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Entry  Wednesday, October 19, 2016, 16:52, Laura Lambert, UC2, 41790-6, LP-SIS, Done, Conditioning UCx#18 

 Wednesday, October 19, 2016, 16:47

Target container was previously coated with TaC spray and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block using one single foil/ layer

The target consists of 165 discs of UCx with 5.4cm in length

Materials: 4 packs of 5 {all made with 'modified' UC2cast} + 145 single discs{20 from 'modified cast'}

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 430A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog327 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, October 20, 2016, 10:11

Tapped up manually to 40A

Vacuum stable.

IG1 = 4.45e-6 Torr.

Initiating auto-ramp.


 Monday, October 24, 2016, 11:19

TGHT = 254A, 2.46V

Still ramping up...~half way to final setpoint

Vacuum dropped, looks good, IG1 = 6.77e-6 Torr


 Wednesday, October 26, 2016, 09:38

Target has remained at max setpoints for ~16hrs.

TGHT = 430A, 4.25V

IG1 = 2.3e-6 Torr

Conditioning/ re-carbonization process is now complete.

Initiating auto-cool at 1.0A/min


 Thursday, October 27, 2016, 15:35

UCx done.

Vented in Ar and transferred to glove box.

Looked inside before inserting 2nd endcap - clean view all the way through the materials to the endcap/ no visible shifting.

Ta coated spring helped hold materials in place, materials expanded minimally ~0.5cm

Pushed materials back to desired length.

Successfully removed a single disc for further analysis.

Second endcap now in with 2x graphite foils.

Both endcaps need expanding.

Ready for assembly.

Requires Rh foil - to be inserted during assembly.


 

Entry  Thursday, February 16, 2017, 15:09, Laura Lambert, UC2, 42218-12, LP-SIS, Done, Conditioning UCx#19 IMG_1578.JPGIMG_1587.JPGIMG_1594.JPGIMG_1598.JPG

 Thursday, February 16, 2017, 15:04

Target container was previously coated with TaC spray and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 200 discs of UCx with 7.3cm in length [6 packs of 5 + 170 single discs].

Discs in target are arranged as follows: 5singles / 1pack / 40singles / 1pack / 40singles / 2packs / 40singles / 1pack / 40singles / 1pack / 5singles

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 475A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog340 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.

NOTE: small bug in evap1 IOC. when current is tapped up 1A, it auto-taps back down 0.01A. should be OK, but will keep an eye on evaporator during conditioning process and acct for changes.


 Friday, February 17, 2017, 09:56

IG1 = 1.56e-6 Torr

Tapped up manually to 35A

Vacuum stable.

IG1 = 1.56e-6 Torr.

Initiating auto-ramp.


 Friday, February 24, 2017, 15:09

Local TGHT 473 A 4.63 V


Monday, February 27, 2017, 09:06 

Target has remained at max setpoints for 20+hrs [epics problems and archives currently not working so unable to find out exact time]

TGHT = 475A, 4.67V

IG1 = 1.48e-6 Torr

Conditioning process is now complete.

Initiating auto-cool at 1.0A/min


 Tuesday, February 28, 2017, 12:00

UCx conditioning process complete.

Vented in Ar and transferred to glove box this morning.


 Tuesday, April 11, 2017, 09:44

A few photos taken of the target post-conditioning.

Note a few flakes came out from one end - end disc from 'open' side flaked off.


 

Entry  Wednesday, July 12, 2017, 17:07, Laura Lambert, UC2, 42218-15, LP-SIS, In progress, Conditioning UCx#21 

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

    Reply  Thursday, July 13, 2017, 14:50, Laura Lambert, UC2, 42218-15, LP-SIS, Problems, Conditioning UCx#21 

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

    Reply  Wednesday, July 19, 2017, 14:15, Laura Lambert, UC2, 42218-15, LP-SIS, Problems resolved, Conditioning UCx#21 

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

    Reply  Wednesday, July 19, 2017, 14:17, Laura Lambert, UC2, 42218-15, LP-SIS, In progress, Conditioning UCx#21 

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

 Wednesday, July 19, 2017, 14:16

Tapped up manually to 30A yesterday.

