|
ID |
Date |
Author |
Target Material |
Target Oven W.O# |
Source |
Status |
Subject |
|
299
|
Tuesday, May 24, 2016, 11:18 |
John Wong | SiC | | TARGET BOAT | In progress | Heat-treatment: Beta-SiC (1um) target discs |
Laura Lambert wrote: |
John Wong wrote: |
The purpose of this experiment is to determined the limiting operating temperature for Beta-SiC. To do so, samples will be heated in sequence to observe any volatile Si coated on the window. The coating is observed above 1400C for the conventional SiC (mixuture of alpha and beta) and this coating leads to HV shorting problem.
Thursday, May 19, 2016, 14:26
Beta-SiC (size ~1um) slurry was prepared and casted on a graphite foil.
Discs are cut into D-shape
Average thickness (including graphite foil) = 0.349mm
Graphite foil = 0.13mm
Actual SiC thickness = 0.219mm (close to normal SiC thickness)
Samples are loaded into a target boat.
Total discs = 120
Total mass = 14.3507g
Thursday, May 19, 2016, 14:32
Omega slope set to = 1.04
Heat-treatment #1: 1400C
Thursday, May 19, 2016, 17:04
TGHT ramping up to 250A at 0.5A/min
|
Friday, May 20, 2016, 08:53
IGP1 = 9.2e-6 Torr.
Increasing ramping rate to 1.0A/min up to 250A
Friday, May 20, 2016, 09:17
IGP1 = 2.1e-5 Torr
TGHT = 215A, 3.1V
OMEGA = 1035C
Stopping auto-ramp and tapping up manually...
Friday, May 20, 2016, 12:26
OMEGA slope changed to 1.04
OMEGA reached ~1430C and kept there for ~1hr.
no change. no coating on window observed
tapped up manually to OMEGA =1500C
TGHT = 350A, 5.8V
Friday, May 20, 2016, 14:17
Not much change to window.
Might be beginning of light dusting, hard to tell.
Will be better observed after longer period of time at 1500C
Will remain at 1500C over weekend.
|
Tuesday, May 24, 2016, 11:15
Sample has been heated over the long weekend. Temp dropped to 1400C. TGHT at 350A/5.78V. Vac at 1.5e-7 Torr.
It is hard to tell if there is any coating on the window. Will increase temperature to 1800C
Tuesday, May 24, 2016, 11:43
Temp at 1620C. TGHT at 440A/7.7V.
At this temperature, the coating would have been seen for the conventional SiC target material. But, no much of change on the window since the TGHT was tapped up from 1400C.
Continue to increase TGHT to reach 1800C
Tuesday, May 24, 2016, 11:58
Temp at 1680C/TGHT 470A/8.4C - a very light film on the window was observed. Not sure if this film was left from previous processes; it is just that the target container is getting very bright and hard to see.
Tuesday, May 24, 2016, 12:15
TGHT at 510A/9.16V - Observed coating on window. Omega got interfered, therefore temp is unknown. But it was read at ~1720C before the window was getting coated and temp started to dropped.
Will leave at this stage for now...
Tuesday, May 24, 2016, 16:57
Window is fully coated. Based on the heating curve, at 500A, the temp should be at ~1900C (wrapped with a layer of heat shield). Temperature reader dropped to1340C due to the coating interference.
Cooling down TGHT at 2A/min. And will exam the materials tomorrow...
|
|
298
|
Friday, May 20, 2016, 08:54 |
Laura Lambert | SiC | | TARGET BOAT | In progress | Heat-treatment: Beta-SiC (1um) target discs |
John Wong wrote: |
The purpose of this experiment is to determined the limiting operating temperature for Beta-SiC. To do so, samples will be heated in sequence to observe any volatile Si coated on the window. The coating is observed above 1400C for the conventional SiC (mixuture of alpha and beta) and this coating leads to HV shorting problem.
Thursday, May 19, 2016, 14:26
Beta-SiC (size ~1um) slurry was prepared and casted on a graphite foil.
Discs are cut into D-shape
Average thickness (including graphite foil) = 0.349mm
Graphite foil = 0.13mm
Actual SiC thickness = 0.219mm (close to normal SiC thickness)
Samples are loaded into a target boat.
Total discs = 120
Total mass = 14.3507g
Thursday, May 19, 2016, 14:32
Omega slope set to = 1.04
Heat-treatment #1: 1400C
Thursday, May 19, 2016, 17:04
TGHT ramping up to 250A at 0.5A/min
|
Friday, May 20, 2016, 08:53
IGP1 = 9.2e-6 Torr.
Increasing ramping rate to 1.0A/min up to 250A
Friday, May 20, 2016, 09:17
IGP1 = 2.1e-5 Torr
TGHT = 215A, 3.1V
OMEGA = 1035C
Stopping auto-ramp and tapping up manually...
Friday, May 20, 2016, 12:26
OMEGA slope changed to 1.04
OMEGA reached ~1430C and kept there for ~1hr.
no change. no coating on window observed
tapped up manually to OMEGA =1500C
TGHT = 350A, 5.8V
Friday, May 20, 2016, 14:17
Not much change to window.
Might be beginning of light dusting, hard to tell.
Will be better observed after longer period of time at 1500C
Will remain at 1500C over weekend.
|
|
297
|
Thursday, May 19, 2016, 14:38 |
John Wong | SiC | | TARGET BOAT | In progress | Heat-treatment: Beta-SiC (1um) target discs | The purpose of this experiment is to determined the limiting operating temperature for Beta-SiC. To do so, samples will be heated in sequence to observe any volatile Si coated on the window. The coating is observed above 1400C for the conventional SiC (mixuture of alpha and beta) and this coating leads to HV shorting problem.
