 inches thick Ta foil. Chamber was pumped down to 6e-6 Torr before the Heat Shield cooling water valve was opened. A small vacuum bump was detected (See attachment #1). It is not clear if it was caused by a water leak or not. After consulting with Peter, I will wait for the vacuum to be below e-07 Torr before turning the target heater on.        Monday, September 24, 2012, 18:02 The vacuum was stable until 1e-06 Torr. The target heater was turned on and tapped up to 60 A (0.8 V).  Evaporator #2 is now auto-ramping overnight at 0.2 A/min, up to 800-850 A, with the maximum voltage limited at 14 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum).     Tuesday, September 25, 2012, 15:11 Sintering process is going smoothly. See Attachment 1. The auto-ramping was increased to 1 A/min up to 800-850 A.     Tuesday, September 25, 2012, 16:11  And the voltage limit was increased to 18 V ! See Attachment 2.    Tuesday, September 25, 2012, 19:13 Around 806 A (readback), voltage increased more quickly than the current. It seems like resistance is building up. After reaching 836 A (readback), the current was tapped down to 800 A (readback)/ 816 A (setting) in an effort to save the Ta boat. See Attachment 3. The current will stay at 800 A for ~4 hours before ramping down.

 Wednesday, September 26, 2012, 14:31

The current was tapped down twice as resistance was building up. After 4 hours at ~800 A, the TGHT was ramped down at 2 A/min. See Attachment 1. The target boat was cooled down for 4 hours before the chiller was turned off.

Also I had trouble measuring the temperature. I was unable to get a clear picture with the pyrometer. Therefore the exact temperature remains unknown, but from previous experiments, 800 A was about 1400°C.

The TaC coated Ta foil is very brittle. There is a lot of crystallisation on the Ta boat. See attachment 2. It is unlikely that the boat would survive many more sintering. Therefore it will be used for BeO pellets tests. 

When John gets back, I suggest we use a new boat coated with TaC, without additional layers. (See message #15 when this target boat was sintered up to 900A (local 893A/16.88V), Measured temp @ 1500°C)

