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ID Date Author Target Materialdown Target Oven W.O# Source Status Subject
  530   Tuesday, February 23, 2021, 08:59 Marla Cervantes NA (Cu-tube) DoneRe coating Test 2

 Tuesday, February 23, 2021, 08:49

Yesterday a heat shield was washed and when dry it was installed in the EVAP2,

A 1mm thick rhenium wire was held within two copper brackets to pass through a Cu tube with the intention of coating its inside face


Tuesday, February 23, 2021, 08:58  IGP1 = 7.7e-7 Torr

Pressure 5.88e-7 Torr, current rate set to 10 A @ 0.5 A/min


Pressure 6.1e-7 Torr, current rate set to 20 A @ 0.5 A/min


Pressure 8.51e-7 Torr current rate set to 30 A @ 0.5 A/min, temperature corrected 1800 degC (measured with filament pyrometer)

After 10 min the current and voltage are stable and the pressure is going down


Tuesday, February 23, 2021, 16:25

It seems like the wire is touching the tube so the system will be cool down.

Pressure 6.8e-7 Torr current rate set to 0A at -0.1 A/min


 Tuesday, February 23, 2021, 17:38

Pressure 6e-7 Torr, TGHT = 23.3 A, 4.854 V, Temp 1788 deg C Omega, 1540 degC filament

current rate set to 0A at 0.2A/min 


Wednesday, February 24, 2021, 09:37

Venting EVAP2 


Wednesday, February 24, 2021, 16:47

The wire and Cu tube were  fix such that the wire's deformation does not lead it to touch the tube, then the assembly was attached again and the EVAP2 was pumped down.

IGP1 = 9.3e-7 Torr, current rate is set to 5 A at 0.5 A/min

Wednesday, February 24, 2021, 17:04

IGP1 = 9e-7 Torr TGHT = 5.175A, 0,749 V

current rate is set to 10 A at 0.5 A/min


Wednesday, February 24, 2021, 17:23

IGP1 = 8.8e-7 Torr, TGHT = 10A, 1.78V

current rate is set to 20 A at 0.5 A/min

Since the wire seemed to be touching the tube, the system was vented.

The tube was shifted and the heat shield installed again, the system was pumped over nigth.


Thursday, February 25, 2021, 09:15

A water leak was performed and no leak was observed

IGP1= 4.95e-7 Torr

Thursday, February 25, 2021, 09:32  The current is increased at 0.5 A/min to 5 A


Thursday, February 25, 2021, 10:00

The current was tapped manually at 0.5 A to 6 A the wire is now glowing dimmly

Current rate set to 10A at .5 A/min

Current rate set to 20 A at 0.5A/min


Current rate set to 30 A at 0.5A/min

Thursday, February 25, 2021, 11:17  IGP1= 5.7e-7 Torr, TGHT=30.5A, 6.718V, filament=1740 degC

voltage and current stable, pressure going down.


Thursday, February 25, 2021, 11:21

Current rate set to 40 A at 0.4 A/min


Thursday, February 25, 2021, 11:53 IGP1 = 5.9e-7 Torr, TGHT = 9.267V, 39.15A, filament = 2060 degC

voltage and current stable, pressure going down.

Current rate set to 50 A @ 0.2A/min

During ramping the voltage reduced a bit and I decided to stop the ramp and reduce the current, the voltage stayed constant but the current started increasing slowly without me inputting it so I decided to ramp down the current at 0.2A/min.

When the current reached 0A the power supplies and the pumps were turned off, after an ~1h when the turbo pump had already stopped, the EVAP2 was vented and open.


The wire sintered to the copper tube confirming that the wire was in contact with the tube during heating.

The Cu tube present a grey metallic coloration indicating a Re coating.

The set up together with the copper heat shield were removed from the

  532   Monday, March 01, 2021, 13:58 Aaron Schmidt    Flex - line HS installed

Flex-Line HS had been fully scrubbed out earlier. All gaskets replaced.