Thursday, May 19, 2016, 14:26
Beta-SiC (size ~1um) slurry was prepared and casted on a graphite foil.
Discs are cut into D-shape
Average thickness (including graphite foil) = 0.349mm
Graphite foil = 0.13mm
Actual SiC thickness = 0.219mm (close to normal SiC thickness)
Samples are loaded into a target boat.
Total discs = 120
Total mass = 14.3507g
Thursday, May 19, 2016, 14:32
Omega slope set to = 1.04
Heat-treatment #1: 1400C
Thursday, May 19, 2016, 17:04
TGHT ramping up to 250A at 0.5A/min
|
|
296
|
Wednesday, May 11, 2016, 17:24 |
John Wong | np-SiC | | TARGET BOAT | Done | Temperature Treament of Nanofiber SiC/PAN | Wednesday, May 11, 2016, 17:15
Nanofiber SiC (~50nm grain size)/PAN was prepared at UBC.
SiC 0.50g, DMF 9.0g, PAN 1.0g, tiny bit of SDS.
The fiber mat was stabilized in air at 250C and then cut into discs, initial mass = 0.1072g
Discs were then bounded with PVA on 9 pieces of rounded graphite foil (green mass gained to 0.6031g)
The stack of naofiber SiC/PAN was loaded on to Ta boated (coated) and wrapped with Ta heat shield.
Chamber is currently being pumped down.
Friday, May 13, 2016, 15:00
TGHT at 390A/6.966V. Temp measured at 1615C.
Will keep at that temperature for a few days.
Monday, May 16, 2016, 15:44
Sample has been heated at ~1600C for 4 days. TGHT at 400A/7.02V.
Cooling down at 2A/min
Tuesday, May 17, 2016, 11:18
Chamber vented. Inspecting samples.
|
|
295
|
Tuesday, May 10, 2016, 11:57 |
Laura Lambert | | 40282-3 | TARGET BOAT | Done | Conditioning Nb samples for Tobias |
John Wong wrote: |
Laura Lambert wrote: |
Wednesday, May 04, 2016, 13:28
Target boat has a layer of niobium foil on the bottom of the boat.
A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos
Larger niobium samples are placed in the slots, holding in place, to avoid warping; smaller niobium sample sitting inside the boat by itself.
Smaller sample closest to OMEGA IR reading [right side]
Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.
Loaded into evap2 yesterday.
Vacuum pump bearings gone - pump replaced this morning by vacuum group.
Pumping down now...
Friday, May 06, 2016, 13:36
HS water valves opened, no leaks detected.
Tapped up manually to 35A.
IGP1 = 2.4e-7 Torr
Setting auto-ramp rate at 0.2A/min to 250A over the weekend.
Will tap up manually monday to final desired temperature of 1400C.
Monday, May 09, 2016, 09:38
OMEGA = 1128C
IGP1 = 1.3e-7 Torr
TGHT = 250A, 3.7V
Tapping up manually to 1400C...
Monday, May 09, 2016, 14:05
Evap2 has reached ~1405C
TGHT = 341A, 5.34V
IGP1 = 1.9e-7 Torr
Will remain at max setpoints for min 4hrs then initiate cool down.
|
Monday, May 09, 2016, 18:18
TGHT at 341A/5.34V for over 4 hours. Vac stables at 1.78e-7 Torr.
Cooling down at 2A/min
|
Tuesday, May 10, 2016, 08:45
Vented in air and opened up this morning.
Samples look good!
|
|
294
|
Monday, May 09, 2016, 18:19 |
John Wong | | 40282-3 | TARGET BOAT | In progress | Conditioning Nb samples for Tobias |
Laura Lambert wrote: |
Wednesday, May 04, 2016, 13:28
Target boat has a layer of niobium foil on the bottom of the boat.
A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos
Larger niobium samples are placed in the slots, holding in place, to avoid warping; smaller niobium sample sitting inside the boat by itself.
Smaller sample closest to OMEGA IR reading [right side]
Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.
Loaded into evap2 yesterday.
Vacuum pump bearings gone - pump replaced this morning by vacuum group.
Pumping down now...
Friday, May 06, 2016, 13:36
HS water valves opened, no leaks detected.
Tapped up manually to 35A.
IGP1 = 2.4e-7 Torr
Setting auto-ramp rate at 0.2A/min to 250A over the weekend.
Will tap up manually monday to final desired temperature of 1400C.
Monday, May 09, 2016, 09:38
OMEGA = 1128C
IGP1 = 1.3e-7 Torr
TGHT = 250A, 3.7V
Tapping up manually to 1400C...
Monday, May 09, 2016, 14:05
Evap2 has reached ~1405C
TGHT = 341A, 5.34V
IGP1 = 1.9e-7 Torr
Will remain at max setpoints for min 4hrs then initiate cool down.
|
Monday, May 09, 2016, 18:18
TGHT at 341A/5.34V for over 4 hours. Vac stables at 1.78e-7 Torr.
Cooling down at 2A/min
|
|
293
|
Wednesday, May 04, 2016, 13:45 |
Laura Lambert | | 40282-3 | TARGET BOAT | In progress | Conditioning Nb samples for Tobias | Wednesday, May 04, 2016, 13:28
Target boat has a layer of niobium foil on the bottom of the boat.
A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos
Larger niobium samples are placed in the slots, holding in place, to avoid warping; smaller niobium sample sitting inside the boat by itself.
Smaller sample closest to OMEGA IR reading [right side]
Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.
Loaded into evap2 yesterday.
