Marla Cervantes wrote:

Marla Cervantes wrote: Wednesday, January 29 2020, 05:55   A P2N container  with heat shields, and with a UO2/C loaded graphite container was installed in the EVAP1 Chamber is currently being evacuated. Thursday, January 30, 2020, 08:56 Pressure limits: Good vacuum 1e-1 Torr Bad vacuum 5e-1 Torr Initial pressure:  IGP1=1.52e-6Torr Current ramp set to 1A/min to 10 A, voltage is stable. Current ramp increased to 1A/10s to 100 A. The pressure started raising around 80 A. Current was kept 5min at at 100 A, voltage was stable Thursday, January 30, 2020, 09:32  Current ramp set to 1A/20s to 150 A (same pressure limits) Pressure keep increasing during heating Thursday, January 30, 2020, 09:53  Current was kept at 150 min during 5 min, the voltage is stable, pressure started to stabilize: IGP1 = 0.027 Torr TGHT = 0.418 V Ramp set to 1A/min to 200 A. Thursday, January 30, 2020, 10:02 Pressure decreasing: TGHT= 153 A   Thursday, January 30, 2020, 10:15 At 155 A while pressure decreasing, the power supply tripped off, Controls has been notified, waiting for instructions.

 Thursday, January 30, 2020, 11:51

Controls respond "It looks like the power supplies were tripped by either the pirani gauge (IEVAP:IGP1) or the Nuclear vent or by both. But, it did not look like that the interlock tree latched the bad condition when the power supplies tripped. I modified the PLC to properly latch the cause of the trip." and gave green light to restart the carbothermal reduction.

Marla Cervantes wrote:

Marla Cervantes wrote: Marla Cervantes wrote: Wednesday, January 29 2020, 05:55   A P2N container  with heat shields, and with a UO2/C loaded graphite container was installed in the EVAP1 Chamber is currently being evacuated. Thursday, January 30, 2020, 08:56 Pressure limits: Good vacuum 1e-1 Torr Bad vacuum 5e-1 Torr Initial pressure:  IGP1=1.52e-6Torr Current ramp set to 1A/min to 10 A, voltage is stable. Current ramp increased to 1A/10s to 100 A. The pressure started raising around 80 A. Current was kept 5min at at 100 A, voltage was stable Thursday, January 30, 2020, 09:32  Current ramp set to 1A/20s to 150 A (same pressure limits) Pressure keep increasing during heating Thursday, January 30, 2020, 09:53  Current was kept at 150 min during 5 min, the voltage is stable, pressure started to stabilize: IGP1 = 0.027 Torr TGHT = 0.418 V Ramp set to 1A/min to 200 A. Thursday, January 30, 2020, 10:02 Pressure decreasing: TGHT= 153 A   Thursday, January 30, 2020, 10:15 At 155 A while pressure decreasing, the power supply tripped off, Controls has been notified, waiting for instructions.    Thursday, January 30, 2020, 11:51 Controls respond "It looks like the power supplies were tripped by either the pirani gauge (IEVAP:IGP1) or the Nuclear vent or by both. But, it did not look like that the interlock tree latched the bad condition when the power supplies tripped. I modified the PLC to properly latch the cause of the trip." and gave green light to restart the carbothermal reduction.

 Thursday, January 30, 2020, 13:09

IGP1=5.9e-6Torr

Ramp set to 1A/10s to 200 A

Pressure rising too fast at 200 A, current reduced manually to 190 A

Pressure start dropping and system tripped, notify to controls again, "The strip tool shows the vacuum level shoot down to 0 then shoot back up for a quick second but that is enough to tell the PLC that IGP is “bad”"

Thursday, January 30, 2020, 15:58 

Restarting process to try to trip the system on purpose 

Initial pressure IGP1 = 2.7e-6Torr

Ramp set to 1/A/10s to 200 A, 0.59 V

Ramp set to 2A/10s to 300 A

Max pressure during process IGP1 = 0.03 Torr

Voltage increased and stabilized (see voltage rising).

Ramp kept at 2A/10s to 400 A

Thursday, January 30, 2020, 16:48 

TGHT = 1.54 V, 399.744 A

IGP1 = 0.00016 Torr and going down

Ramp set to 2A/10s to 500 A

Thursday, January 30, 2020, 17:02 

TGHT= 1.9V, 499.2 A

IGP1 = 0.00014 Torr

Ramp set to 2A/10s to 600 A

Ramp set to 0.5 A/min to 700 A, ramp stopped at 680 A

Manually tapped to 697 A

Pressure dropping indicated that carbothermal reduction is done.

Unfortunately, the system did not trip. 

Contact Gelo for the  next run, such that he can monitor the system and we can spot the problem.

Marla Cervantes wrote:

Marla Cervantes wrote: Marla Cervantes wrote: Marla Cervantes wrote: Wednesday, January 29 2020, 05:55   A P2N container  with heat shields, and with a UO2/C loaded graphite container was installed in the EVAP1 Chamber is currently being evacuated. Thursday, January 30, 2020, 08:56 Pressure limits: Good vacuum 1e-1 Torr Bad vacuum 5e-1 Torr Initial pressure:  IGP1=1.52e-6Torr Current ramp set to 1A/min to 10 A, voltage is stable. Current ramp increased to 1A/10s to 100 A. The pressure started raising around 80 A. Current was kept 5min at at 100 A, voltage was stable Thursday, January 30, 2020, 09:32  Current ramp set to 1A/20s to 150 A (same pressure limits) Pressure keep increasing during heating Thursday, January 30, 2020, 09:53  Current was kept at 150 min during 5 min, the voltage is stable, pressure started to stabilize: IGP1 = 0.027 Torr TGHT = 0.418 V Ramp set to 1A/min to 200 A. Thursday, January 30, 2020, 10:02 Pressure decreasing: TGHT= 153 A   Thursday, January 30, 2020, 10:15 At 155 A while pressure decreasing, the power supply tripped off, Controls has been notified, waiting for instructions.    Thursday, January 30, 2020, 11:51 Controls respond "It looks like the power supplies were tripped by either the pirani gauge (IEVAP:IGP1) or the Nuclear vent or by both. But, it did not look like that the interlock tree latched the bad condition when the power supplies tripped. I modified the PLC to properly latch the cause of the trip." and gave green light to restart the carbothermal reduction.  Thursday, January 30, 2020, 13:09 IGP1=5.9e-6Torr Ramp set to 1A/10s to 200 A Pressure rising too fast at 200 A, current reduced manually to 190 A Pressure start dropping and system tripped, notify to controls again, "The strip tool shows the vacuum level shoot down to 0 then shoot back up for a quick second but that is enough to tell the PLC that IGP is “bad”" Thursday, January 30, 2020, 15:58  Restarting process to try to trip the system on purpose  Initial pressure IGP1 = 2.7e-6Torr Ramp set to 1/A/10s to 200 A, 0.59 V Ramp set to 2A/10s to 300 A Max pressure during process IGP1 = 0.03 Torr Voltage increased and stabilized (see voltage rising). Ramp kept at 2A/10s to 400 A Thursday, January 30, 2020, 16:48  TGHT = 1.54 V, 399.744 A IGP1 = 0.00016 Torr and going down Ramp set to 2A/10s to 500 A Thursday, January 30, 2020, 17:02  TGHT= 1.9V, 499.2 A IGP1 = 0.00014 Torr Ramp set to 2A/10s to 600 A Ramp set to 0.5 A/min to 700 A, ramp stopped at 680 A Manually tapped to 697 A Pressure dropping indicated that carbothermal reduction is done. Unfortunately, the system did not trip.  Contact Gelo for the  next run, such that he can monitor the system and we can spot the problem.

 Friday, January 31, 2020, 15:35

The EVP1 was vent with Ar and the P2N target was transferred to the glove box.

 Tuesday, May 26, 2019, 18:20

A loaded graphite cartridge was set in a tantalum boated and wrapped with 3 tantalum sheets (Friday May 22, 2020)

The set up was installed in the EVAP1 and pumped down during the weekend.

IGP1 = 7.10 e-7 Torr

Good vacuum = 1e-1 Torr

Bad vacuum = 5e-1 Torr

Current ramp is 1A per 10s from 0A to 120A

Wednesday, June 03, 2020, 08:11 

A loaded graphite cartridge was set in a tantalum boated and wrapped with 3 tantalum sheets (Friday May 29, 2020)

The set up was installed in the EVAP1 then IEVAP:IGP1 was replaced (elogs 260 and 261).  

Vacuum was turned on after Ion Gauge swap.

IGP1 = 3.6 e-5 Torr

Good vacuum = 5e-2 Torr

Bad vacuum = 5e-1 Torr

Current ramp is 1A per 10s from 0A to 120A

Wednesday, June 03, 2020, 09:59 

After about 20 minutes at 120 A, TGHT tripped again exactly as before.

Will restart ramp at 1A per 10s from 0A to 120A .  Will set good vacuum to 1e-2 Torr

IGP1= 4.3e-05 Torr

Wednesday, June 03, 2020, 10:57

IGP1 =  9e-4 Torr

Pressure peaked around 4e-3 Torr and now trending down

TGHT =120 A

Wednesday, June 03, 2020, 11:23

IGP1=9.5e-5 Torr

Good Vacuum 1e-02 Torr

Bad Vacuum 5e-1 Torr

Starting TGHT ramp to 550 A at 3A per 10s  

Wednesday, June 03, 2020, 14:41

ramp up was good.  TGHT at 550 A since 12:30 pm.  TGHT did not trip. *note adjusted good vacuum.  Ramping takes a little longer but doesn't trigger TGHT shutdown.

Wednesday, June 03, 2020, 22:55

IGP1 =  3.5e-5 Torr

TGHT = 249.4 A, 5.7 V

Start ramp down at -2A per minute to 0 A

Marla Cervantes wrote:

Marla Cervantes wrote: Marla Cervantes wrote: Marla Cervantes wrote: Marla Cervantes wrote: Wednesday, January 29 2020, 05:55   A P2N container  with heat shields, and with a UO2/C loaded graphite container was installed in the EVAP1 Chamber is currently being evacuated. Thursday, January 30, 2020, 08:56 Pressure limits: Good vacuum 1e-1 Torr Bad vacuum 5e-1 Torr Initial pressure:  IGP1=1.52e-6Torr Current ramp set to 1A/min to 10 A, voltage is stable. Current ramp increased to 1A/10s to 100 A. The pressure started raising around 80 A. Current was kept 5min at at 100 A, voltage was stable Thursday, January 30, 2020, 09:32  Current ramp set to 1A/20s to 150 A (same pressure limits) Pressure keep increasing during heating Thursday, January 30, 2020, 09:53  Current was kept at 150 min during 5 min, the voltage is stable, pressure started to stabilize: IGP1 = 0.027 Torr TGHT = 0.418 V Ramp set to 1A/min to 200 A. Thursday, January 30, 2020, 10:02 Pressure decreasing: TGHT= 153 A   Thursday, January 30, 2020, 10:15 At 155 A while pressure decreasing, the power supply tripped off, Controls has been notified, waiting for instructions.    Thursday, January 30, 2020, 11:51 Controls respond "It looks like the power supplies were tripped by either the pirani gauge (IEVAP:IGP1) or the Nuclear vent or by both. But, it did not look like that the interlock tree latched the bad condition when the power supplies tripped. I modified the PLC to properly latch the cause of the trip." and gave green light to restart the carbothermal reduction.  Thursday, January 30, 2020, 13:09 IGP1=5.9e-6Torr Ramp set to 1A/10s to 200 A Pressure rising too fast at 200 A, current reduced manually to 190 A Pressure start dropping and system tripped, notify to controls again, "The strip tool shows the vacuum level shoot down to 0 then shoot back up for a quick second but that is enough to tell the PLC that IGP is “bad”" Thursday, January 30, 2020, 15:58  Restarting process to try to trip the system on purpose  Initial pressure IGP1 = 2.7e-6Torr Ramp set to 1/A/10s to 200 A, 0.59 V Ramp set to 2A/10s to 300 A Max pressure during process IGP1 = 0.03 Torr Voltage increased and stabilized (see voltage rising). Ramp kept at 2A/10s to 400 A Thursday, January 30, 2020, 16:48  TGHT = 1.54 V, 399.744 A IGP1 = 0.00016 Torr and going down Ramp set to 2A/10s to 500 A Thursday, January 30, 2020, 17:02  TGHT= 1.9V, 499.2 A IGP1 = 0.00014 Torr Ramp set to 2A/10s to 600 A Ramp set to 0.5 A/min to 700 A, ramp stopped at 680 A Manually tapped to 697 A Pressure dropping indicated that carbothermal reduction is done. Unfortunately, the system did not trip.  Contact Gelo for the  next run, such that he can monitor the system and we can spot the problem.  Friday, January 31, 2020, 15:35 The EVP1 was vent with Ar and the P2N target was transferred to the glove box.

 Thursday, August 13, 2020, 14:33

XRD analysis of the P2N material showed that the carbothermal reduction was not completed

The material was loaded again in its oven, new Ta caps where secured to the edges, the body remained the same

The oven was set in the EVAP1 using Ar to avoid oxidation of the P2N material

Currently pumping down.

 Saturday, August 15, 2020, 14:45 

Vacuum is having a strange behavior, pressure shows that is going from 8e-11 to 4e-6 Torr (fig. 200815-Vaccum_P2N)

Proceeded to turn off turbo pump

Tuesday, August 18, 2020, 10:38

The IGP1 head was replaced with the EVAP1's IGP1 head

The vacuum will be started again

Marla Cervantes wrote:

Marla Cervantes wrote: Marla Cervantes wrote: Marla Cervantes wrote: Marla Cervantes wrote: Marla Cervantes wrote: Wednesday, January 29 2020, 05:55   A P2N container  with heat shields, and with a UO2/C loaded graphite container was installed in the EVAP1 Chamber is currently being evacuated. Thursday, January 30, 2020, 08:56 Pressure limits: Good vacuum 1e-1 Torr Bad vacuum 5e-1 Torr Initial pressure:  IGP1=1.52e-6Torr Current ramp set to 1A/min to 10 A, voltage is stable. Current ramp increased to 1A/10s to 100 A. The pressure started raising around 80 A. Current was kept 5min at at 100 A, voltage was stable Thursday, January 30, 2020, 09:32  Current ramp set to 1A/20s to 150 A (same pressure limits) Pressure keep increasing during heating Thursday, January 30, 2020, 09:53  Current was kept at 150 min during 5 min, the voltage is stable, pressure started to stabilize: IGP1 = 0.027 Torr TGHT = 0.418 V Ramp set to 1A/min to 200 A. Thursday, January 30, 2020, 10:02 Pressure decreasing: TGHT= 153 A   Thursday, January 30, 2020, 10:15 At 155 A while pressure decreasing, the power supply tripped off, Controls has been notified, waiting for instructions.    Thursday, January 30, 2020, 11:51 Controls respond "It looks like the power supplies were tripped by either the pirani gauge (IEVAP:IGP1) or the Nuclear vent or by both. But, it did not look like that the interlock tree latched the bad condition when the power supplies tripped. I modified the PLC to properly latch the cause of the trip." and gave green light to restart the carbothermal reduction.  Thursday, January 30, 2020, 13:09 IGP1=5.9e-6Torr Ramp set to 1A/10s to 200 A Pressure rising too fast at 200 A, current reduced manually to 190 A Pressure start dropping and system tripped, notify to controls again, "The strip tool shows the vacuum level shoot down to 0 then shoot back up for a quick second but that is enough to tell the PLC that IGP is “bad”" Thursday, January 30, 2020, 15:58  Restarting process to try to trip the system on purpose  Initial pressure IGP1 = 2.7e-6Torr Ramp set to 1/A/10s to 200 A, 0.59 V Ramp set to 2A/10s to 300 A Max pressure during process IGP1 = 0.03 Torr Voltage increased and stabilized (see voltage rising). Ramp kept at 2A/10s to 400 A Thursday, January 30, 2020, 16:48  TGHT = 1.54 V, 399.744 A IGP1 = 0.00016 Torr and going down Ramp set to 2A/10s to 500 A Thursday, January 30, 2020, 17:02  TGHT= 1.9V, 499.2 A IGP1 = 0.00014 Torr Ramp set to 2A/10s to 600 A Ramp set to 0.5 A/min to 700 A, ramp stopped at 680 A Manually tapped to 697 A Pressure dropping indicated that carbothermal reduction is done. Unfortunately, the system did not trip.  Contact Gelo for the  next run, such that he can monitor the system and we can spot the problem.  Friday, January 31, 2020, 15:35 The EVP1 was vent with Ar and the P2N target was transferred to the glove box.  Thursday, August 13, 2020, 14:33 XRD analysis of the P2N material showed that the carbothermal reduction was not completed The material was loaded again in its oven, new Ta caps where secured to the edges, the body remained the same The oven was set in the EVAP1 using Ar to avoid oxidation of the P2N material Currently pumping down.  Saturday, August 15, 2020, 14:45  Vacuum is having a strange behavior, pressure shows that is going from 8e-11 to 4e-6 Torr (fig. 200815-Vaccum_P2N) Proceeded to turn off turbo pump Tuesday, August 18, 2020, 10:38 The IGP1 head was replaced with the EVAP1's IGP1 head The vacuum will be started again