Empty. Quick check for leaks.

Monday, March 01, 2021, 13:57: Roughing.

Monday, March 01, 2021, 14:13: TP1 on. 

Monday, March 01, 2021, 15:18: Vacuum @ 1.01e-05T. Open HS waterline. 

Monday, March 01, 2021, 15:24: Vacuum @ 9.30e-06T & dropping. Waterline ok. 

Monday, March 01, 2021, 15:25: Turbo pump off. Vent when ready. 

  537   Tuesday, March 23, 2021, 08:07 Aaron Schmidt    Re - Ta test. Leak check.

 Modified HS installed with new brackets as per Marla.

Tuesday, March 23, 2021, 08:02: Vacuum @ 3.64e-07T. Waterlines opened.

Tuesday, March 23, 2021, 08:06: Vacuum @ 3.60e-07T. Stable.

  539   Thursday, March 25, 2021, 07:57 Aaron Schmidt    Re - Ta test. Leak check.

Thursday, March 25, 2021, 07:55: Vacuum @ 5.12e-07T. Waterlines opened.

Thursday, March 25, 2021, 07:55: Vacuum @ 5.09e-07T. Stable.

  543   Sunday, March 28, 2021, 11:24 Marla Cervantes NA (Ta-tube) DoneRe-coat 3

Objective: Coating the inner surface of a tantalum tube to make a destructive test and use a reference for the tantalum boats coatings

Results: The tube was coated


Sunday, March 28, 2021, 11:23

No water leak

IGP1 = 2.3e-7 torr


Sunday, March 28, 2021, 16:10

The wire was heated in the same manner as the last three runs

From 0A to 7A the autoramp was set to 0.5A/min

At 8A the wire started the glow dimmly 

Above 8A, the wire was heated manually at 0.5A until 16A where the step was changed to 1A, 

the temperature was measured with the filament pyrometer every 2 A starting at 10A

At 42 A the step was changed to 0.6A until 42.6A, 4.38V (2020 °C), the wire was kept at that temperature for 90 min

After that time, the current was ramped down at 0.5A/min until ~20A when the current rampping was changed too 1A/min


 

 

  555   Wednesday, September 08, 2021, 12:43 Darwin Ortiz Rosales 44139-8-SKTARGET BOATDoneC Conditioning

 Wednesday, September 08, 2021, 12:36

297 C discs were loaded onto a Ta tube wrapped in 3 Ta heatshields. (10 of which are analysis discs).  They should be the first to be pushed out as they were loaded last.

The discs were loaded upside down to facilitate transfer to final container post conditioning.

a Ta foil disc was placed at the front end and a Ta spring at the back end of the tube.

The weight of the whole system is 254.4 g

Evap 2 was left to reduce pressure overnight.

Target temperature is 2000 C for five hours @ approx 450A

Good vacuum = 3e-2 Torr

Bad vacumm= 5e-2 Torr


 Thursday, September 09, 2021, 08:46IGP1= 7.5 e-07 Torr

Will manually ramp up TGHT to 80 A 


Thursday, September 09, 2021, 09:09 

pressure began to rise at 50A so will leave at 50 A waiting for stabilization.

Current began to shoot up to rapidly, lowered current to 40A.  


Thursday, September 09, 2021, 10:34

At IGP1= 1.3e-4 Torr manually increasing current again 


Thursday, September 09, 2021, 12:52 

IGP1= 8.6e-5 and dropping

TGHT = 60A, 0.87 V

Will begin autoramp to 120A at 1A/min


Thursday, September 09, 2021, 14:06

IGP1= 3.2e-05Torr

TGH T= 120A, 1.9V

Set autoramp to 1A/10s to 200A 


Thursday, September 09, 2021, 14:57

IGP1=  1.5e-05 Torr

TGHT = 200A, 3.4V

Set Autoram to 2A/10s to 450A

OMEGA = 1249 C

 At 258A OMEGA = 1420 C

continue ramp up at 2A/10s to 450

projected 2000 C is 454 A


 

Thursday, September 09, 2021, 16:10 

Tapped up to 470 A and OMEGA 1993C.  Will leave at this current because T may rise.  