Vacuum pump bearings gone - pump replaced this morning by vacuum group.
Pumping down now...
Friday, May 06, 2016, 13:36
HS water valves opened, no leaks detected.
Tapped up manually to 35A.
IGP1 = 2.4e-7 Torr
Setting auto-ramp rate at 0.2A/min to 250A over the weekend.
Will tap up manually monday to final desired temperature of 1400C.
Monday, May 09, 2016, 09:38
OMEGA = 1128C
IGP1 = 1.3e-7 Torr
TGHT = 250A, 3.7V
Tapping up manually to 1400C...
Monday, May 09, 2016, 14:05
Evap2 has reached ~1405C
TGHT = 341A, 5.34V
IGP1 = 1.9e-7 Torr
Will remain at max setpoints for min 4hrs then initiate cool down.
|
Attachment 1: Nb_samples_in_boat_(2).jpg
|
|
|
292
|
Tuesday, May 03, 2016, 14:44 |
Laura Lambert | | | | | VACUUM PUMP REPLACEMENT | Tuesday, May 03, 2016, 14:29
Turned vacuum pump on this morning, sounded awful: loud grinding bad noises.
Called vacuum group, will replace pump tomorrow morning.
Sounds like materials coming out from all the out-gassing during sintering processes has ruined the bearings.
|
|
291
|
Tuesday, April 26, 2016, 13:50 |
Laura Lambert | Empty | 40860-2 | LP-IG-LIS | Done | sintering TaC coating on UCx#16 container | Tuesday, April 26, 2016, 13:32
Container coated with TaC using 'flushing technique'.
Wrapped with 3 x Ta heat shields, incl center block - new method of each layer being one long single Ta foil covering entire container incl center block
Currently pumping down in evap2
Wednesday, April 27, 2016, 10:25
IGP1 = 2.6e-7 Torr.
HS water valves opened, no leaks detected.
Tapped up manually to 35A.
Waited ~35min
Vacuum stable, IGP1 = 6.7e-7 Torr
Initiated auto-ramp at 0.2A/min for the TGHT with a final setpoint of 400A
Final desired temperature = 1900C
Thursday, April 28, 2016, 14:41
Previously TBHT not on when sintering IGLIS container [since no ionizer tube] - John decided will turn on for this round
Tapped up TBHT manually to 140A, 1.69V
IGP1 = 4.5e-7 Torr
OMEGA = 1635C
TGHT = 382A, 5.8V
Initiating auto-ramp of TBHT at 0.1A/min with a final setpoint of 230A.
Friday, April 29, 2016, 08:40
IGP1 = 2.22-7 Torr
TGHT = 400A, 6.1V
TBHT = 233A, 2.9V
OMEGA = 1719C
Tapping up manually to OMEGA = 1900C
Friday, April 29, 2016, 15:22
IGP1 = 3.0e-7 Torr
TGHT = 460A, 7.52V
TBHT =230A, 2.93V
OMEGA = 1904C
Target container has remained at max temperature setpoint of 1900C for 4.5hrs.
Initiating auto cool for TGHT and TBHT at 2.0A/min and 1.0A/min respectively.
Monday, May 02, 2016, 08:35
Vented in air and opened up this morning.
Container looks good.
See attached photos.
|
Attachment 1: TaC_coating_sintered1.jpg
|
|
Attachment 2: TaC_coating_sintered2.jpg
|
|
Attachment 3: TaC_coating_sintered3.jpg
|
|
|
290
|
Tuesday, April 19, 2016, 09:28 |
Anders Mjos | Ta | 41790-1 | LP-SIS | Done | Ta#47 LP-SIS (with new center block) conditioning |
John Wong wrote: |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Anders Mjos wrote: |
Laura Lambert wrote: |
Aurelia Laxdal wrote: |
Started Ta#47 heating at Evap2 using the autoramp program. The TGHT current is setup to go to 300A (for now) and the TBHT to 230A (final value).
|
Monday, March 14, 2016, 09:20
One thermocouple was not welded on correctly and is not working.
Cooling evap2 back down, to remove target and re-weld thermocouple.
Once thermocouple replaced, will ramp back up and continue with tests/ conditioning of target.
|
Monday, March 14, 2016, 13:12: Stopped turbo pump
|
After EVAP2 was vented the thermocouple problem was fixed: it was the wire at on connector inside the box not making proper contact. The lid of the heat shield was also replaced since the one initially mounted had no holes, so one couldn't see the center block. Restarted pumping down at 4:30pm. Just started again the autoramp program: TGHT set to 300A (for the time being) and TBHT to 230A. Temperature measurements will resume tomorrow morning.
|
Raised the TGHT at 620A. The TBHT was already set at 230A. The temperature is at 1902 deg C. As per John's instructions the target will condition at these setpoints over the week-end.
|
Today, lowered the TGHT from 620A (at 1894 deg C) to 300A. TBHT is still at 230A.
|
Cooling down the target.
|
Thursday, March 24, 2016, 11:29
Target was removed from the Evaporator.
The thermocouples broke off.