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Thursday, April 27, 2017, 14:01 Target container contains 470 discs of SiC  Target packed length = 16cm.  Mass of SiC(green)  = 52.13g Discs in target are arranged as follows: 5singles / 1pack / 65singles / 1pack / 75singles / 1pack / 75singles / 2packs / 75singles / 1pack / 75singles / 1pack / 55singles / 1pack / 5singles Container is wrapped with 1x heatshield around each side of cooling fins; no end caps are inserted yet - coated spring inserted both sides to hold discs in place. Sintering temp = 1800C Chamber is currently being pumped down.  Friday, April 28, 2017, 13:06 HS water valves turned on this morning, no leaks detected. Tapped up manually to 40A Waited ~3hrs , vacuum stable. IGP1 = 4.13e-6 Torr Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively. TGHT max = 400A.  TBHT max at 230A.  Slope on OMEGA = 1.08 [see elog i.d. # 326 for reasoning behind OMEGA slope choice]  Tuesday, May 02, 2017, 09:24 IGP1 = 2.34e-6 Torr TBHT = 230A, 3.15V TGHT = 298A, 3.96V OMEGA = 1030C Vacuum stable, increasing ramping rate up to 0.5A/min  Tuesday, May 02, 2017, 13:20 IGP1 = 1.3e-5 Torr TGHT = 400A, 5.6V OMEGA = 1175C Increasing max setpoint to 500A     Wednesday, May 03, 2017, 13:33 TGHT had remained at 500A for 16hrs, vacuum had initially come down nicely. Vacuum was starting to creep up when i came in this morning before 8am,  IGP1 was at 1.2e-5 Torr TGHT = 500A, 7.77V OMEGA = 1440C Around 8:30 vacuum started to spike, so the TGHT was tapped down rapidly to 450A Tapping the TGHT down made no difference to the vacuum. By the time 450A was hit, it was too late and the spike in vacuum caused the evaporator to trip off. Turbo pump in epics showed on, turbo pump showed on according to TP direct controls. Everything was shut off and the venting tapped, this made it obvious the turbo pump was already off as there was no ramping down noises from the turbo pump. TP control box turned off then on again, at this point the controls showed a 'fail' message. Turns out the turbo pump control box was fried and that's what had caused the turbo pump to fail with no notice in epics causing the vacuum to spontaneously spike. Waiting on a new one from vacuum group... See photos attached of striptool screenshots.  Wednesday, May 03, 2017, 15:03 New TP control boxed installed. Turbo pump turned on, everything pumped down. Vacuum good, IGP1 = 6.92e-7 Torr. IGP2 still not working, won't turn on via epics. Tried unplugging and plugging back in...still appears red with 'fail' message...    Wednesday, May 03, 2017, 16:07 Unplugging and plugging back in seemed to work now that evap2 under vacuum IGP2 works again. Will look into replacement ion gauge...    Wednesday, May 03, 2017, 16:09 HS water valves opened, no leaks detected. Tapped up manually to 40A. Vacuum stable. IGP1 = 3.6e-7 Torr Initiated auto-ramp at 1.0A/min and 0.5A/min to 300A and 230A for the TGHT and TBHT respectively.  Thursday, May 04, 2017, 08:41 Reached 300A, 230A 10hrs ago. IGP1 = 1.5e-7 Torr OMEGA = 1070C Increasing max setpoint to 500A at a rate of 0.5A/min for TGHT  Thursday, May 04, 2017, 14:58 Back up to max setpoint that was reached before evap2 tripped off. TGHT = 500A, 7.65V IGP1 = 9.3e-7 Torr OMEGA = 1450C Increasing max setpoint to 550A, ramping up at a lower rate of 0.2A/min since this will be done overnight.  Friday, May 05, 2017, 08:53 TGHT = 550A, 8.64V IGP1 = 2.8e-7 Torr OMEGA = 1560C Increasing max setpoint to 600A at a ramping rate of 0.5A/min  Friday, May 05, 2017, 11:09 TGHT = 600A, 9.58V IGP1 = 7.3e-7 Torr OMEGA = 1670C Increasing max setpoint to 625A at a ramping rate of 0.5A/min  Friday, May 05, 2017, 12:05 TGHT = 625A, 10.05V IGP1 = 9.9e-7 Torr OMEGA = 1710C Increasing max setpoint to 650A at a ramping rate of 0.5A/min  Friday, May 05, 2017, 13:13 TGHT = 650A, 10.57V IGP1 = 1.1e-6 Torr OMEGA  = 1740C Mikron through left side windown on outside bottom left edge on container = 1750C Tapping up manually to 1800C  Friday, May 05, 2017, 13:42 Adjusted slope to 1.09 so same spot on leg using MIKRON = OMEGA TGHT = 680A, 11.08V IGP1 = 1.6e-6 Torr OMEGA = 1795C MIKRON = 1795C Plotting a temperature curve, the predicted required current to reach 1800C was 670A using a slope of 1.08 Currently sitting 10A above predicted required current. After several minutes, temperature dropped a few degrees to 1790C Window remains clear and uncoated. Tapped up to TGHT = 685A, 11.2V OMEGA = 1795C Will remain at this setpoint over the weekend.  Monday, May 08, 2017, 08:59 TGHT = 685A, 11.08V TBHT = 230A, 3.24V IGP1 = 1.98e-7 Torr OMEGA has lowered to 1342C Evap2 sat at max setpoints over the wknd. Will check window port before cooling...   *UPDATE ON TRIP-OFF* A closer look into the details using archives [see photos attached]: TP tripped off TBHT and TGHT at ~8e-5Torr Anything in the evaporator requires ~1hr to cool before turning things off. In this scenario, the target was @ ~1440C. so ~30min post TP trip, the target may still be at ~1000C. Anything above 0.02Torr could be close enough to atmopheric pressure that this would be cooling too fast and could lead to breaking the target/ cracking the Ta metal. As one can see in the screenshots attached, the vacuum lingered around 0.005Torr for ~2hrs before anything was done. This provided enough time for the target to cool before it was introduced to atmospheric pressure when the BV was closed when trying to figure out the problem. In summary, the target 'should' be OK...will inspect target further when removed from the evaporator.  Tuesday, May 09, 2017, 09:16 TGHT = 685A, 11.04V TGHT power supply = 686A, 11.31V TBHT = 230A, 3.24V TBHT power supply = 236A, 3.32V IGP1 = 1.6e-7 Torr IGP1 direct readout = 2.3e-7 mbar IGP2 = 6.8e-8 Torr IGP2 direct readout = 8.46e-8 Torr Evap2 reached max setpoint friday afternoon. Window clearly coated - see attached photo. Initiating auto cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.  Wednesday, May 10, 2017, 09:18 Vented in air and opened up this morning. Inspected container carefully for any cracks/ marks due to TP tripping off at 1450C Target looks good!  One sample disc removed for SEM. When removing disc for sample, the SiC came off the graphite backing and just SiC flake came out - see photo Photos attached showing inside container with no Si crystal formation/ good clear path all the way through target and sample removed for tests

