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Message ID: 281     Entry time: Wednesday, June 01, 2022, 08:42
Author: Darwin Ortiz Rosales 
Target Material: UO2/C 
Target Oven W.O#: Target Boat 
Source:  
Status: Done 
Subject: UO2 reduction Provisional ID C211209-1  

Wednesday, June 01, 2022, 08:39

A loaded graphite cartridge was set in a tantalum boated and wrapped with 3 tantalum sheets (previous day)

IGP1 = 1.6 e-6 Torr

Good vacuum = 5e-2 Torr

Bad vacuum = 5e-1 Torr

Current ramp is 1A per 10s from 0A to 40A then continue to 80A at 1A/10s.  Then at 1A/min to 120 A and allow degas and then autoramp 1A/10s from 120A to (450-550A)

 


Wednesday, June 01, 2022, 09:51

IGP1= 3.0e-4 Torr

TGHT = 120A, 1.0V

Start autoramp at 1A/10s to 420A


Wednesday, June 01, 2022, 10:02

Increased ramp rate to 3A/10 s as per SOP to 440 A then will slow down the ramp to observe pressure behavior.


Wednesday, June 01, 2022, 10:19

At 430 A, autoramp set to 1A/10s to 500A as pressure was increasing. 

Will observe behavior of pressure curve then leave for 4 hours


Wednesday, June 01, 2022, 11:04

Pressure started dropping at 520A.  Stopped ramping and will leave for 4 hours.


Wednesday, June 01, 2022, 14:48

Autoramp to 400 A at 2A/30s and leave for 8 hour treatment


Wednesday, June 01, 2022, 23:00

IGP1= 2.1e-6 Torr

TGHT= 400A

Ramping down @-2A/min to 0A


Thursday, June 02, 2022, 10:09

IGP1= 6.7e-7 Torr

Ready to dismount

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