Continued manual tap up today and reached 60A.

Initiated auto-ramp.

IG1 = 4.4e-6 Torr


 

    Reply  Thursday, July 20, 2017, 15:00, Laura Lambert, UC2, 42218-15, LP-SIS, Problems, Conditioning UCx#21 Capture.JPGCapture3.JPG

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

 Wednesday, July 19, 2017, 14:16

Tapped up manually to 30A yesterday.

Continued manual tap up today and reached 60A.

Initiated auto-ramp.

IG1 = 4.4e-6 Torr


 

 Thursday, July 20, 2017, 14:48

TGHT tripped off yesterday evening 

Auto-ramping was fixed but a few more glitches in the system caused the TGHT to trip.

Please refer to photos.

When auto-ramp is running and vacuum reaches the parameter set for 'Good Vacuum', the auto-ramp should stop until the vacuum drops below the good vacuum at which point it can then continue to auto-ramp.

When auto-ramp is running and vacuum reaches the parameter set for 'Bad Vacuum', the auto-ramp should initiate auto-cool/ramp-down until the vacuum drops to the good vacuum parameter at which point it can then proceed with the 'Good Vacuum' requirement.

With this scenario, the auto-ramp system ignored the parameters set for good and bad vacuum, proceeded past both points and continued to ramp until the vacuum eventually reached it's trip off vacuum causing the TGHT to trip.

The TGHT current was at ~90A when it tripped off, so the target should be OK.


 

    Reply  Thursday, July 20, 2017, 15:35, Laura Lambert, UC2, 42218-15, LP-SIS, Problems resolved, Conditioning UCx#21 

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

 Wednesday, July 19, 2017, 14:16

Tapped up manually to 30A yesterday.

Continued manual tap up today and reached 60A.

Initiated auto-ramp.

IG1 = 4.4e-6 Torr


 

 Thursday, July 20, 2017, 14:48

TGHT tripped off yesterday evening 

Auto-ramping was fixed but a few more glitches in the system caused the TGHT to trip.

Please refer to photos.

When auto-ramp is running and vacuum reaches the parameter set for 'Good Vacuum', the auto-ramp should stop until the vacuum drops below the good vacuum at which point it can then continue to auto-ramp.

When auto-ramp is running and vacuum reaches the parameter set for 'Bad Vacuum', the auto-ramp should initiate auto-cool/ramp-down until the vacuum drops to the good vacuum parameter at which point it can then proceed with the 'Good Vacuum' requirement.

With this scenario, the auto-ramp system ignored the parameters set for good and bad vacuum, proceeded past both points and continued to ramp until the vacuum eventually reached it's trip off vacuum causing the TGHT to trip.

The TGHT current was at ~90A when it tripped off, so the target should be OK.


 

 Thursday, July 20, 2017, 15:14

Turns out the auto-ramp was reading the vacuum of 'IGP1' which is what the old ion gauge used to be called for evap1 and is currently one on evap2

AKA attempting to take a vacuum reading from one that doesn't exist for evap1

This ion gauge is now labelled 'IGP' and the auto-ramp system now uses 'IGP' for the vacuum parameter confirmations.

Changed a few things in the auto-ramp system:

-Updated messages.

-Auto-ramp aborts when TGHT/TBHT trips off.

-Displays setpoint it is ramping up to for next step

-Confirms which ion gauge it is reading

-Displays final setpoint and increment on message board

-No longer displays TBHT as 'tripped off' when not running.

System updated.


 

    Reply  Thursday, July 20, 2017, 15:57, Laura Lambert, UC2, 42218-15, LP-SIS, Done, Conditioning UCx#21 IMG_3249.JPGIMG_3251.JPGIMG_3257.JPGIMG_3258.JPGIMG_3260.JPG

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

 Wednesday, July 19, 2017, 14:16

Tapped up manually to 30A yesterday.