 Tuesday, August 18, 2020, 20:44

The pressure reading are normal after swapping the IGP1's gauge head

Wednesday, August 19, 2020, 07:47 

XRD analysis of the P2N material showed that the carbothermal reduction was not completed

The material was loaded again in its oven, new Ta caps where secured to the edges, the body remained the same

The oven was set in the EVAP1 using Ar to avoid oxidation of the P2N material

See elog 263

Wednesday, August 19, 2020, 07:47

Good vacuum 1e-1 Torr

Bad vacuum 5e-1 Torr

IGP1 = 4.11e-6 Torr

Autoramp set to 1A/10s to 150 A.

Wednesday, August 19, 2020, 10:00

TGHT = .45 V, 149.8 A

IGP1 = 9.1e-5 Torr

 Autoramp set to 1A/10s to 200 A.

Wednesday, August 19, 2020, 10:13

TGHT = 0.6 V, 200.2 A

IGP1 = 3e-4 Torr and increasing

After 6 min:

good vacuum =  5e-2 Torr

bad vacuum = 1e-1 Torr

autoramp set to 1A/30s to 250 A

Since the pressure was decreasing, the ramp was changed to  1A/10s to 250 A, vacuum limits remained the same

Wednesday, August 19, 2020, 10:28

Good vacuum 1e-1 Torr

Bad vacuum 5e-1 Torr

IGP1 = 1.7e-4 Torr

TGHT =  0.78 V, 250.1 A

Autoramp set to 2.5 A/10 s to 700 A

Wednesday, August 19, 2020, 11:17

 Good vacuum 1e-1 Torr

Bad vacuum 5e-1 Torr

IGP1 = 2e-4 Torr

TGHT = 2.64 V, 699 A

Autoramp set to 2 A/10 s to 800 A

 Wednesday, August 19, 2020, 11:29

 Good vacuum 1e-1 Torr

Bad vacuum 5e-1 Torr

IGP1 = 5.2e-5 Torr

TGHT = 3.1 V, 798.8 A

Note: Voltage starts to become unstable, an power is around 2.3 kW, pressure has not increased enough to indicate reduction with certainty

In order to reach 3 kW autoramp set to 1A/10 s to 900 A

Wednesday, August 19, 2020, 12:18

The current was increased to 1000 A expecting to see a high peak in pressure but there was not an increase in preasure.

The target is being ramped down to 850 A 

 Tuesday, September 08, 2020, 20:44

A P2N oven with three heat shields, loaded with a graphite container filled with UO2/C ring-discs was set in the EVAP1

EVAP1 is currently being evacuated.

Wednesday, September 09, 2020, 10:11

IGP1 = 4.7e-6 Torr

Good vacuum 1e-1 Torr

Bad vacuum 5e-1 Torr

Autoramp set to 1A/10s to 150 A.

Wednesday, September 09, 2020, 10:50 

TGHT = .32 V, 149.8 A

IGP1 = 6.5e-5 Torr

Autoramp set to 1A/10s to 200 A 

Wednesday, September 09, 2020, 11:00

TGHT =0.46 V, 200 A

IGP1 =  6e-4 Torr and going up

good vacuum =  5e-2 Torr

bad vacuum = 1e-2 Torr

autoramp set to 1A/10s to 250 A

autoramp stopped at 215 A, since pressure kept increasing, the current was manually decreased to 180 A.

 Wednesday, September 09, 2020, 11:16

TGHT = 0.4 V, 179.7 A,

IGP1 = 8.5e-4 Torr an going down

good vacuum =  5e-2 Torr

bad vacuum = 1e-2 Torr

autoramp set to 1A/30s to 200 A

Wednesday, September 09, 2020, 11:32

TGHT = 0.46 V, 200.2 A,

IGP1 = 3e-3 Torr an going down

good vacuum =  5e-2 Torr

bad vacuum = 1e-2 Torr

autoramp set to 1A/30s to 300 A

Wednesday, September 09, 2020, 11:38

IGP1 = 1e-3 Torr 

Since the pressure was decreasing, the ramp was stopped at 210 and changed to  1A/10s to 300 A, vacuum limits remained the same

Wednesday, September 09, 2020, 11:53

The pressure reached the bad vacuum limit 1e-2 Torr and stopped

After ~8min the pressure limits were changed to:

good vacuum =  5e-2 Torr

bad vacuum = 1e-1 Torr

Wednesday, September 09, 2020, 12:05 

IGP1 = 1.15e-3 Torr

Autoramp set to 2.5 A/10 s to 700 A

Pressure increased! and ramp paused at 685 A

re-started autoramp to 700 A at 1A/10s

Wednesday, September 09, 2020, 13:56

Pressure kept increasing after 700 A, so autoramp was set to 750 A at  1A/10s

Pressure kept increasing

At 750 A pressure started reducing, autoramp was set to 760 A at 1A/10 s

System tripped suddenly (Gelo was notified)

The carbothermal reduction seemed complete 

 Thursday, September 10, 2020, 14:01

A P2N target was carbothermal reduced but at the maximum current, the power supply tripped (elog. 267)

Therefore, the target was not hot long enough to fully outgas, that is why it will be reheated.