 


Thursday, September 09, 2021, 21:21

OMEGA 2011 C

IGP1 = 6.9e-06 Torr

Ramping down @ -1 A/min

 


Thursday, September 09, 2021, 17:27

Temperature kept around 2000 C by reducing current.  It was reduced to 455A and Temperature stabilized .  Time of ramp down will be  21:10 

  556   Tuesday, September 14, 2021, 09:33 Darwin Ortiz Rosales 42218-5LP-IG-LISDoneTaC coating/sintering

Tuesday, September 14, 2021, 09:32

Ta IGLIS tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature = 1900 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 was pumped down over previous night

Good vacuum = 3.00 e-5 Torr

Bad vacuum = 5.00 e-4 Torr

IGP1= 1.12 e-06 Torr

Initiate manual ramp to 50 A @ 1A/min


Tuesday, September 14, 2021, 14:44

 IGP1= 1.25e-06 Torr

TGHT = 50A, 0.58V  TBHT = 49A, 0.56V

Start autoramp to 400 A TGHT and 230A TBHT @ 1A/min


Heated to 1880 C and held for 4 hours.  Log info written down but could not be found in system later.

Coating proceeded without issues.

  557   Wednesday, October 13, 2021, 08:35 Aaron Schmidt   ProblemsTroubleshoot - Pump down issues.

Swapped out the Cu gaskets for SS gaskets in the HS top lines. (x2)

Wednesday, October 13, 2021, 08:35: Roughing.

Wednesday, October 13, 2021, 08:50: Turbo pump on. TP Current 6.06-6.10A.

Wednesday, October 13, 2021, 08:59: TP maxed out at 3-4 KRPM, yet went "Green/On".

Wednesday, October 13, 2021, 09:00: Change FULL to Low setting. Restart. TP Current 6.15A.

Wednesday, October 13, 2021, 09:08: Timed out. Restarted from 5 KRPM. 

Wednesday, October 13, 2021, 09:14: Stalling @ 5 KRPM. Stop TP. Contact vacuum group.


Monday, October 18, 2021, 09:03: Roughing. Reboot TP controller. 

Monday, October 18, 2021, 09:25: Walkthrough soft start w/ vacuum group. TP timed out. Soft start failed. 

Monday, October 18, 2021, 09:31: EVAP 2 vented. TP to be disconnected & removed.

Monday, October 18, 2021, 09:55: TP removed. Quick check, barely spins when spin by hand gently. Replacement or refurbishment needed. 


500 lpm turbo pumps installed. TV551 Varian. SN: 202311 (Slightly active from BL1A - will not cross contaminate. Field only - Tagged) 

Wednesday, October 20, 2021, 11:35: Roughing. 

Wednesday, October 20, 2021, 11:52: TP on. 

Wednesday, October 20, 2021, 11:59: TP at speed. 

Wednesday, October 20, 2021, 12:02: Vacuum @ 6.13e-05T. Open HS waterline.

Wednesday, October 20, 2021, 12:03: Vacuum @ 5.63e-05T & dropping.

Wednesday, October 20, 2021, 12:04: Vacuum @ 5.32e-05T. TGHT PS on. 

  565   Thursday, November 25, 2021, 14:00 Aaron Schmidt    Lower insulator replaced

 The Helicoil had mostly pulled out of the old one.

Thursday, November 25, 2021, 13:58: Insulator replaced. EVAP 2 is ready for use with ISAC targets.

  571   Tuesday, April 12, 2022, 13:41 Aaron Schmidt   MaintenanceNew Flex - line HS installed

Old HS sprang a leak in the copper tubing.  