Continued manual tap up today and reached 60A.

Initiated auto-ramp.

IG1 = 4.4e-6 Torr


 

 Thursday, July 20, 2017, 14:48

TGHT tripped off yesterday evening 

Auto-ramping was fixed but a few more glitches in the system caused the TGHT to trip.

Please refer to photos.

When auto-ramp is running and vacuum reaches the parameter set for 'Good Vacuum', the auto-ramp should stop until the vacuum drops below the good vacuum at which point it can then continue to auto-ramp.

When auto-ramp is running and vacuum reaches the parameter set for 'Bad Vacuum', the auto-ramp should initiate auto-cool/ramp-down until the vacuum drops to the good vacuum parameter at which point it can then proceed with the 'Good Vacuum' requirement.

With this scenario, the auto-ramp system ignored the parameters set for good and bad vacuum, proceeded past both points and continued to ramp until the vacuum eventually reached it's trip off vacuum causing the TGHT to trip.

The TGHT current was at ~90A when it tripped off, so the target should be OK.


 

 Thursday, July 20, 2017, 15:14

Turns out the auto-ramp was reading the vacuum of 'IGP1' which is what the old ion gauge used to be called for evap1 and is currently one on evap2

AKA attempting to take a vacuum reading from one that doesn't exist for evap1

This ion gauge is now labelled 'IGP' and the auto-ramp system now uses 'IGP' for the vacuum parameter confirmations.

Changed a few things in the auto-ramp system:

-Updated messages.

-Auto-ramp aborts when TGHT/TBHT trips off.

-Displays setpoint it is ramping up to for next step

-Confirms which ion gauge it is reading

-Displays final setpoint and increment on message board

-No longer displays TBHT as 'tripped off' when not running.

System updated.


 

Thursday, July 20, 2017, 15:57

Tapped up manually to 35A, 0.45V

IG1 = 5.26e-6 Torr

Re-initiated auto-ramp at 0.1A/min.


 Friday, July 21, 2017, 13:50

TGHT = 81A, 0.92V

IG1 = 5.2e-5 Torr

Vacuum currently yo-yo-ing, but stable.

Changing vacuum limits.

Vacuum limit stop at 1.0e-4 Torr, backing off at 5.0e-4 Torr.

TP = 28.4C, RT = 27.3C


 Thursday, July 27, 2017, 09:02

TGHT = 431A, 4.37V

IG1 = 1.32e-5 Torr

Vacuum stable.

Increasing ramping rate to 0.2A/min

TP = 26.7C, RT = 22.0C


 Friday, July 28, 2017, 09:35

TGHT = 450A, 4.59V

IG1 = 5.4e-6 Torr

Target has remained at max setpoint for 23hrs.

TP = 25.9C, RT = 19.5C

Initiating auto-cool at 1.0A/min


 Friday, August 04, 2017, 13:59

Evap1 was vented in Ar and transferred to the glove box on monday.

A few discs on opened end had slightly shifted [see photo], discs moved back in place - can see down into target.

Discoloration of Ta container to gold in some spots - this is normal as seen with most UCx targets

Target looks good.

Still requires 2nd endcap to be inserted.


 Monday, August 21, 2017, 11:13

Both endcaps in.

No Rh foil inserted.

Endcaps require expanding.


 

Entry  Tuesday, March 20, 2018, 14:52, Laura Lambert, UC2, 42218-13, LP-SIS, Done, Conditioning UCx#22 

 Tuesday, March 20, 2018, 14:43

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 230 discs of UCx with 7.28cm in length [6 packs of 5 + 200 single discs].

Discs in target are arranged as follows: 1pack / 55singles / 1pack / 50singles / 2packs / 50singles / 1pack / 45singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

An extra 5 single discs are loaded on the right side on top of the last pack, these discs will be removed after conditioning and analysed using SEM and XRD

The chamber is currently pumping down.

