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Entry  Thursday, April 27, 2017, 15:54, Laura Lambert, SiC, 39530-10, HP-FEBIAD, In progress, Sintering SiC#36 
    Reply  Wednesday, May 03, 2017, 13:48, Laura Lambert, SiC, 39530-10, HP-FEBIAD, Problems, Sintering SiC#36 vacuum_trip3.JPGvacuum_trip4.JPG
       Reply  Wednesday, May 03, 2017, 16:09, Laura Lambert, SiC, 39530-10, HP-FEBIAD, Problems resolved, Sintering SiC#36 
          Reply  Wednesday, May 03, 2017, 16:10, Laura Lambert, SiC, 39530-10, HP-FEBIAD, Done, Sintering SiC#36 8x
             Reply  Thursday, May 11, 2017, 11:36, Laura Lambert, SiC, 39530-10, HP-FEBIAD, Done, Sintering SiC#36 - not SiC#36: now back-up [SiC#36 should be HP-FEBIAD-CTL!!!] 
Message ID: 361     Entry time: Wednesday, May 03, 2017, 13:48     In reply to: 360     Reply to this: 362
Author: Laura Lambert 
Target Material: SiC 
Target Oven W.O#: 39530-10 
Source: HP-FEBIAD 
Status: Problems 
Subject: Sintering SiC#36 

Laura Lambert wrote:

 Thursday, April 27, 2017, 14:01

Target container contains 470 discs of SiC 

Target packed length = 16cm. 

Mass of SiC(green)  = 52.13g

Discs in target are arranged as follows: 5singles / 1pack / 65singles / 1pack / 75singles / 1pack / 75singles / 2packs / 75singles / 1pack / 75singles / 1pack / 55singles / 1pack / 5singles

Container is wrapped with 1x heatshield around each side of cooling fins; no end caps are inserted yet - coated spring inserted both sides to hold discs in place.

Sintering temp = 1800C

Chamber is currently being pumped down. 


Friday, April 28, 2017, 13:06

HS water valves turned on this morning, no leaks detected.

Tapped up manually to 40A

Waited ~3hrs , vacuum stable.

IGP1 = 4.13e-6 Torr

Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

TGHT max = 400A.  TBHT max at 230A. 

Slope on OMEGA = 1.08 [see elog i.d. # 326 for reasoning behind OMEGA slope choice]


 Tuesday, May 02, 2017, 09:24

IGP1 = 2.34e-6 Torr

TBHT = 230A, 3.15V

TGHT = 298A, 3.96V

OMEGA = 1030C

Vacuum stable, increasing ramping rate up to 0.5A/min


 Tuesday, May 02, 2017, 13:20

IGP1 = 1.3e-5 Torr

TGHT = 400A, 5.6V

OMEGA = 1175C

Increasing max setpoint to 500A


 

  Wednesday, May 03, 2017, 13:33

TGHT had remained at 500A for 16hrs, vacuum had initially come down nicely.

Vacuum was starting to creep up when i came in this morning before 8am,  IGP1 was at 1.2e-5 Torr

TGHT = 500A, 7.77V

OMEGA = 1440C

Around 8:30 vacuum started to spike, so the TGHT was tapped down rapidly to 450A

Tapping the TGHT down made no difference to the vacuum.

By the time 450A was hit, it was too late and the spike in vacuum caused the evaporator to trip off.

Turbo pump in epics showed on, turbo pump showed on according to TP direct controls.

Everything was shut off and the venting tapped, this made it obvious the turbo pump was already off as there was no ramping down noises from the turbo pump.

TP control box turned off then on again, at this point the controls showed a 'fail' message.

Turns out the turbo pump control box was fried and that's what had caused the turbo pump to fail with no notice in epics causing the vacuum to spontaneously spike.

Waiting on a new one from vacuum group...

See photos attached of striptool screenshots.


 Wednesday, May 03, 2017, 15:03

New TP control boxed installed.

Turbo pump turned on, everything pumped down.

Vacuum good, IGP1 = 6.92e-7 Torr.

IGP2 still not working, won't turn on via epics.

Tried unplugging and plugging back in...still appears red with 'fail' message...


 

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