Wednesday, June 01, 2022, 08:39
A loaded graphite cartridge was set in a tantalum boated and wrapped with 3 tantalum sheets (previous day)
IGP1 = 1.6 e-6 Torr
Good vacuum = 5e-2 Torr
Bad vacuum = 5e-1 Torr
Current ramp is 1A per 10s from 0A to 40A then continue to 80A at 1A/10s. Then at 1A/min to 120 A and allow degas and then autoramp 1A/10s from 120A to (450-550A)
Wednesday, June 01, 2022, 09:51
IGP1= 3.0e-4 Torr
TGHT = 120A, 1.0V
Start autoramp at 1A/10s to 420A
Wednesday, June 01, 2022, 10:02
Increased ramp rate to 3A/10 s as per SOP to 440 A then will slow down the ramp to observe pressure behavior.
Wednesday, June 01, 2022, 10:19
At 430 A, autoramp set to 1A/10s to 500A as pressure was increasing.
Will observe behavior of pressure curve then leave for 4 hours
Wednesday, June 01, 2022, 11:04
Pressure started dropping at 520A. Stopped ramping and will leave for 4 hours.
Wednesday, June 01, 2022, 14:48
Autoramp to 400 A at 2A/30s and leave for 8 hour treatment
Wednesday, June 01, 2022, 23:00
IGP1= 2.1e-6 Torr
TGHT= 400A
Ramping down @-2A/min to 0A
Thursday, June 02, 2022, 10:09
IGP1= 6.7e-7 Torr
Ready to dismount |