TGHT will be ramped up to 445A and TBHT will be ramped up to 230A [same parameters used to reach 1900C in evap2 when sintering TaC coating - elog402 evap2]

NOTE: This will be the first UCx target to go online using the TBHT in evap1 after the target is loaded with materials.


 Wednesday, March 21, 2018, 09:37

IGP1 = 2.47e-6 Torr

Tapped up manually to 40A.

TGHT = 40A, 0.61V

TBHT = 40A, 0.78V

Waited ~1hr, vacuum stable IG1 = 9.3e-6 Torr

Initiating auto-ramp for TGHT at a rate of 0.2A/min

Initiating auto-ramp for TBHT at a rate of 0.1A/min

Parameter setup: 5.0e-5 good vac, 8.0e-5 bad vac.


Wednesday, March 21, 2018, 13:02

TGHT = 57A, 0.72V

TBHT = 48A, 0.85V

IG1 = 5.8e-5 Torr

Vacuum stable.

Changing vacuum limits.

Vacuum limit stop at 3.0e-4 Torr, backing off at 6.0e-4 Torr.


 Monday, March 26, 2018, 09:32

TGHT = 450A, 4.54V

TBHT = 230A, 2.75V

IGP1 = 8.99e-7 Torr

Target has remained at max setpoint over weekend.

Initiating auto-cool at 1.0A/min for the TGHT and 0.5A/min for the TBHT.


 Wednesday, March 28, 2018, 11:31

Evap1 was vented in Ar and transferred to the glove box yesterday.

Inspection of target still required as well as 2nd endcap to be inserted.


 

Entry  Friday, May 11, 2018, 12:36, Marla Cervantes, UC2, 41369-2, LP-SIS, Done, UCx Fully loaded graphite insert thermal test - FL#1 180511-FL1_520A.png

 Thursday, May 10, 2018, 16:00 

Graphite insert fully loaded with UCx was loaded into previously TaC coated target container.

No end caps on Ta target container.

Weight of graphite tube + UCx discs = 27 g

Currently pumping down in evap1.


Friday, May 11, 2018, 11:41 

IGP1 = 1.13e-6 Torr

Good vac at 3.0e-4, bad vac at 6.0e-4 Torr.

Tapped up manually to 100A.

Pressure increased to ~2e-5 Torr

Vacuum stabilized after 40 min

IGP1 = 1e-5 Torr

Initiating auto ramp for TGHT @ 20 A/min to a max setpoint of 520 A

Initiating auto ramp for TBHT @ 10 A/min to a max setpoint of 245 A

Preassure increased o 1e-4 Torr and the auto ramp was aborted

After 8 min IGP1 = 3e-5 Torr

Initiating auto ramp for TGHT @ 10 A/min to a max setpoint of 520 A

Initiating auto ramp for TBHT @ 5 A/min to a max setpoint of 245 A

The vacuum is more stable.

TBHT reached 230 A at 13:00

TGHT reached 520 A at 13:24

Final pressure 1.15e-4 Torr

Target will stay at max current point for a week.


 Friday, May 18, 2018, 13:01
 
IGP1 = 8.03e-7 Torr
 
TGHT 5.67 V, 519.3 A
 
TBHT 2.59 V, 228.3 A
 
Initiation auto cool at  TGHT  -5 A/min
 
Initiation auto cool at  TBHT  -2 A/min
 
Friday, May 18, 2018, 13:58
 
Accelerating auto cool   TGHT  -10 A/min
 
Accelerating auto cool at  TBHT  -5 A/min

 Friday, May 18, 2018, 18:31

Evap1 was vented in Ar and UCx target was transferred to the glove box

Entry  Friday, August 03, 2018, 17:49, John Wong, UC2, , LP-SIS, In progress, Conditioning UCx#24 

Friday, August 03, 2018, 17:44

Target consists of 230 UCx discs, total packing length of 7.1cm. 

Container was previously coated/sintered with TaC (see elog #415) in Evap#2 with TGHT set to 450A/7.5V and TBHT 230A/4.2

Vacuum initial setting:

Good Vac = 5.0 e-5 Torr, Bad vac = 8.0 e-5 Torr.

pressure level will be monitored accordingly...