HS#44378-15

Tuesday, April 12, 2022, 13:35: Roughing. 

Tuesday, April 12, 2022, 13:49: TP1 switched on. 

Tuesday, April 12, 2022, 13:57: TP1 stable (green).

Tuesday, April 12, 2022, 14:10: Vacuum @ 3.71e-05T & dropping.

Tuesday, April 12, 2022, 14:11: HS waterline opened. 

Tuesday, April 12, 2022, 14:12: Vacuum @ 3.32e-05T.

Tuesday, April 12, 2022, 14:22: Vacuum @ 2.19e-05T (Stable).

  575   Tuesday, May 10, 2022, 14:43 Aaron Schmidt   MaintenanceActive TP removed / Swap / Slow start TP

 Tuesday, May 10, 2022, 14:42: TV551 Varian. SN: 202311 (Slightly active from BL1A - will not cross contaminate. Field only - Tagged) was removed as it was meant to be a temporary fix. Replacement (Refurbished) pump is to be installed. (Tomorrow - Use slow start function as per vacuum group) 


Thursday, May 12, 2022, 13:30: Agilent TP & hardware installed.

SN: IT21381010 

Thursday, May 12, 2022, 13:41: Roughing.

Thursday, May 12, 2022, 13:46: Halt. 


Friday, May 13, 2022, 07:05: Roughing. 

Friday, May 13, 2022, 07:18: TP1 on.

Friday, May 13, 2022, 07:23: Up to 14 KRPM. Pause/Halted startup (Whining?). Slow start w/ vacuum group.

Process to perform a TP slow start:

- Hold both top buttons on the controller for about 3 seconds

- Right Yes/No left to continue. 

- Advance to soft start - 20 min. 

- Back to remote start & go.

Friday, May 13, 2022, 08:26: TP1 on w/ slow start.

Friday, May 13, 2022, 08:39: 13 KRPM & climbing.

Friday, May 13, 2022, 09:10: TP at full speed. 38 KRPM. 0.5A 9w. This pump whines, but is operating fine. Likely will switch again when another is available. (It appears to have been dropped, Noted by Edi. Likely when shipped) 

Friday, May 13, 2022, 09:14: TP off. Slow start function off. Back to normal function. 

  579   Wednesday, June 08, 2022, 10:00 Flora Wu boat Donecarbonize PAN 10% discs

Thursday, June 09, 2022, 11:25

Total number of foils: 14 electrospun fiber pellets 

Total weight = 208.3 g

container has 3 Ta heat shields.

Desired temperature at 1800 C

Omega slope set at 0.990 

Good vac = 3.0e-5 Torr,

Bad vac = 5.0e-5 Torr.

Pumping down in progress


 Thursday, June 09, 2022, 11:25

chamber pumped down below 5e-5

initiate auto ramping, 1A/min ----> 100 A


 (see eLog 581)

 

  581   Thursday, June 09, 2022, 19:20 John Wong boat Donecarbonize PAN 10% discs

Flora Wu wrote:

Thursday, June 09, 2022, 11:25

Total number of foils: 14 electrospun fiber pellets 

Total weight = 208.3 g

container has 3 Ta heat shields.

Desired temperature at 1800 C

Omega slope set at 0.990 

Good vac = 3.0e-5 Torr,

Bad vac = 5.0e-5 Torr.

Pumping down in progress


 Thursday, June 09, 2022, 11:25

chamber pumped down below 5e-5

initiate auto ramping, 1A/min ----> 100 A


 

 

 Thursday, June 09, 2022, 19:16

Pressure came down below 10e-5 Torr as TGHT ramped up to 100A.

Continue auto ramping to reach 250A at 1A/min.


 Thursday, June 09, 2022, 22:52

TGHT is hovering around 127A/1.68 V due to erractic pressure, see attachment #1..  Notice the backing line is at atm pressure - I don't recall this happened in the past

Temp is still low to be detected on Omega.  Will leave this overnight.


