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Entry  Thursday, April 27, 2017, 15:54, Laura Lambert, SiC, 39530-10, HP-FEBIAD, In progress, Sintering SiC#36 
    Reply  Wednesday, May 03, 2017, 13:48, Laura Lambert, SiC, 39530-10, HP-FEBIAD, Problems, Sintering SiC#36 vacuum_trip3.JPGvacuum_trip4.JPG
       Reply  Wednesday, May 03, 2017, 16:09, Laura Lambert, SiC, 39530-10, HP-FEBIAD, Problems resolved, Sintering SiC#36 
          Reply  Wednesday, May 03, 2017, 16:10, Laura Lambert, SiC, 39530-10, HP-FEBIAD, Done, Sintering SiC#36 8x
             Reply  Thursday, May 11, 2017, 11:36, Laura Lambert, SiC, 39530-10, HP-FEBIAD, Done, Sintering SiC#36 - not SiC#36: now back-up [SiC#36 should be HP-FEBIAD-CTL!!!] 
Message ID: 360     Entry time: Thursday, April 27, 2017, 15:54     Reply to this: 361
Author: Laura Lambert 
Target Material: SiC 
Target Oven W.O#: 39530-10 
Source: HP-FEBIAD 
Status: In progress 
Subject: Sintering SiC#36 

 Thursday, April 27, 2017, 14:01

Target container contains 470 discs of SiC 

Target packed length = 16cm. 

Mass of SiC(green)  = 52.13g

Discs in target are arranged as follows: 5singles / 1pack / 65singles / 1pack / 75singles / 1pack / 75singles / 2packs / 75singles / 1pack / 75singles / 1pack / 55singles / 1pack / 5singles

Container is wrapped with 1x heatshield around each side of cooling fins; no end caps are inserted yet - coated spring inserted both sides to hold discs in place.

Sintering temp = 1800C

Chamber is currently being pumped down. 


Friday, April 28, 2017, 13:06

HS water valves turned on this morning, no leaks detected.

Tapped up manually to 40A

Waited ~3hrs , vacuum stable.

IGP1 = 4.13e-6 Torr

Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

TGHT max = 400A.  TBHT max at 230A. 

Slope on OMEGA = 1.08 [see elog i.d. # 326 for reasoning behind OMEGA slope choice]


 Tuesday, May 02, 2017, 09:24

IGP1 = 2.34e-6 Torr

TBHT = 230A, 3.15V

TGHT = 298A, 3.96V

OMEGA = 1030C

Vacuum stable, increasing ramping rate up to 0.5A/min


 Tuesday, May 02, 2017, 13:20

IGP1 = 1.3e-5 Torr

TGHT = 400A, 5.6V

OMEGA = 1175C

Increasing max setpoint to 500A


 

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