 

Auto-ramping setting

TGHT: 60 wait time, 0.2A/min, final 450A

TGHT: 60 wait time, 0.2A/min, final 230A.

 

Chamber is currently being pumped down.Good


 Monday, August 06, 2018, 00:04

Pressure at 3.6e-6 Torr. 

Initiate autoramping.


 Friday, August 10, 2018, 11:02

TGHT/TBHT have been at 450A(4.5V)/230A(2.9) for over 15 hours.

Pressure is stabilized at 5.2e-6 Torr. 

Initiated auto-cooling at 2A/min for TGHT and 1A/min for TBHT.


 

Entry  Thursday, October 11, 2018, 18:13, John Wong, UC2, , LP-SIS, In progress, Conditioning UCx#25 UC#25_conditioning.JPGUC#25_conditioning-450A.JPG

Thursday, October 11, 2018, 18:06

Target consists of 284 UCx discs, total packing length of 8.0 cm. 

Container was previously coated/sintered with TaC (see elog #417) in Evap#2 with TGHT set to 400A and TBHT 230A, but there was a problem with the readback.  Will ramp up TGHT to 400A to see if the carbonization is complete; if not, additional 50A on TGHT can be applied.

One end-cap is inserted on the right, wrt to the ionizer, and left end is open. 

Vacuum initial setting:

Good Vac = 5.0 e-5 Torr, Bad vac = 8.0 e-5 Torr.

pressure level will be monitored accordingly...

Auto-ramping setting

TGHT: 60 wait time, 0.2A/min, final 400A (or addtional of 50 A if required as mentioned above)

TGHT: 60 wait time, 0.2A/min, final 230A.

 Chamber is currently being pumped down.


 Friday, October 12, 2018, 15:35

Chamber has pumped down to 1.8e-6 Torr. 

Stepping up TGHT and TBHT to 40A.


 Friday, October 12, 2018, 17:07

TGHT/TBTH was held at 40A reaching max pressure of 1.7e-5 before slowly coming down. 

Initiated autoramping.


 Thursday, October 18, 2018, 11:10

TGHT reached to 400A/3.98V, pressure is coming down from the upper limit at around 320A which indicated the carbonization is approaching to completion (see attachment#1).  However, two more out-gassing steps are typically observed as TGHT reached around 450 A (see previous UCx conditioning process).  Currently the pressure is at 1.04 e-5 torr. 

Auto-ramping TGHT to 450A at 1A/min, continue to observe the vacuum...


 Thursday, October 18, 2018, 12:57

TGHT reached to 450A/4.6V. Pressure is coming down from 1.6 e-5 Torr. (see attachment#2).  Will remain at this heating current until pressure reached to mid 10-6 torr.


 

    Reply  Tuesday, October 23, 2018, 10:24, Marla Cervantes, UC2, , LP-SIS, Problems, Conditioning UCx#25 

John Wong wrote:

Thursday, October 11, 2018, 18:06

Target consists of 284 UCx discs, total packing length of 8.0 cm. 

Container was previously coated/sintered with TaC (see elog #417) in Evap#2 with TGHT set to 400A and TBHT 230A, but there was a problem with the readback.  Will ramp up TGHT to 400A to see if the carbonization is complete; if not, additional 50A on TGHT can be applied.

One end-cap is inserted on the right, wrt to the ionizer, and left end is open. 

Vacuum initial setting:

Good Vac = 5.0 e-5 Torr, Bad vac = 8.0 e-5 Torr.

pressure level will be monitored accordingly...

Auto-ramping setting

TGHT: 60 wait time, 0.2A/min, final 400A (or addtional of 50 A if required as mentioned above)

TGHT: 60 wait time, 0.2A/min, final 230A.

 Chamber is currently being pumped down.


 Friday, October 12, 2018, 15:35

Chamber has pumped down to 1.8e-6 Torr. 