 Friday, June 10, 2022, 09:07

TGHT has been holding at 250A/3.76V since 2:45am.  Pressure comes down as THGT above 200 A.  Backing line is back down normal.

Temp reading at 1040 C. 

see attachment #2.

Continue to ramp up to 300A, monitoring temp/pressure.


 Friday, June 10, 2022, 10:31

TGHT reached to 300A/4.63V, temp at 1145C.  Pressure at 1.8e-6 and coming down. 

Continue to ramp up to 350A.


 Friday, June 10, 2022, 11:59

TGHT at 350A/5.66V, temp at 1300 C, Pressure at 8.1e-7 Torr, and coming down.

Continue to ramp up to 400A.


Friday, June 10, 2022, 13:19

TGHT reached to 400A/6.73V.  Pressure coming down from 1.04e-6 Torr. 

Temp at 1690.  Will set up manually to reach 1800 C. 


 Friday, June 10, 2022, 13:50

TGHT stepped up to 432A/7.42V.  Pressure coming down from 1.3 e-6 Torr. 

Temp at 1800 C.  See attachment#3 and #4 for the screenshot and temp-current plot.

Dumped striptool data to /usr1/evpr/carbonize_pan10_elog581_a and b.

Will keep at this setting over the weekend, and cooling down will take place on Sunday evening. 

 


 Sunday, June 12, 2022, 22:30

TGHT has been holding at 432A/7.40V since Friday.  Temperature has gone up slightly to 1825. 

See attachment#5 for the overall process. 

Initiated cooling down at -2A/min.

Chamber will be vented on Monday morning.


 

Attachment 1: evap2-screenshot_01.PNG
evap2-screenshot_01.PNG
Attachment 2: evap2-screenshot_02.png
evap2-screenshot_02.png
Attachment 3: evap2-screenshot_3.png
evap2-screenshot_3.png
Attachment 4: temp-current-plot.xlsx
Attachment 5: evap2-screenshot_04.PNG
evap2-screenshot_04.PNG
  591   Wednesday, September 14, 2022, 11:48 Darwin Ortiz Rosales  TARGET BOATDoneGrahite disc conditioning 220907G

Wednesday, September 14, 2022, 9:30

A Ta container tube was wrapped with 3 Ta heatshields.

322 graphite discs were loaded.

one Tantalum cup (modified to fit losely) was inserted on the front end along with a Ta spring.

A Ta spring was also installed on the back end to maintain the discs inside the tube.

The system was left to establish vacuum over night.

Good vacuum set to5e-03Torr

Bad vacuum was set to 5e-2 Torr

Total weight of system including springs = 249.63 g

Two Ta foils were installed on the copper heatshield facing the ends of the container.

The initial weight of the front Ta foil = 22.5 g

The initial weight of the back Ta foil will be determined by difference after cleaning =

OMEGA slope = 0.99

The target will be heated to 2100 C, held there for 10 hours.  The target will be removed, the end Ta foils will be removed to analyses, new Ta end foils will be installed and the Target will be heated to 2100 plus 10 A higher than previous and left at that temperature for 2 hours.


Wednesday, September 14, 2022, 9:47

IGP1= 4.57e--7 Torr

initial Utoramp at 1A/10s to 80A and held at 80 amps until pressure good.


 Wednesday, September 14, 2022, 11:54

Start autoramp at 1A/20s to 120A


 Wednesday, September 14, 2022, 12:22

Autoramp at 1A/20s to 200A

 


Wednesday, September 14, 2022, 12:34

Autoramp increased to 2A/20s when TGHT = 154A


Wednesday, September 14, 2022, 13:46

 Autoramping to 512A as projected current for 2100 C



 Wednesday, September 14, 2022, 14:24

OMEGA = 1945 C @ 512A

Tapped to 540A, 10.5V and OMEGA = 2075. Will leave at this current and see Temperature behaeviour.