Desired current 650 A

Thursday, September 10, 2020, 14:07 

IGP1 =  3.3e-6 Torr

Autoramp set to 650 A at 1 A/10 s 

Thursday, September 10, 2020, 16:06

Ramp reached desired current

TGHT = 2.4 V, 649 A

IGP1 = 3e-3 Torr 

 Friday, September 11, 2020, 11:17

TGHT = 2.24 V, 649.2 A

IGP1 = 3.7e-6 Torr

Friday, September 11, 2020, 12:55 

 TGHT = 2.2 V, 648.8 A

IGP1 = 3.7e-6 Torr

Autoramp set to 700 A at 1 A/10 s,

No more gas was released, the system was ramped down to 0 A at 2 A/min

Friday, September 11, 2020, 18:17

TGHT = 0.35 V, 133 A

IGP1 = 2.7e-6 Torr

 Friday, September 11, 2020, 20:01

TGHT = 0 V, 2.56 A

IGP1 = 2.6e-6 Torr

Monday, September 14, 2020, 16:19

EVAP1 was vented with Ar and the P2N material was transferred to the preparatory glove box. 

Green target material characteristics  (elog 105)

#discs = 49

Average disc thickness = 0.453mm

Empty cartridge weight = 9.42 g

Full cartridge weight = 39.86 g

UO2+C weight = 30.44 g 

Tuesday, March 30, 2021, 16:04

The target material was loaded in a P2N oven, wrapped with three heat shields, and set in the EVAP1

EVAP1 is currently being evacuated.

Wednesday, March 31, 2021, 09:42

IGP1 = 3.24e-6 Torr

Good vacuum 1e-1 Torr

Bad vacuum 5e-1 Torr

Autoramp set to 1A/10s to 150 A. 

Wednesday, March 31, 2021, 10:17

TGHT = .54 V, 149.88 A

IGP1 = 6.3e-4 Torr and increasing

Max pressure = 0.06 Torr

Wednesday, March 31, 2021, 10:33 

IGP1= 0.004 Torr

Autoramp set to 1A/10s to 200 A

Wednesday, March 31, 2021, 10:43

Maximum pressure 0.03 Torr and going down

Autoramp set to 1A/10s to 250 A

Wednesday, March 31, 2021, 11:04 

TGHT = 1.1 V, 299.9 A

IGP1 = 6e-4 Torr and going down

Autoramp set to 2.5 A/10 s to 700 A

Wednesday, March 31, 2021, 11:35

Ramp stopped at 690 A

TGHT = 2.9V, 689.1A

IGP1 = 0.127 Torr 

Wednesday, March 31, 2021, 11:37

Autoramp  set to 700 A at 1A/20s

Manually ramped to 740 A (3V) to make sure carbothermal reduction is done.

 Wednesday, March 31, 2021, 12:00

The power supply tripped, Gelo was monitoring the heating process.

Wednesday, March 31, 2021, 14:33

The target will be heated for 4 hours to get read of impurities.

IGP1 = 6e-6 Torr 

Autoramp set to 650 at 1A/10s 

Wednesday, March 31, 2021, 20:37

TGHT = 2.77 V, 669.6A 

IGP1 = 8.5e-6 Torr

EVAP1 ramped down to 0 A at 2 A/min

Target #34 was installed in the EVAP1 and pumped down (Tuesday June 29, 2021).

Target #34 is going to be conditioned on a Ta boat wrapped with 3 Ta foils.

IGP1 = 1.85e-6 Torr

Good vacuum = 1e-1 Torr

Bad vacuum = 5e-1 Torr

Power desired 1.6kW. This is the second target conditioned this way. 

Subsequent targets should be conditioned following thermal reduction.

 Thursday, July 01, 2021, 06:05

IGP1= 1.35e-06 Torr

Start autoramp @2A/30s to 400A

Thursday, July 01, 2021, 07:59

Pressure increase was observed near 400A 

will ramp to 450A and  keep for 8 hours

IGP1= 1.4 e-05 Torr

450A and 4.0V reached at 8:14 am on Thursday July 01, 2021

Rampdown @-2A/min was started at 4.14 pm on Thursday July 01, 2021 IGP1 stable at 2.7e-06Torr

Cannot transfer into glovebox yet because moisture is a bit high after regeneration.  Moisture is dropping. Will wait until moisture is sufficiently low.

Monday, July 05, 2021, 20:43

Cartridge was removed and placed in bag inside glovebox

Removed 10 discs for analysis but might place them back inside depending on final decision.  We had previously removed 10 discs after thermal reduction.

 Wednesday, July 07, 2021, 14:39

Target Provisional ID = 200929 was installed in the EVAP1 and pumped down (Tuesday July 7, 2021).

Target is going to be thermally reduced for 8 hours and then conditioned for an additional 8 hours

IGP1 = 2.0 e-6 Torr

Good vacuum = 1e-1 Torr

Bad vacuum = 5e-1 Torr

Power desired 1.6kW.