Stepping up TGHT and TBHT to 40A.


 Friday, October 12, 2018, 17:07

TGHT/TBTH was held at 40A reaching max pressure of 1.7e-5 before slowly coming down. 

Initiated autoramping.


 Thursday, October 18, 2018, 11:10

TGHT reached to 400A/3.98V, pressure is coming down from the upper limit at around 320A which indicated the carbonization is approaching to completion (see attachment#1).  However, two more out-gassing steps are typically observed as TGHT reached around 450 A (see previous UCx conditioning process).  Currently the pressure is at 1.04 e-5 torr. 

Auto-ramping TGHT to 450A at 1A/min, continue to observe the vacuum...


 Thursday, October 18, 2018, 12:57

TGHT reached to 450A/4.6V. Pressure is coming down from 1.6 e-5 Torr. (see attachment#2).  Will remain at this heating current until pressure reached to mid 10-6 torr.


 

 Friday, October 19, 2018, 10:00

TRIUMF had a total power outage, the TBHT  and TGHT current had been ramped down already.


 

    Reply  Tuesday, October 23, 2018, 10:49, Marla Cervantes, UC2, , LP-SIS, Problems resolved, Conditioning UCx#25 

Marla Cervantes wrote:

John Wong wrote:

Thursday, October 11, 2018, 18:06

Target consists of 284 UCx discs, total packing length of 8.0 cm. 

Container was previously coated/sintered with TaC (see elog #417) in Evap#2 with TGHT set to 400A and TBHT 230A, but there was a problem with the readback.  Will ramp up TGHT to 400A to see if the carbonization is complete; if not, additional 50A on TGHT can be applied.

One end-cap is inserted on the right, wrt to the ionizer, and left end is open. 

Vacuum initial setting:

Good Vac = 5.0 e-5 Torr, Bad vac = 8.0 e-5 Torr.

pressure level will be monitored accordingly...

Auto-ramping setting

TGHT: 60 wait time, 0.2A/min, final 400A (or addtional of 50 A if required as mentioned above)

TGHT: 60 wait time, 0.2A/min, final 230A.

 Chamber is currently being pumped down.


 Friday, October 12, 2018, 15:35

Chamber has pumped down to 1.8e-6 Torr. 

Stepping up TGHT and TBHT to 40A.


 Friday, October 12, 2018, 17:07

TGHT/TBTH was held at 40A reaching max pressure of 1.7e-5 before slowly coming down. 

Initiated autoramping.


 Thursday, October 18, 2018, 11:10

TGHT reached to 400A/3.98V, pressure is coming down from the upper limit at around 320A which indicated the carbonization is approaching to completion (see attachment#1).  However, two more out-gassing steps are typically observed as TGHT reached around 450 A (see previous UCx conditioning process).  Currently the pressure is at 1.04 e-5 torr. 

Auto-ramping TGHT to 450A at 1A/min, continue to observe the vacuum...


 Thursday, October 18, 2018, 12:57

TGHT reached to 450A/4.6V. Pressure is coming down from 1.6 e-5 Torr. (see attachment#2).  Will remain at this heating current until pressure reached to mid 10-6 torr.


 

 Friday, October 19, 2018, 10:00

TRIUMF had a total power outage, the TBHT  and TGHT current had been ramped down already.


 

  Sunday, October 21, 2018, 1:00 pm

the pumps went out, and the communication with the IEVAP was recovered on Sunday, the vacuum was 160 mTorr,

the pumps were turned on again.


 

    Reply  Tuesday, October 23, 2018, 10:55, Marla Cervantes, UC2, , LP-SIS, Done, Conditioning UCx#25 OrangeCoat.jpgIonizerTube.jpgClosedSide.jpg

Marla Cervantes wrote:

Marla Cervantes wrote:

John Wong wrote:

Thursday, October 11, 2018, 18:06

Target consists of 284 UCx discs, total packing length of 8.0 cm. 