After 10 min OMEGA reads 2080C.  Will start cooling at 12:20 am


Wednesday, September 14, 2022, 14:29

OMEGA = 2104C will ramp down slightly to keep 2100C


Wednesday, September 14, 2022, 14:31

OMEGA = 2098 @ 530A, 10.4V


Wednesday, September 14, 2022, 14:33

OMEGA = 2100 @ 410A,9.8V


Wednesday, September 14, 2022, 14:45

OMEGA = 2093 at 500A, 9.75V


Wednesday, September 14, 2022, 15:07

497A, 9.6V, OMEGA 2100

 


Wednesday, September 14, 2022, 22:09

@ approximately 515 pm noticed that OMEGA was reading 1600 C while TGHT was at 497A and 10.0V

Suspect damage to the container and possible damage

Left at the same current.

Just now the OMEGA is reading 2200C at 497A and 9.7V.  Out of precaution, lowered the current to 475A and the volatage is 9.2V

OMEGA now reads 2152 C.  Will leave at this current until 12:30 am when the 10 hour heating will end and will start rampdown at -2A/min


Thursday, September 15, 2022, 00:05

TGHT= 475A, 9.2V

OMEGA= 2126 C

IGP1= 1.33e-6 Torr

lowered current to 470A, 9.1 V, IGP1= 1.3e-6 Torr, OMEGA stabilized at 2120C


Thursday, September 15, 2022, 00:09

IGP1= 1.3e-6 Torr

will increase 10A to see pressure response. OMEGA= 2130C

Increase in IGP1 to 1.4e-6 Torr observed but immediately started to trend down


Thursday, September 15, 2022, 00:16

IGP1= 1.36e-6 Torr

OMEGA = 2131A

TGHT = 480 A


Thursday, September 15, 2022, 00:18

Start ramp down at -2A/min


Thursday, September 15, 2022, 09:45

IGP1=4.35e-07 Torr

TGHT turned off

Starting dismounting of target tube


Thursday, September 22, 2022, 07:04

Container tube was crystalized and was easily cut with a small pair of nail scissors.  All but 18 discs were transferred to a new container.  WO# 44691-3

  593   Thursday, September 29, 2022, 10:02 Darwin Ortiz Rosales 44139-3TARGET BOATDone220926-Graphite conditioning in target tube

Thursday, September 29, 2022, 09:57

A Ta container tube was wrapped with 3 Ta heatshields.

338 graphite discs were loaded.

one Tantalum cup (modified to fit losely) was inserted on the front end along with a Ta spring.

on the backside there is no spring but four discs glued together with PVA

The system was left to establish vacuum over night.

Good vacuum set to5e-04Torr

Bad vacuum was set to 5e-2 Torr

Total weight of system including springs = 249.07 g

OMEGA slope = 0.99

The target will be heated to 2100 C, held there for 10 hours.  The target Temperature vs Power will be tabulated and the current required to reach 2100 will  be extrapolated to avoid using OMEGA at higher temperatures.

a)  The target will be removed, weighed and inspected

b) If the target boat is still good, run again at 10A higher than previous for 2 hours.

c) The target will be removed, weighed and inspected

d) i) If the weight is the same or negligible, experiment ends

  ii) if the weight has decreased and target still intact, repeat from step b and document all measurements and settings


 Thursday, September 29, 2022, 10:04

IGP1= 1.4e-04 Torr

TGHT= 80.0 A, 1.0V

Will allow pressure to drop and then continue heating


Thursday, September 29, 2022, 10:20

IGP1= 7.9e-05 Torr pressure on downward trend

Start heating at 2A/min to 200A


The target started dropping in temperature as current increased.  Suspected OMEGA issue.

Started cooling at -2A/min

Will continue next week.


Monday, October 03, 2022, 11:05

Upon inspection, the window though which the OMEGA laser travels was coated with dark precipitate (mostly a spot in the direct path of the laser).