Need to insert Re foil prior to installing
|
Tuesday, April 19, 2016, 09:28: Uploaded thermoucouple data. |
Attachment 1: 2016-03-11_Evaporator_2.4ch
|
°C Date Time T1 - C T2 - C T3 - C T4 - C
1 2016/03/11 14:25:25 21.1 24.7
2 2016/03/11 14:25:55 25.0 24.8
3 2016/03/11 14:26:25 21.6 - - -
4 2016/03/11 14:26:55 21.0 - - -
5 2016/03/11 14:27:25 21.3 - - -
6 2016/03/11 14:27:55 21.1 - - -
7 2016/03/11 14:28:25 21.1 - - -
8 2016/03/11 14:28:55 21.0 - - -
9 2016/03/11 14:29:25 21.1 - - -
10 2016/03/11 14:29:55 21.1 - - -
11 2016/03/11 14:30:25 21.1 - - -
12 2016/03/11 14:30:55 21.1 - - -
13 2016/03/11 14:31:25 21.1 - - -
14 2016/03/11 14:31:55 21.1 - - -
15 2016/03/11 14:32:25 21.1 - - -
16 2016/03/11 14:32:55 21.1 - - -
17 2016/03/11 14:33:25 20.0 - - -
18 2016/03/11 14:33:55 20.2 - - -
19 2016/03/11 14:34:25 20.8 - - -
20 2016/03/11 14:34:55 20.8 - - -
21 2016/03/11 14:35:25 21.1 - - -
22 2016/03/11 14:35:55 19.7 - - -
23 2016/03/11 14:36:25 20.8 - - -
24 2016/03/11 14:36:55 20.7 - - -
25 2016/03/11 14:37:25 21.3 - - -
26 2016/03/11 14:37:55 21.1 - - -
27 2016/03/11 14:38:25 21.2 - - -
28 2016/03/11 14:38:55 20.2 - - -
29 2016/03/11 14:39:25 20.7 - - -
30 2016/03/11 14:39:55 20.8 - - -
31 2016/03/11 14:40:25 21.3 - - -
32 2016/03/11 14:40:55 19.7 - - -
33 2016/03/11 14:41:25 20.8 - - -
34 2016/03/11 14:41:55 20.8 - - -
35 2016/03/11 14:42:25 20.8 - - -
36 2016/03/11 14:42:55 20.8 - - -
37 2016/03/11 14:43:25 20.8 - - -
38 2016/03/11 14:43:55 20.8 - - -
39 2016/03/11 14:44:25 20.8 - - -
40 2016/03/11 14:44:55 20.2 - - -
41 2016/03/11 14:45:25 20.8 - - -
42 2016/03/11 14:45:55 21.3 - - -
43 2016/03/11 14:46:25 20.8 - - -
44 2016/03/11 14:46:55 20.4 - - -
45 2016/03/11 14:47:25 20.8 - - -
46 2016/03/11 14:47:55 20.8 - - -
47 2016/03/11 14:48:25 20.8 - - -
48 2016/03/11 14:48:55 20.3 - - -
49 2016/03/11 14:49:25 20.4 - - -
50 2016/03/11 14:49:55 19.9 - - -
51 2016/03/11 14:50:25 20.4 - - -
52 2016/03/11 14:50:55 20.8 - - -
53 2016/03/11 14:51:25 20.5 - - -
54 2016/03/11 14:51:55 20.4 - - -
55 2016/03/11 14:52:25 20.5 - - -
56 2016/03/11 14:52:55 20.4 - - -
57 2016/03/11 14:53:25 20.8 - - -
58 2016/03/11 14:53:55 20.8 - - -
59 2016/03/11 14:54:25 20.3 - - -
60 2016/03/11 14:54:55 19.8 - - -
61 2016/03/11 14:55:25 20.3 - - -
62 2016/03/11 14:55:55 20.4 - - -
63 2016/03/11 14:56:25 21.3 - - -
64 2016/03/11 14:56:55 21.3 - - -
65 2016/03/11 14:57:25 20.5 - - -
66 2016/03/11 14:57:55 21.3 - - -
67 2016/03/11 14:58:25 21.3 - - -
68 2016/03/11 14:58:55 20.4 - - -
69 2016/03/11 14:59:25 20.0 - - -
70 2016/03/11 14:59:55 20.4 - - -
71 2016/03/11 15:00:25 19.8 - - -
72 2016/03/11 15:00:55 19.8 - - -
73 2016/03/11 15:01:25 19.8 - - -
74 2016/03/11 15:01:55 20.4 - - -
75 2016/03/11 15:02:25 20.4 - - -
76 2016/03/11 15:02:55 20.3 - - -
77 2016/03/11 15:03:25 21.2 - - -
78 2016/03/11 15:03:55 20.0 - - -
79 2016/03/11 15:04:25 21.0 - - -
80 2016/03/11 15:04:55 20.5 - - -
81 2016/03/11 15:05:25 20.0 - - -
82 2016/03/11 15:05:55 20.5 - - -
83 2016/03/11 15:06:25 20.5 - - -
84 2016/03/11 15:06:55 21.4 - - -
85 2016/03/11 15:07:25 21.4 - - -
86 2016/03/11 15:07:55 20.5 - - -
87 2016/03/11 15:08:25 20.5 - - -
88 2016/03/11 15:08:55 20.5 - - -
89 2016/03/11 15:09:25 21.4 - - -
90 2016/03/11 15:09:55 20.5 - - -
91 2016/03/11 15:10:25 21.0 - - -
92 2016/03/11 15:10:55 21.0 - - -
93 2016/03/11 15:11:25 20.0 - - -
94 2016/03/11 15:11:55 21.0 - - -
95 2016/03/11 15:12:25 21.0 - - -
96 2016/03/11 15:12:55 20.5 - - -
97 2016/03/11 15:13:25 21.0 - - -
98 2016/03/11 15:13:55 20.5 - - -
99 2016/03/11 15:14:25 20.5 - - -
100 2016/03/11 15:14:55 20.5 - - -
101 2016/03/11 15:15:25 20.0 - - -