Container was previously coated/sintered with TaC (see elog #417) in Evap#2 with TGHT set to 400A and TBHT 230A, but there was a problem with the readback.  Will ramp up TGHT to 400A to see if the carbonization is complete; if not, additional 50A on TGHT can be applied.

One end-cap is inserted on the right, wrt to the ionizer, and left end is open. 

Vacuum initial setting:

Good Vac = 5.0 e-5 Torr, Bad vac = 8.0 e-5 Torr.

pressure level will be monitored accordingly...

Auto-ramping setting

TGHT: 60 wait time, 0.2A/min, final 400A (or addtional of 50 A if required as mentioned above)

TGHT: 60 wait time, 0.2A/min, final 230A.

 Chamber is currently being pumped down.


 Friday, October 12, 2018, 15:35

Chamber has pumped down to 1.8e-6 Torr. 

Stepping up TGHT and TBHT to 40A.


 Friday, October 12, 2018, 17:07

TGHT/TBTH was held at 40A reaching max pressure of 1.7e-5 before slowly coming down. 

Initiated autoramping.


 Thursday, October 18, 2018, 11:10

TGHT reached to 400A/3.98V, pressure is coming down from the upper limit at around 320A which indicated the carbonization is approaching to completion (see attachment#1).  However, two more out-gassing steps are typically observed as TGHT reached around 450 A (see previous UCx conditioning process).  Currently the pressure is at 1.04 e-5 torr. 

Auto-ramping TGHT to 450A at 1A/min, continue to observe the vacuum...


 Thursday, October 18, 2018, 12:57

TGHT reached to 450A/4.6V. Pressure is coming down from 1.6 e-5 Torr. (see attachment#2).  Will remain at this heating current until pressure reached to mid 10-6 torr.


 

 Friday, October 19, 2018, 10:00

TRIUMF had a total power outage, the TBHT  and TGHT current had been ramped down already.


 

  Sunday, October 21, 2018, 1:00 pm

the pumps went out, and the communication with the IEVAP was recovered on Sunday, the vacuum was 160 mTorr,

the pumps were turned on again.


 

 Monday, October 22, 2018, 9:00

The target was transferred to the Ar glove box.


 Tuesday, October 23, 2018, 10:19

Target was inspected:

- Discs were in place

- Orange coating formed on the open end of target container

Spring was removed, two graphite discs were introduced, end cap was placed.

Entry  Tuesday, October 30, 2018, 10:17, Marla Cervantes, UC2, 43044-7 , LP-SIS, In progress, UCx Fully loaded graphite insert thermal test - FL#1 Heat_test.JPG

 Tuesday, October 30, 2018, 10:12

A new LP-SIS was coated and syntered (e-log 420 Evaporator_2) 

The container was loaded with a graphite insert loaded with UCx

Graphite insert + UCx mass = 26.927 g

A current of 440 A TGHT and 230 A TBHT will be inputed to the contianer


IGP1 = 8.72e-7 Torr

 The current was tapped manually to 440 A TGHT and 230 A TBHT (see fig. Heatinf test)

Maximum pressure during heating = 1.7e-3 Torr.

Target will stay at maximum current for 1 week.

 

    Reply  Wednesday, October 31, 2018, 10:30, Marla Cervantes, UC2, 43044-7 , LP-SIS, Problems, UCx Fully loaded graphite insert thermal test - FL#1 current-trip_off.JPGepics.JPG

Marla Cervantes wrote:

 Tuesday, October 30, 2018, 10:12

A new LP-SIS was coated and syntered (e-log 420 Evaporator_2) 

The container was loaded with a graphite insert loaded with UCx

Graphite insert + UCx mass = 26.927 g

A current of 440 A TGHT and 230 A TBHT will be inputed to the contianer


IGP1 = 8.72e-7 Torr

 The current was tapped manually to 440 A TGHT and 230 A TBHT (see fig. Heating test)

Maximum pressure during heating = 1.7e-3 Torr.

Target will stay at maximum current for 1 week.