 Thursday, April 27, 2017, 14:01

Target container contains 470 discs of SiC 

Target packed length = 16cm. 

Mass of SiC(green)  = 52.13g

Discs in target are arranged as follows: 5singles / 1pack / 65singles / 1pack / 75singles / 1pack / 75singles / 2packs / 75singles / 1pack / 75singles / 1pack / 55singles / 1pack / 5singles

Container is wrapped with 1x heatshield around each side of cooling fins; no end caps are inserted yet - coated spring inserted both sides to hold discs in place.

Sintering temp = 1800C

Chamber is currently being pumped down. 

Friday, April 28, 2017, 13:06

HS water valves turned on this morning, no leaks detected.

Tapped up manually to 40A

Waited ~3hrs , vacuum stable.

IGP1 = 4.13e-6 Torr

Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

TGHT max = 400A.  TBHT max at 230A. 

Slope on OMEGA = 1.08 [see elog i.d. # 326 for reasoning behind OMEGA slope choice]

 Tuesday, May 02, 2017, 09:24

IGP1 = 2.34e-6 Torr

TBHT = 230A, 3.15V

TGHT = 298A, 3.96V

OMEGA = 1030C

Vacuum stable, increasing ramping rate up to 0.5A/min

 Tuesday, May 02, 2017, 13:20

IGP1 = 1.3e-5 Torr

TGHT = 400A, 5.6V

OMEGA = 1175C

Increasing max setpoint to 500A

Laura Lambert wrote:

Thursday, April 27, 2017, 14:01 Target container contains 470 discs of SiC  Target packed length = 16cm.  Mass of SiC(green)  = 52.13g Discs in target are arranged as follows: 5singles / 1pack / 65singles / 1pack / 75singles / 1pack / 75singles / 2packs / 75singles / 1pack / 75singles / 1pack / 55singles / 1pack / 5singles Container is wrapped with 1x heatshield around each side of cooling fins; no end caps are inserted yet - coated spring inserted both sides to hold discs in place. Sintering temp = 1800C Chamber is currently being pumped down.  Friday, April 28, 2017, 13:06 HS water valves turned on this morning, no leaks detected. Tapped up manually to 40A Waited ~3hrs , vacuum stable. IGP1 = 4.13e-6 Torr Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively. TGHT max = 400A.  TBHT max at 230A.  Slope on OMEGA = 1.08 [see elog i.d. # 326 for reasoning behind OMEGA slope choice]  Tuesday, May 02, 2017, 09:24 IGP1 = 2.34e-6 Torr TBHT = 230A, 3.15V TGHT = 298A, 3.96V OMEGA = 1030C Vacuum stable, increasing ramping rate up to 0.5A/min  Tuesday, May 02, 2017, 13:20 IGP1 = 1.3e-5 Torr TGHT = 400A, 5.6V OMEGA = 1175C Increasing max setpoint to 500A

  Wednesday, May 03, 2017, 13:33

TGHT had remained at 500A for 16hrs, vacuum had initially come down nicely.