10 extra discs included for analysis

Wednesday, July 07, 2021, 14:49 

Ramping up TGHT at 6A/min [wait interval = 10 s at increments of 1A]

Wednesday, July 07, 2021, 15:58

IGP1= 5.7 e-5 Torr and trending down.  Will start ramp up to 450A at  18A/min [wait interval 10s at 3A increments]

Wednesday, July 07, 2021, 16:20 

IGP1= 2.2e-3 Torr

Will continue ramping TGHT to 500A and watch pressure

Wednesday, July 07, 2021, 16:26

Continue ramping to 550 at 3A/10s

 Wednesday, July 07, 2021, 16:29

holding at 550A, 5.1V for 8 hours 

Wednesday, July 07, 2021, 23:41 

TGHT = 550A, 5.7 V

begin ramp down at -2A/min to 450A and leave for 8 hours

Thursday, July 08, 2021, 08:20

 IGP1= 2.7 e-06 Torr

TGHT = 450A, 4.5V

Will start ramp down at -2A/min to 0A 

 Thursday, September 23, 2021, 06:55

A loaded graphite cartridge was set in a tantalum boated and wrapped with 3 tantalum sheets (Wednesday September 22)

IGP1 = 3.6 e-5 Torr

Good vacuum = 5e-2 Torr

Bad vacuum = 5e-1 Torr

Current ramp is 2A per min from 0A to 120A and 1A/10s from 120A to (450-550A)

Thursday, September 23, 2021, 07:09 

IGP1 = 1.84 e-06 Torr

Start Autoramp to 120A @ 2A/min 

Thursday, September 23, 2021, 10:25

Start Autoramp to 550A @ 1A/10s

 IGP1= 1.05e-05 Torr

TGHT= 120 A, 1.06 V

Thursday, September 23, 2021, 11:57 

Pressure drop observed at 530A.  Start 4 hour count.  

Thursday, September 23, 2021, 15:57 

IGP1= 9.1e-06 Torr

After 4 hour reduction started rampdown to 400A at 2A/30s.

8 hour conditioning to start at 16:15 pm

Friday, September 24, 2021, 00:16

TGHT= 399.8 A, 3.5V

IGP1= 2.4 e-06 Torr 

Start ramp down at 2A/min

Wednesday, June 01, 2022, 08:39

A loaded graphite cartridge was set in a tantalum boated and wrapped with 3 tantalum sheets (previous day)

IGP1 = 1.6 e-6 Torr

Good vacuum = 5e-2 Torr

Bad vacuum = 5e-1 Torr

Current ramp is 1A per 10s from 0A to 40A then continue to 80A at 1A/10s.  Then at 1A/min to 120 A and allow degas and then autoramp 1A/10s from 120A to (450-550A)

Wednesday, June 01, 2022, 09:51

IGP1= 3.0e-4 Torr

TGHT = 120A, 1.0V

Start autoramp at 1A/10s to 420A

Wednesday, June 01, 2022, 10:02

Increased ramp rate to 3A/10 s as per SOP to 440 A then will slow down the ramp to observe pressure behavior.

Wednesday, June 01, 2022, 10:19

At 430 A, autoramp set to 1A/10s to 500A as pressure was increasing. 

Will observe behavior of pressure curve then leave for 4 hours

Wednesday, June 01, 2022, 11:04

Pressure started dropping at 520A.  Stopped ramping and will leave for 4 hours.

Wednesday, June 01, 2022, 14:48

Autoramp to 400 A at 2A/30s and leave for 8 hour treatment

Wednesday, June 01, 2022, 23:00

IGP1= 2.1e-6 Torr

TGHT= 400A

Ramping down @-2A/min to 0A

Thursday, June 02, 2022, 10:09

IGP1= 6.7e-7 Torr

Ready to dismount

Friday, June 03, 2022, 06:24

A loaded graphite cartridge was set in a tantalum boated and wrapped with 3 tantalum sheets (previous day)

IGP1 = 1.4 e-6 Torr

Good vacuum = 5e-2 Torr

Bad vacuum = 5e-1 Torr

Current ramp is 1A per 10s from 0A  to 80A at 1A/10s.  Then at 1A/min to 120 A, allow degas and then autoramp 1A/10s from 120A to (450-550A)

Friday, June 03, 2022, 06:52

starting autoramp at 1A/min to 120A

Friday, June 03, 2022, 07:30

note*: At approximately 108A the pressure did not rise again but was stable.

Friday, June 03, 2022, 07:46

started autoramp at 1A/10s to 450A 

Friday, June 03, 2022, 09:29

start autoramp to 500A at 1A/min

Friday, June 03, 2022, 09:40

pressure keeps stable as ramping continues. 

increased ramp rate to 2A/min

Friday, June 03, 2022, 09:56

Drop in pressure observed as current increased at 2A/min.

Final current is 490A.  Will keep at this current for 4 hours. 

Friday, June 03, 2022, 14:05

Start auroramp to 400A at -2A/30s

will keep at 400A for 8 hours

Friday, June 03, 2022, 22:06

Start autoramp down at -2A/min to 0A

IGP1= 1.6e-06 Torr

TGHT= 400A, 3.6 V

Tuesday, June 07, 2022, 07:05

A loaded graphite cartridge was set in a tantalum boated and wrapped with 3 tantalum sheets (previous day)

IGP1 = 1.2 e-6 Torr

Good vacuum = 5e-2 Torr

Bad vacuum = 5e-1 Torr

Current ramp is 1A per 10s from 0A to 80A at 1A/10s.  Then at 1A/min to 120 A and allow degas and then autoramp 1A/10s from 120A to (450-550A)

Tuesday, June 07, 2022, 08:28

IGP1=9.8e-5 Torr

TGHT = 120A, 0.85V

Start autoramp at 1A/10s to 420A

Tuesday, June 07, 2022, 08:45

Increased ramp rate to 3A/10 s as per SOP to 450 A then will slow down the ramp to observe pressure behavior.