102 2016/03/11 15:15:55 21.0 - - -
103 2016/03/11 15:16:25 21.0 - - -
104 2016/03/11 15:16:55 19.9 - - -
105 2016/03/11 15:17:25 21.0 - - -
106 2016/03/11 15:17:55 21.4 - - -
107 2016/03/11 15:18:25 20.8 - - -
108 2016/03/11 15:18:55 20.5 - - -
109 2016/03/11 15:19:25 21.0 - - -
110 2016/03/11 15:19:55 20.0 - - -
111 2016/03/11 15:20:25 19.9 - - -
112 2016/03/11 15:20:55 21.4 - - -
113 2016/03/11 15:21:25 20.8 - - -
114 2016/03/11 15:21:55 20.8 - - -
115 2016/03/11 15:22:25 20.8 - - -
116 2016/03/11 15:22:55 20.3 - - -
117 2016/03/11 15:23:25 21.3 - - -
118 2016/03/11 15:23:55 20.8 - - -
119 2016/03/11 15:24:25 20.8 - - -
120 2016/03/11 15:24:55 20.4 - - -
121 2016/03/11 15:25:25 21.0 - - -
122 2016/03/11 15:25:55 20.5 - - -
123 2016/03/11 15:26:25 20.4 - - -
124 2016/03/11 15:26:55 20.8 - - -
125 2016/03/11 15:27:25 21.3 - - -
126 2016/03/11 15:27:55 21.3 - - -
127 2016/03/11 15:28:25 20.8 - - -
128 2016/03/11 15:28:55 21.3 - - -
129 2016/03/11 15:29:25 21.3 - - -
130 2016/03/11 15:29:55 20.7 - - -
131 2016/03/11 15:30:25 21.3 - - -
132 2016/03/11 15:30:55 21.3 - - -
133 2016/03/11 15:31:25 20.8 - - -
134 2016/03/11 15:31:55 20.7 - - -
135 2016/03/11 15:32:25 21.3 - - -
136 2016/03/11 15:32:55 21.3 - - -
137 2016/03/11 15:33:25 20.8 - - -
138 2016/03/11 15:33:55 20.8 - - -
139 2016/03/11 15:34:25 20.8 - - -
140 2016/03/11 15:34:55 19.9 - - -
141 2016/03/11 15:35:25 21.3 - - -
142 2016/03/11 15:35:55 20.8 - - -
143 2016/03/11 15:36:25 20.8 - - -
144 2016/03/11 15:36:55 21.3 - - -
145 2016/03/11 15:37:25 20.4 - - -
146 2016/03/11 15:37:55 20.2 - - -
147 2016/03/11 15:38:25 21.3 - - -
148 2016/03/11 15:38:55 20.7 - - -
149 2016/03/11 15:39:25 20.8 - - -
150 2016/03/11 15:39:55 20.8 - - -
151 2016/03/11 15:40:25 20.7 - - -
152 2016/03/11 15:40:55 20.3 - - -
153 2016/03/11 15:41:25 20.8 - - -
154 2016/03/11 15:41:55 19.8 - - -
155 2016/03/11 15:42:25 19.7 - - -
156 2016/03/11 15:42:55 21.2 - - -
157 2016/03/11 15:43:25 20.7 - - -
158 2016/03/11 15:43:55 20.2 - - -
159 2016/03/11 15:44:25 20.8 - - -
160 2016/03/11 15:44:55 20.7 - - -
161 2016/03/11 15:45:25 20.8 - - -
162 2016/03/11 15:45:55 21.3 - - -
163 2016/03/11 15:46:25 20.8 - - -
164 2016/03/11 15:46:55 20.2 - - -
165 2016/03/11 15:47:25 21.3 - - -
166 2016/03/11 15:47:55 20.8 - - -
167 2016/03/11 15:48:25 21.3 - - -
168 2016/03/11 15:48:55 21.3 - - -
169 2016/03/11 15:49:25 21.3 - - -
170 2016/03/11 15:49:55 20.8 - - -
171 2016/03/11 15:50:25 19.8 - - -
172 2016/03/11 15:50:55 20.8 - - -
173 2016/03/11 15:51:25 21.3 - - -
174 2016/03/11 15:51:55 19.7 - - -
175 2016/03/11 15:52:25 20.8 - - -
176 2016/03/11 15:52:55 20.8 - - -
177 2016/03/11 15:53:25 20.4 - - -
178 2016/03/11 15:53:55 20.8 - - -
179 2016/03/11 15:54:25 21.3 - - -
180 2016/03/11 15:54:55 21.3 - - -
181 2016/03/11 15:55:25 20.8 - - -
182 2016/03/11 15:55:55 20.8 - - -
183 2016/03/11 15:56:25 20.4 - - -
184 2016/03/11 15:56:55 19.8 - - -
185 2016/03/11 15:57:25 21.3 - - -
186 2016/03/11 15:57:55 21.3 - - -
187 2016/03/11 15:58:25 21.3 - - -
188 2016/03/11 15:58:55 20.4 - - -
189 2016/03/11 15:59:25 21.3 - - -
190 2016/03/11 15:59:55 20.8 - - -
191 2016/03/11 16:00:25 20.8 - - -
192 2016/03/11 16:00:55 19.7 - - -
193 2016/03/11 16:01:25 20.3 - - -
194 2016/03/11 16:01:55 21.3 - - -
195 2016/03/11 16:02:25 20.8 - - -
196 2016/03/11 16:02:55 21.3 - - -
197 2016/03/11 16:03:25 21.3 - - -
198 2016/03/11 16:03:55 20.8 - - -
199 2016/03/11 16:04:25 20.2 - - -
200 2016/03/11 16:04:55 21.3 - - -
201 2016/03/11 16:05:25 20.2 - - -
202 2016/03/11 16:05:55 20.2 - - -
203 2016/03/11 16:06:25 20.3 - - -
204 2016/03/11 16:06:55 20.2 - - -