Cleaned the window and started pumpdown.


Monday, October 03, 2022, 12:57

start heating @2A/20s = 6A/min because the target had previously been heated past additive evaporation point.

IGP1= 3.8e-06 Torr


Monday, October 03, 2022, 18:41

Will heat to 500A and leave for 10 hours.  The regression shows too high current to reach 2100.  Not reasonable.  So will work with 500A as a baseline.

 

 

 


Tuesday, October 04, 2022, 06:52

Temperature @500 A read 1742C

maintained for 10 hours

start rampdown at -2A/min 

OMEGA currently 1099C

Current = 500 A

Voltage =9.9 V

IGP1= 5.9e-7 Torr


Tuesday, October 04, 2022, 21:32

Quartz window was completely covered with graphite like dust.  final weight after heating = 244.57 g (a couple of discs came loose and they were weighed separately and not included in the next heating).

weighted target and added one extra heatshield because it looked like a lot of heat was escaping.  Will treat at 500A again for 2 hours.  The extra heat-shield should provide hotter environment.

new initial weight = 254.24 g (don't have a balance with greater precision .


Wednesday, October 05, 2022, 07:42

IGP1= 3.8e-07 Torr

ramping to 280A @ 3A/min


Wednesday, October 05, 2022, 11:40

ramping to 350 @ 3A/min

Then ramp to 500A

500A at 12:50


Wednesday, October 05, 2022, 15:52

ramping down at -2A/min


Thursday, October 06, 2022, 09:27

IGP1= 1.8e-07 Torr

Will dismount and weigh, then decide how to proceed

 

according to second regression, second heating was ~2000 C.  OMEGA not reliable after 1700 C in this case. 


Thursday, October 06, 2022, 12:34

The final weight after the second heating was = 254.19 g

reinstalled target and cleaned quartz window. 

will heat up to 510 A


Friday, October 07, 2022, 07:46

IGP1=  3.0 e-07 Torr

ramp at 2A/min to 500A.  will pause to take data points for regression.


Friday, October 07, 2022, 13:05

Start rampdown after two hours at 500A, 10.3V

-2A/min

 

  606   Friday, December 02, 2022, 09:50 Darwin Ortiz Rosales 45220-12TARGET BOATDoneGrahite disc conditioning 221130-Graphite

Friday, December 02, 2022, 09:46

297 graphite discs packed into a Ta tube wrapped in four heatshields.

Good vacuum 5.0e-04 Torr

Bad vacuum 5.0 e-02 Torr

Will be conditioned @ 2000 C for 5 hours and then for one hour at 10A greater than final current.  Final current will be calculated from

regression.

 IGP1= 5.7 e-07 Torr

ramping to 40A @ 2A/min TGHT


Friday, December 02, 2022, 20:59

Was ramped to 320A but the window must be coated because Temperature readings are drastically off. Will cool down and repeat on Monday after cleaning window.  Will ramp down at -2A/min

OMEGA= 1360 C, expect much higher.


Tuesday, December 06, 2022, 10:58

ramp started at 4A/min .  Initial pressure was 2.6 e-07 Torr


Tuesday, December 06, 2022, 12:45

OMEGA readings low (1290 @ 331A, 5.6V )

Will tap up until pressure bump observed.


Tuesday, December 06, 2022, 13:04

 Pressure bump observed around 440 A, 7.9 V

IGP1= 8.4 e-06 Torr. 

Current stopped and will keep at this current for 10 hours (11 pm rampdown)


Tuesday, December 06, 2022, 13:24

Ramped to 500A, Will leave at 500A for the rest of the conditioning.

 


Tuesday, December 06, 2022, 23:05

Starting rampdown at -2A/min

IGP1= 4.9e-07 Torr

TGHT= 500A, 9.3V

 


Wednesday, December 07, 2022, 09:43

Dismounting today.