 Wednesday, October 31, 2018, 10:09

The current tripped off,  around 5:00 am, the pressure was below 1e-5 Torr (see fig. current-trip_off).

On a previous test, we measured the maximum temperature of the power supply = 33.3 C (e-log 227).

Power supply overheating doesn't seem to be the problem.

EPICS windows are half withe and not answering correctly.

Also, TBHT says that IGP1 < 500 mTorr, and its interlock needs reset (see figure EPICS).

    Reply  Wednesday, October 31, 2018, 15:23, Marla Cervantes, UC2, 43044-7 , LP-SIS, Done, UCx Fully loaded graphite insert thermal test - FL#1 Ta-container.png

Marla Cervantes wrote:

Marla Cervantes wrote:

 Tuesday, October 30, 2018, 10:12

A new LP-SIS was coated and syntered (e-log 420 Evaporator_2) 

The container was loaded with a graphite insert loaded with UCx

Graphite insert + UCx mass = 26.927 g

A current of 440 A TGHT and 230 A TBHT will be inputed to the contianer


IGP1 = 8.72e-7 Torr

 The current was tapped manually to 440 A TGHT and 230 A TBHT (see fig. Heating test)

Maximum pressure during heating = 1.7e-3 Torr.

Target will stay at maximum current for 1 week.

 Wednesday, October 31, 2018, 10:09

The current tripped off,  around 5:00 am, the pressure was below 1e-5 Torr (see fig. current-trip_off).

On a previous test, we measured the maximum temperature of the power supply = 33.3 C (e-log 227).

Power supply overheating doesn't seem to be the problem.

EPICS windows are half withe and not answering correctly.

Also, TBHT says that IGP1 < 500 mTorr, and its interlock needs reset (see figure EPICS).

 Wednesday, October 31, 2018, 15:20

The problem was reported to controls, it will be also reported to power supply group.

In the meantime, the target will be ramp-up again with the auto ramp at:

TGHT = 20 A/min to 440 A

TBHT = 10 A/min to 230 A 

The pressure before heating is 4.07e-7 Torr


Wednesday, October 31, 2018, 19:24

The maximum pressure during heating was 6.57e-6 Torr.

Current pressure 3.00e-6Torr


Wednesday, November 07, 2018, 18:37

IGP1 = 9.7e-7 Torr

 TGHT = -2 A/min to 0A

TBHT = -1 A/min to 0A 


 Thursday, November 08, 2018, 16:16

EVAP1 was vented with Ar, and target was transferred to glove box.

The mass of the loaded graphite insert changed to 26.854 g

That is a difference of 0.075 g

The tantalum container "cathode" crystalized (see fig)

The rest of the tantalum container did not change.

Entry  Wednesday, September 18, 2019, 09:57, Marla Cervantes, UC2, 44062-4, LP-SIS, Done, UCx28 Conditioning #1 

Wednesday, September 18, 2019, 07:48

A TaC coated target container  was loaded with a graphite cartridge with UCx

The target container has 3 heat shields


IGP1 = 9.3e-6 Torr

Autoramp set up to:

TGHT= 0.2 A/min to 438 A (same current used to reach 1900C in evap2 when sintering TaC coating - elog-455 evap2)

TBHT= 0.1 A/min 230 A

The limits are:

Good vacuum 5e-5 Torr

Bad vacuum 8e-5 Torr


Wednesday, September 18, 2019, 09:55

The autoramp where changed to 1 A/min on both the TGHt and the TGHT.


 Wednesday, September 18, 2019, 21:06

After 4 hours at TGHT = 4.15 V, 437.76 A and TBHT = 2.77 V, 228.31 A (and pressure of 1.07e-5 Torr)

The autoramp was set to TGHT = - 1 A/min and TBHT = -0.5 Torr


Tuesday, September 29, 2019, 14:05

 The EVAP1 was vented with Ar and the target was removed, 

The target was directly assembled after removing it from EVAP1

Finally, the assembly was transferred to the glove box

ELOG V2.9.2-2455