205 2016/03/11 16:07:25 19.7 - - -
206 2016/03/11 16:07:55 21.3 - - -
207 2016/03/11 16:08:25 19.7 - - -
208 2016/03/11 16:08:55 21.3 - - -
209 2016/03/11 16:09:25 20.8 - - -
210 2016/03/11 16:09:55 20.8 - - -
211 2016/03/11 16:10:25 20.8 - - -
212 2016/03/11 16:10:55 21.3 - - -
213 2016/03/11 16:11:25 21.3 - - -
214 2016/03/11 16:11:55 21.3 - - -
215 2016/03/11 16:12:25 20.8 - - -
216 2016/03/11 16:12:55 20.8 - - -
217 2016/03/11 16:13:25 20.1 - - -
218 2016/03/11 16:13:55 20.2 - - -
219 2016/03/11 16:14:25 21.3 - - -
220 2016/03/11 16:14:55 21.3 - - -
221 2016/03/11 16:15:25 20.8 - - -
222 2016/03/11 16:15:55 20.8 - - -
223 2016/03/11 16:16:25 20.3 - - -
224 2016/03/11 16:16:55 21.1 - - -
225 2016/03/11 16:17:25 20.8 - - -
226 2016/03/11 16:17:55 20.3 - - -
227 2016/03/11 16:18:25 20.3 - - -
228 2016/03/11 16:18:55 20.6 - - -
229 2016/03/11 16:19:25 19.8 - - -
230 2016/03/11 16:19:55 20.2 - - -
231 2016/03/11 16:20:25 20.8 - - -
232 2016/03/11 16:20:55 20.6 - - -
233 2016/03/11 16:21:25 21.3 - - -
234 2016/03/11 16:21:55 20.6 - - -
235 2016/03/11 16:22:25 20.8 - - -
236 2016/03/11 16:22:55 20.8 - - -
237 2016/03/11 16:23:25 21.1 - - -
238 2016/03/11 16:23:55 20.8 - - -
239 2016/03/11 16:24:25 20.4 - - -
240 2016/03/11 16:24:55 20.2 - - -
241 2016/03/11 16:25:25 21.3 - - -
242 2016/03/11 16:25:55 20.8 - - -
243 2016/03/11 16:26:25 20.4 - - -
244 2016/03/11 16:26:55 20.8 - - -
245 2016/03/11 16:27:25 19.8 - - -
246 2016/03/11 16:27:55 19.9 - - -
247 2016/03/11 16:28:25 20.2 - - -
248 2016/03/11 16:28:55 20.8 - - -
249 2016/03/11 16:29:25 20.8 - - -
250 2016/03/11 16:29:55 21.3 - - -
251 2016/03/11 16:30:25 21.1 - - -
252 2016/03/11 16:30:55 20.8 - - -
253 2016/03/11 16:31:25 21.3 - - -
254 2016/03/11 16:31:55 21.3 - - -
255 2016/03/11 16:32:25 21.3 - - -
256 2016/03/11 16:32:55 20.8 - - -
257 2016/03/11 16:33:25 21.1 - - -
258 2016/03/11 16:33:55 20.8 - - -
259 2016/03/11 16:34:25 20.3 - - -
260 2016/03/11 16:34:55 21.2 - - -
261 2016/03/11 16:35:25 20.8 - - -
262 2016/03/11 16:35:55 20.8 - - -
263 2016/03/11 16:36:25 20.8 - - -
264 2016/03/11 16:36:55 21.3 - - -
265 2016/03/11 16:37:25 21.3 - - -
266 2016/03/11 16:37:55 21.3 - - -
267 2016/03/11 16:38:25 21.3 - - -
268 2016/03/11 16:38:55 19.8 - - -
269 2016/03/11 16:39:25 20.2 - - -
270 2016/03/11 16:39:55 20.8 - - -
271 2016/03/11 16:40:25 20.8 - - -
272 2016/03/11 16:40:55 20.8 - - -
273 2016/03/11 16:41:25 20.8 - - -
274 2016/03/11 16:41:55 20.8 - - -
275 2016/03/11 16:42:25 21.3 - - -
276 2016/03/11 16:42:55 21.3 - - -
277 2016/03/11 16:43:25 20.7 - - -
278 2016/03/11 16:43:55 20.2 - - -
279 2016/03/11 16:44:25 20.3 - - -
280 2016/03/11 16:44:55 20.4 - - -
281 2016/03/11 16:45:25 20.2 - - -
282 2016/03/11 16:45:55 20.2 - - -
283 2016/03/11 16:46:25 21.3 - - -
284 2016/03/11 16:46:55 20.8 - - -
285 2016/03/11 16:47:25 20.8 - - -
286 2016/03/11 16:47:55 20.8 - - -
287 2016/03/11 16:48:25 20.7 - - -
288 2016/03/11 16:48:55 20.8 - - -
289 2016/03/11 16:49:25 19.9 - - -
290 2016/03/11 16:49:55 20.2 - - -
291 2016/03/11 16:50:25 21.3 - - -
292 2016/03/11 16:50:55 21.3 - - -
293 2016/03/11 16:51:25 20.5 - - -
294 2016/03/11 16:51:55 21.3 - - -
295 2016/03/11 16:52:25 21.3 - - -
296 2016/03/11 16:52:55 21.3 - - -
297 2016/03/11 16:53:25 20.8 - - -
298 2016/03/11 16:53:55 20.5 - - -
299 2016/03/11 16:54:25 20.5 - - -
... 53646 more lines ...
|
Attachment 2: 2016-03-11_Evaporator_2.xlsx
|
|
289
|
Thursday, April 07, 2016, 15:23 |
John Wong | SiC | | TARGET BOAT | Done | E-spun SiC/PAN thermal treatment | Thursday, April 07, 2016, 15:18
E-spun SiC/PAN fiber mats were produced at UBC.