Tuesday, June 07, 2022, 09:04

slowed autoramp to 2A/min to observe (1A/30s)

some erratic pressure oscillations observed then stabilized. 

Tuesday, June 07, 2022, 09:32

At TGHT = 495A pressure started dropping even while current ramping up.  Stopped ramp.  Will keep for 4 hours.

TGHT = 495.6A, 4.7V

Tuesday, June 07, 2022, 13:30

TGHT = 495.6 A, 4.7V

IGP1= 8.5 e-6 Torr

Start rampdown to 400A at 2A/30s and leave for 8 hour treatment

Friday, October 07, 2022, 07:55

Cartridge-220928UCx was installed in the EVAP1 and pumped down yesterday.

Material will be reduced in LP-SIS wrapped with 3 Ta foils.

IGP1 = 2.1e-6 Torr

a cap was installed to collect material coming out from the ionizer tube

The initial weight of the cap 1 + small bag was recorded to be: 2.82 g   Final weight of cap1 + small bag = 2.84g (see attached picture)

Good vacuum = 5e-4 Torr

Bad vacuum = 5e-2 Torr

Power desired 1900W as approximate power used online. 

Will autoramp @2A/min to 30A, then slow down ramp to 1A/min to 120A.

After first pressure bump cleared, will ramp up to 400 A @ 2A/20s to 425A on TGHT.  TBHT will be topped off at 230A. 

from 425A, TGHT will be ramped at 1A/min and monitored for pressure behaeviour. 

sytem will be left at reduction current for 4 hours.  Then, the current will be dropped to 1900W and allow to run for 8 hours.

The cup will be collected and the system will be run again in increments of two hours. 

*slight change from test plan to save time*

Friday, October 07, 2022, 21:55

A true pressure max was not observed.  A max while current still rising.  stopped at 560A on TGHT and 5.3V

will leave at the above conditions for 4 hours.

Suspect that the thinner Ta shields make a difference.  Suggest to add a fourth shield and process the previous cartridge in a tube rather than a boat.  Treat for four hours (pressure max) and then test increasing the current to see if there is a pressure bump.  If no pressure bump then lower current to deposit 1900W for 8 additional hours. 

After 4 hours at max current, the current was dropped to 450A (TGHT) and left for 8 hours.

Saturday, October 08, 2022, 09:26

start autoramp down @-2A/min for TGHT and -1A/min for TBHT

Cap+ bag = 2.82 g

final cap +bag = 2.84 g

Tuesday, October 11, 2022, 10:15

Today will switch end-cup.  Will weigh new end-cup and place inside the evap1 glovebox.  Then will remove used end-cap and install new end-cap.  Used end-cup will be weighed on same balance as before.  All mass measurements will be done with the same balance. Note, that a makeshift balance air isolation container was built to allow balance to not be affected by air currents.

 Cap 2+bag initial weight = 2.80 g +/- 0.01 g

Cap 2+bag final weight = 2.81g +/- 0.01 g

No visible deposition on cap

Wednesday, October 12, 2022, 07:51

Start ramp up at 2A/min.  TGHT to 450A, TBHT to 230A

IGP1= 6.7e-07Torr

Wednesday, October 12, 2022, 09:47

Ramping up @ 4A/min to same final settings: TGHT = 450A and TBHT = 230A

Wednesday, October 12, 2022, 11:15

@10:45am 450A, 4.15V were reached on TGHT

Will leave for 2 hours at 450A then ramp down, then switch cap. 

Monday, October 17, 2022, 09:40

The second cap was taken out over the weekend  (attachment number 2).

The final weight of this cap with bag = 2.81 +/- 0.01 g

Installed a nex cap (3) with initial weigh of cap +bag = 2.74 g

Allowed vacuum to settle over Sunday and will start ramping today

Will ramp to 470 A and hold for 2 hours.  Ramp rate  2A /30s

IGP1= 4.6e-07 Torr

 Monday, October 17, 2022, 11:39

ramping with no issues.  will finish ramp around 12:03 pm and will start rampdown @ around 2:05 pm.

Monday, October 17, 2022, 12:03

TGHT= 470A, 4.5V

TBHT= 228A, 2.9V

IGP1= 5.6e-06 Torr

Monday, October 17, 2022, 14:05

Start rampdown at 2A/min TGHT and 1A/min TBHT to zero amp

current IGP1= 2.6e-06 Torr

TGHT = 470A, 4.5V

TBHT= 228.3A, 2.9V

Tuesday, October 18, 2022, 09:39

IGP1=4.4e-7 Torr

ready to dismount

Tuesday, October 18, 2022, 13:50

Cap 3 + bag initial weight = 2.74 g

Final weight of cap+bag = 2.74 g (no change)

no visible deposition on cap either

Monday, November 28, 2022, 05:58

Left weekend to pump down

current IGPI= 7.23e-7 Torr

Material will be reduced in LP-SIS wrapped with 3 Ta foils.

a cap was installed to collect material coming out from the ionizer tube

Initial weight of target material plus cartridge was recorded

All relevant data and findings will be reported and added to docushare as document :

Good vacuum = 5e-4 Torr

Bad vacuum = 5e-2 Torr

Power desired 1900W as approximate power used online. 

Will autoramp @2A/min to 30A, then slow down ramp to 1A/min to 120A.

