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Message ID: 455     Entry time: Friday, September 06, 2019, 11:58
Author: Darwin Ortiz Rosales 
Target Material:  
Target Oven W.O#: 44062-4 
Source: LP-SIS 
Status: Done 
Subject: TaC coating/sintering 

Friday, September 06, 2019, 11:20

Container was coated with Tac and wrapped with 2 Ta heat shields.

Desired temp=1900 C, Omega slope set =0.990

Chamber pumped down over night and will be initially tapped manually to 40A for both TGHT and TBHT.

Subsequently, current will be automatically ramped up in increments of 1A/min to reach 400A for TGHT and 230A for TBHT.

Then TGHT will be manually tapped to target temperature and allow to stabilize for a minimum of 3 hours.

Good vac at 3.0e-5 Torr

Bad vac at 5.0e-5 Torr


Friday, September 06, 2019, 11:32

IEVAP2:IGP1=9.6e-7 Torr

Tapping to 40A (TGHT and TBHT).


Friday, September 06, 2019, 12:54

Start autoramp

1A/min TGHT and TBHT

IGP1=4.0e-06 Torr


Friday, September 06, 2019, 13:29

TGHT = 70A, TBHT=70A, pressure started to spike rapidly so aborted autoramp and lowered the current to 66A for both TGHT and TBHT.

pressure continued to rise so tapped current to 60A.  A drop observed.  Will allow to stabilize.


Friday, September 06, 2019, 14:06

IGP1=5.3e-06 Torr.  Restart previous ramping. 


At 66A paused ramping.  IPG1= 1.0e-5 Torr

Friday, September 06, 2019, 15:44

IGP1=6.0e-6 Torr

Start modified autoramping: 0.4A/min for TGHT and TBHT.  Will manually tap up in the morning, over ham and eggs. 


Saturday, September 07, 2019, 10:52

 Will tap up to 423 A on TGHT as per attachment #1 regression

IGP1= 1.13e-6 Torr

OMEGA = 1802 C

TGHT= 401.0 A, 6.84V

TBHT=233.6A, 4.1V


Saturday, September 07, 2019, 11:06

Tapped up TGHT to 438A

OMEGA= 1903C

Will monitor and adjust if necessary.


Saturday, September 07, 2019, 15:06

IGP1 =  1.17e-6 Torr

TGHT = 7.46 V, 439.3 A

TBHT = 4.13 V, 233.4 A

Autoramps

TGHT = -2 A/min, TBHT = -1 A/min


Monday, September 09, 2019, 16:34

The EVAP2 was vented and the target container was removed. 

 

Attachment 1: 190906LPSIS_Sintering.PNG  48 kB  Uploaded Saturday, September 07, 2019, 11:53  | Show | Hide all
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