12%PAN solution; 50% SiC to weight of PAN.
Materials used:
1.2g PAN, 8.8g DMF, 0.6g SiC, SDS ~0.1% to SiC
Fiber mats were heat treated at 250C in air. Then cut into 18" discs and loaded into Ta target boat with heatshield wrapped.
3 temperature treatments will carry out: 1200C, 1400C and 1600C
Chamber is being pumped down
Friday, April 08, 2016, 10:02
TGHT at 285A, Temp at ~1200C. Will remain at this temp for a few hours before cooling down.
Some samples will be taken out for analysis.
Next week, temperature treatment will continue at 1400C
Friday, April 08, 2016, 14:26
Samples have been heated at 1200C for just over 4 hours.
Initiated auto-cooling at 2A/min
Tuesday, April 12, 2016, 17:51
Heat treatment #2 - 1400C.
Initial mass after 1200C = 0.0312g
Monday, April 18, 2016, 12:55
Samples was heated at 1400C (TGHT maintained at ~370A) for 4 days (see attachment 1).
Chamber is vented; samples will be inspected.
Tuesday, April 19, 2016, 17:49
Results
Sample mass after 1200C = 0.0312g
Sample mass after 1400C = 0.0294g
~5.78% mass loss.
Tuesday, April 19, 2016, 17:57
Heat Treatment#3: 1600C
sample mass before heating = 0.0238g (this sample is taken from the batch after it was heated at 1400C)
Chamber is being pumped.
Thursday, April 21, 2016, 11:07
TGHT stepped up to 330A, temp measured at 1422C.
Thursday, April 21, 2016, 12:05
TGHT at 415A/7.16V; temp at 1610C
Thursday, April 21, 2016, 17:49
Temp dropped to 1590. Increased TGHT to 425A; temp reads 1602A.
Friday, April 22, 2016, 10:57
Voltage increased to 7.33V, TGHT stepped down to 418A, temp maintained at 1610A.
Monday, April 25, 2016, 12:08
Sample was heat treated for almost 4 days. Temperature dropped to 1578C, TGHT at 418/7.26V. (see attachment #2)
Ramping down TGHT 2A/min.
Monday, April 25, 2016, 16:00
Result:
Mass after 1600C = 0.0104g, 5.63% mass loss.
Will do XRD/EDX
|
Attachment 1: SiC_PAN_1400c.PNG
|
|
Attachment 2: archiver.PNG
|
|
|
288
|
Wednesday, March 30, 2016, 11:32 |
John Wong | | Target boat | TARGET BOAT | Done | Thermostablization Polycarbosilane Fibers (UBC MTRL Samples) | Wednesday, March 30, 2016, 11:30
Polycarbosilane fibers were prepared by UBC MTRL.
Two samples with different fiber sizes were loaded in target boat and wrapped with heat shields.
Samples will be heated up to 1600C.
Chamber is currently being pumped down
Thursday, March 31, 2016, 16:49
Ramping up TGHT to 300A at 1A/min
Tuesday, April 05, 2016, 13:02
Samples was heated at 1600C for about 3 hours.
Then it was cooled down at 2A/min.
The process is complete.
|
|
287
|
Thursday, March 24, 2016, 12:05 |
John Wong | SiC | | TARGET BOAT | Done | Test#3: E-spin SiC with PAN | Thursday, March 24, 2016, 11:37
SiC powder (<1um) [10%] was mixed with PAN solution [10%]. Solution was sonicated before e-spinning.
Fiber mat was binded to graphite foil and heat treated to 250C in air for 1 hour.
Samples were cut in pieces and rolled up and inserted in Ta target container (TaC coated). Heat shield was added.
Heat Treatment #1:
Temperature: 1600C (~350A)
Ramping up TGHT to 300A at 1A/min.
Tuesday, March 29, 2016, 11:11
TGHT was maintained at 410A for 1600C for 2 days (see attachment 1). However at around 22:30 on March 28, there was a sudden increase in voltage.
Temperature raised up to 1750C. Not sure there was a fault with the control system and it was caused by the Ta-heat shield. (see attachment #2).
Target was cooled down around 2am on March 29.
Samples will be removed from the chamber.
|
Attachment 1: Screen_Shot_2016-03-26_at_3.39.35_PM.png
|
|
Attachment 2: TGHT_faulty.PNG
|
|
|
286
|
Thursday, March 24, 2016, 11:32 |
John Wong | Ta | 41790-1 | LP-SIS | Done | Ta#47 LP-SIS (with new center block) conditioning |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Anders Mjos wrote: |
Laura Lambert wrote: |
Aurelia Laxdal wrote: |
Started Ta#47 heating at Evap2 using the autoramp program. The TGHT current is setup to go to 300A (for now) and the TBHT to 230A (final value).
|
Monday, March 14, 2016, 09:20
One thermocouple was not welded on correctly and is not working.
Cooling evap2 back down, to remove target and re-weld thermocouple.