After first pressure bump cleared, will ramp up to 400 A @ 2A/20s to 425A on TGHT.  TBHT will be topped off at 230A. 

from 425A, TGHT will be ramped at 1A/min and monitored for pressure behaeviour. 

sytem will be left at reduction current for 4 hours.  Then, the current will be dropped to 425 A and allow to run for 8 hours.

The cup will be collected and the system will be run again for two hours. at the same current until no material visible on cap.  Then it will be run at 450A for increments of two hours until no significant mass change of target material.

Monday, November 28, 2022, 06:05

started initial heating to 30A at 2A/min on both TGHT and TBHT.

Monday, November 28, 2022, 08:46

was ramping at 6A/min (2A/20s) on both tGHT and TBHT but aborted due to pressure spike.  will allow pressure to stabilize.

TGHT = 162A, 1.35V

TBH 162A, 1.9V

Monday, November 28, 2022, 08:51

Restarting the heating at 6A/min (2A/20s)

Monday, November 28, 2022, 09:21

Pausing heating @ TGHT= 323 A 3.0V

Allow pressure to stabilize to better spot reduction current

Monday, November 28, 2022, 09:49

Started heating TGHT at 2A/min so reduction current can be better resolved

Monday, November 28, 2022, 10:12

heating aborted to allow pressure to stabilize

IGP1> 5.0e-4 Torr

Monday, November 28, 2022, 11:31

IGP1= 1.5e-4 Torr start autoramp TGHT @1A/min

Monday, November 28, 2022, 11:51

paused heating.  Second peak has been passed.  Will let pressure drop before starting heating again to try and better observe reduction peak.

Monday, November 28, 2022, 12:46

start autoramp at 2A/min from 389A on TGHT

IGP1- 6.4e-6 Torr

Monday, November 28, 2022, 14:21

Pressure starts to drop at around 535A, but large bump observed around 386A. 

Will leave four hours. 

TGHT= 539A, 4.98V

TBHT= 229A, 2.9V

Monday, November 28, 2022, 18:19

Ramping down at 4A/min to 425A

Currently IGP1= 6.2e-6 Torr

TGHT = 539A, 4.98 V

TBHT= 230A, 2.98V

Monday, November 28, 2022, 22:23

425 A on TGHT reached at 6:50 pm.  Will ramp down at 2:50 am .  -2A/min TGHT and -1A/min TBHT

Tuesday, November 29, 2022, 09:34

Final IGP1 when TGHT and TBHT = 0A  is 5.0e-7 Torr

Tuesday, November 29, 2022, 14:08

Weighed materials and reloaded

Currently at 1.1 e-05 Torr

Will initiate heat ramp at 2A/min to 425 A

@241A increase ramp rate to 4A/min on TGHT

Wednesday, November 30, 2022, 12:44

heating B finished and cartridge loading for heating C

Current pressure = 2.09 E-05 Torr.  Will ramp up to 450A at 4A/min and regulate as needed.

Will heat at 450A TGHT for 2 hours, TBHT max= 230A

Wednesday, November 30, 2022, 16:30

Starting rampdown @-2A/min TGHT and -1A/min TBHT

Final heating was @ 450A, 4.0V TGHT and 230A, 2.7V TBHT

Friday, December 02, 2022, 09:00

IGP1= 7.2 e-07 Torr

Starting ramp at 2A/min to 450A on TGHT and 230A on TBHT

Friday, December 02, 2022, 10:02

pressure stated dropping.  Will increase ramp to 4A/min (2A/30s)

Friday, December 02, 2022, 15:35

Starting ramp down at -2A/min TGHT and -1A/min TBHT

IGP1= 2.6 e-06 Torr

TGHT 450A   4.2V

TBHT  230A  2.9V

Monday, December 19, 2022, 10:38

Cartridge with 175 discs (including 5 analysis discs) loaded into a graphite cartridge. 

To be reduced inside a Ta container tube.  Tube wrapped in 3 Ta foil heatshields

Will keep at reducing current for 4 hours and then 10 hours @ 425A

Good Vacuum: 5.0e-04 Torr

Bad Vacuum: 5.0e-02 Torr

Initial pressure was 6.36 e-07 Torr

Autoramped to 56A @ 1A/30s

Outgassing bump observed starting at 50A and at 56A the maximum pressure was ~1.9e-05 Torr

Monday, December 19, 2022, 10:47

started autoramping at 1A/30s to 90A

Monday, December 19, 2022, 10:50

observed that pressure not increasing radically, therefore ramping up faster.  2A/30s

Monday, December 19, 2022, 10:58

Second pressure bump observed at 90A, 1.0V

leaving at this current until pressure drops

Monday, December 19, 2022, 17:15

ramped to 280A and left at 280 until pressure started dropping

ramping again to 500A @ 2A/30s

Monday, December 19, 2022, 17:26

Stopped at 330A due to pressure hike.  Will allow pressure to drop then continue ramp.

Monday, December 19, 2022, 18:00

restarting ramp @ 2A/30s

Monday, December 19, 2022, 18:11

Pressure started dropping around 350A corresponding to additive gas-off.  Will rampt to 500A @ 2A/30 seconds and then at 1A/30s to 530A

Final current was 548A, 6.7 V.  Will test increasing current after 4 hours (11 pm)

Monday, December 19, 2022, 23:10

ramping down @ 2A/min to 425A .  should be done by 12:00 am and cooling at9:00 am (includes 1 hour ramp down to 425).

Ramping down to zero @ -2A/min

Wednesday, December 21, 2022, 10:47

Final IGP1= 3.7e-07 Torr