IGP1 final = 9.6e-08 Torr


Wednesday, December 07, 2022, 13:29

Reinstalled in the evaporator.  Window was not shaded.  Will try heating to 500A once more.

ramp at 6A/min

  634   Wednesday, May 24, 2023, 15:23 Darwin Ortiz Rosales 44139-4LP TUBEDoneGraphite inside insert Experiment 1

 

Wednesday, May 24, 2023, 15:22

A Ta container tube was wrapped with 4 Ta heatshields.  Note final container is 45220-11

219 graphite discs were loaded.

a TaC coated Ta spring at the front end.

The system was left to establish vacuum over previous night.

Good vacuum set to5e-04Torr

Bad vacuum was set to 5e-2 Torr

Total weight of system including spring= 250.1 g

OMEGA slope = 0.99

The target will be heated to 2000 C, held there for 10 hours. 

Initial ramp at 1A/min to 200A

Then ramp at 0.5A/min while taking temperature readings periodically unti l250A.

At 250 A will let pressure stabilize and then ramp at 1A/min to 2000C or 450A.  

Will hold at target Temperature or Current for 10 hours before starting ramp-down.


 Wednesday, May 24, 2023, 15:50

Currently heating at 0.5A/min to250A.  Taking temperature/current measurements

IGP1= 1.06e-06 Torr


Wednesday, May 24, 2023, 18:28

heating at 1A/min to 275A to collect more temperature data


Wednesday, May 24, 2023, 19:22

Slight offset between set and RD current observed. 

Ramping at 1A/min to 440A according to the regression below

Should be around 2000 C.


Wednesday, May 24, 2023, 20:22

Currently at 339 A, 4.8V

OMEGA = 1614 C, IGP1= 2.04e-06 Torr

Will ramp up at 2A/min to 450A as new data point suggests


Wednesday, May 24, 2023, 21:05

1730 C   411.0 A 6.9 V

heating curve has new slope suggesting 500A as minimum to reach 2000 C

Increasing ramp to 1A/10s to reach 450A


Wednesday, May 24, 2023, 21:17

TGHT

1804 C   441.0 A 7.4 V

IGP1= 3.9e-06 Torr

Continue ramping to 480A


Wednesday, May 24, 2023, 22:11

Offset between setpoint of current and readback.  readback 10A below. 

1941 C   480.0 A 8.5V

Will keep at this setting until 7:30 am tomorrow then start ramp down @-2A/min


Thursday, May 25, 2023, 07:25

OMEGA=1912C, IGP1 =1.29e-06 Torr, TGHT = 480A, 9.0V

begin ramp down at -2A/min


Thursday, May 25, 2023, 09:52

Some odd current readback behaeviour noticed.  Have contacted Gelo from controls.  He will look at it next week.  Discrepancy between read back and set point and drop in read back currrent. See picture

 

 

Attachment 1: Screenshot_Graphite_insert_Exp1.png
Screenshot_Graphite_insert_Exp1.png
  635   Monday, June 05, 2023, 14:52 Aaron Schmidt    Swapped turbo pumps.

 Previous TP would only spin up to 4KRPM. New TP installed.

Monday, June 05, 2023, 14:50: Roughing. 

Monday, June 05, 2023, 15:10: Controller reset. TP on. 

  668   Wednesday, August 07, 2024, 15:37 Aaron Schmidt    Turning on EVAP2's turbo pump

Wednesday, August 07, 2024, 15:36: Roughing. Had initially been roughed & TP started w/ Marla CS, however it timed out. Restarting.

Wednesday, August 07, 2024, 15:37: TP on.

Wednesday, August 07, 2024, 15:46: Tripped at 4 KRPM. Restarted. Up to 5 KRPM.

Failed to start.


Thursday, August 08, 2024, 10:00: TP started. 

Thursday, August 08, 2024, 10:12: TP Tripped but nearly spun up. Reset & Restarted. TP Green / on.

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