Vacuum was starting to creep up when i came in this morning before 8am,  IGP1 was at 1.2e-5 Torr

TGHT = 500A, 7.77V

OMEGA = 1440C

Around 8:30 vacuum started to spike, so the TGHT was tapped down rapidly to 450A

Tapping the TGHT down made no difference to the vacuum.

By the time 450A was hit, it was too late and the spike in vacuum caused the evaporator to trip off.

Turbo pump in epics showed on, turbo pump showed on according to TP direct controls.

Everything was shut off and the venting tapped, this made it obvious the turbo pump was already off as there was no ramping down noises from the turbo pump.

TP control box turned off then on again, at this point the controls showed a 'fail' message.

Turns out the turbo pump control box was fried and that's what had caused the turbo pump to fail with no notice in epics causing the vacuum to spontaneously spike.

Waiting on a new one from vacuum group...

See photos attached of striptool screenshots.

 Wednesday, May 03, 2017, 15:03

New TP control boxed installed.

Turbo pump turned on, everything pumped down.

Vacuum good, IGP1 = 6.92e-7 Torr.

IGP2 still not working, won't turn on via epics.

Tried unplugging and plugging back in...still appears red with 'fail' message...

Laura Lambert wrote:

Laura Lambert wrote:  Thursday, April 27, 2017, 14:01 Target container contains 470 discs of SiC  Target packed length = 16cm.  Mass of SiC(green)  = 52.13g Discs in target are arranged as follows: 5singles / 1pack / 65singles / 1pack / 75singles / 1pack / 75singles / 2packs / 75singles / 1pack / 75singles / 1pack / 55singles / 1pack / 5singles Container is wrapped with 1x heatshield around each side of cooling fins; no end caps are inserted yet - coated spring inserted both sides to hold discs in place. Sintering temp = 1800C Chamber is currently being pumped down.  Friday, April 28, 2017, 13:06 HS water valves turned on this morning, no leaks detected. Tapped up manually to 40A Waited ~3hrs , vacuum stable. IGP1 = 4.13e-6 Torr Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively. TGHT max = 400A.  TBHT max at 230A.  Slope on OMEGA = 1.08 [see elog i.d. # 326 for reasoning behind OMEGA slope choice]  Tuesday, May 02, 2017, 09:24 IGP1 = 2.34e-6 Torr TBHT = 230A, 3.15V TGHT = 298A, 3.96V OMEGA = 1030C Vacuum stable, increasing ramping rate up to 0.5A/min  Tuesday, May 02, 2017, 13:20 IGP1 = 1.3e-5 Torr TGHT = 400A, 5.6V OMEGA = 1175C Increasing max setpoint to 500A     Wednesday, May 03, 2017, 13:33 TGHT had remained at 500A for 16hrs, vacuum had initially come down nicely. Vacuum was starting to creep up when i came in this morning before 8am,  IGP1 was at 1.2e-5 Torr TGHT = 500A, 7.77V OMEGA = 1440C Around 8:30 vacuum started to spike, so the TGHT was tapped down rapidly to 450A Tapping the TGHT down made no difference to the vacuum. By the time 450A was hit, it was too late and the spike in vacuum caused the evaporator to trip off. Turbo pump in epics showed on, turbo pump showed on according to TP direct controls. Everything was shut off and the venting tapped, this made it obvious the turbo pump was already off as there was no ramping down noises from the turbo pump. TP control box turned off then on again, at this point the controls showed a 'fail' message. Turns out the turbo pump control box was fried and that's what had caused the turbo pump to fail with no notice in epics causing the vacuum to spontaneously spike. Waiting on a new one from vacuum group... See photos attached of striptool screenshots.  Wednesday, May 03, 2017, 15:03 New TP control boxed installed. Turbo pump turned on, everything pumped down. Vacuum good, IGP1 = 6.92e-7 Torr. IGP2 still not working, won't turn on via epics. Tried unplugging and plugging back in...still appears red with 'fail' message...

 Wednesday, May 03, 2017, 16:07

Unplugging and plugging back in seemed to work now that evap2 under vacuum

IGP2 works again.

Will look into replacement ion gauge...