Once thermocouple replaced, will ramp back up and continue with tests/ conditioning of target.
|
Monday, March 14, 2016, 13:12: Stopped turbo pump
|
After EVAP2 was vented the thermocouple problem was fixed: it was the wire at on connector inside the box not making proper contact. The lid of the heat shield was also replaced since the one initially mounted had no holes, so one couldn't see the center block. Restarted pumping down at 4:30pm. Just started again the autoramp program: TGHT set to 300A (for the time being) and TBHT to 230A. Temperature measurements will resume tomorrow morning.
|
Raised the TGHT at 620A. The TBHT was already set at 230A. The temperature is at 1902 deg C. As per John's instructions the target will condition at these setpoints over the week-end.
|
Today, lowered the TGHT from 620A (at 1894 deg C) to 300A. TBHT is still at 230A.
|
Cooling down the target.
|
Thursday, March 24, 2016, 11:29
Target was removed from the Evaporator.
The thermocouples broke off.
Need to insert Re foil prior to installing
|
|
285
|
Tuesday, March 22, 2016, 11:31 |
Aurelia Laxdal | Ta | 41790-1 | LP-SIS | In progress | Ta#47 LP-SIS (with new center block) conditioning |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Anders Mjos wrote: |
Laura Lambert wrote: |
Aurelia Laxdal wrote: |
Started Ta#47 heating at Evap2 using the autoramp program. The TGHT current is setup to go to 300A (for now) and the TBHT to 230A (final value).
|
Monday, March 14, 2016, 09:20
One thermocouple was not welded on correctly and is not working.
Cooling evap2 back down, to remove target and re-weld thermocouple.
Once thermocouple replaced, will ramp back up and continue with tests/ conditioning of target.
|
Monday, March 14, 2016, 13:12: Stopped turbo pump
|
After EVAP2 was vented the thermocouple problem was fixed: it was the wire at on connector inside the box not making proper contact. The lid of the heat shield was also replaced since the one initially mounted had no holes, so one couldn't see the center block. Restarted pumping down at 4:30pm. Just started again the autoramp program: TGHT set to 300A (for the time being) and TBHT to 230A. Temperature measurements will resume tomorrow morning.
|
Raised the TGHT at 620A. The TBHT was already set at 230A. The temperature is at 1902 deg C. As per John's instructions the target will condition at these setpoints over the week-end.
|
Today, lowered the TGHT from 620A (at 1894 deg C) to 300A. TBHT is still at 230A.
|
Cooling down the target.
|
|
284
|
Monday, March 21, 2016, 18:57 |
Aurelia Laxdal | Ta | 41790-1 | LP-SIS | In progress | Ta#47 LP-SIS (with new center block) conditioning |
Aurelia Laxdal wrote: |
Aurelia Laxdal wrote: |
Anders Mjos wrote: |
Laura Lambert wrote: |
Aurelia Laxdal wrote: |
Started Ta#47 heating at Evap2 using the autoramp program. The TGHT current is setup to go to 300A (for now) and the TBHT to 230A (final value).
|
Monday, March 14, 2016, 09:20
One thermocouple was not welded on correctly and is not working.
Cooling evap2 back down, to remove target and re-weld thermocouple.
Once thermocouple replaced, will ramp back up and continue with tests/ conditioning of target.
|
Monday, March 14, 2016, 13:12: Stopped turbo pump
|
After EVAP2 was vented the thermocouple problem was fixed: it was the wire at on connector inside the box not making proper contact. The lid of the heat shield was also replaced since the one initially mounted had no holes, so one couldn't see the center block. Restarted pumping down at 4:30pm. Just started again the autoramp program: TGHT set to 300A (for the time being) and TBHT to 230A. Temperature measurements will resume tomorrow morning.
|
Raised the TGHT at 620A. The TBHT was already set at 230A. The temperature is at 1902 deg C. As per John's instructions the target will condition at these setpoints over the week-end.
|
Today, lowered the TGHT from 620A (at 1894 deg C) to 300A. TBHT is still at 230A. |
|
283
|
Friday, March 18, 2016, 17:13 |
Aurelia Laxdal | Ta | 41790-1 | LP-SIS | In progress | Ta#47 LP-SIS (with new center block) conditioning |
Aurelia Laxdal wrote: |
Anders Mjos wrote: |
Laura Lambert wrote: |
Aurelia Laxdal wrote: |
Started Ta#47 heating at Evap2 using the autoramp program. The TGHT current is setup to go to 300A (for now) and the TBHT to 230A (final value).
|
Monday, March 14, 2016, 09:20
One thermocouple was not welded on correctly and is not working.
Cooling evap2 back down, to remove target and re-weld thermocouple.
Once thermocouple replaced, will ramp back up and continue with tests/ conditioning of target.
|
Monday, March 14, 2016, 13:12: Stopped turbo pump
|
After EVAP2 was vented the thermocouple problem was fixed: it was the wire at on connector inside the box not making proper contact. The lid of the heat shield was also replaced since the one initially mounted had no holes, so one couldn't see the center block. Restarted pumping down at 4:30pm. Just started again the autoramp program: TGHT set to 300A (for the time being) and TBHT to 230A. Temperature measurements will resume tomorrow morning.
|
Raised the TGHT at 620A. The TBHT was already set at 230A. The temperature is at 1902 deg C. As per John's instructions the target will condition at these setpoints over the week-end. |
|
282
|
Monday, March 14, 2016, 19:22 |
Aurelia Laxdal | Ta | 41790-1 | LP-SIS | In progress | Ta#47 LP-SIS (with new center block) conditioning |
Anders Mjos wrote: |
Laura Lambert wrote: |
Aurelia Laxdal wrote: |
Started Ta#47 heating at Evap2 using the autoramp program. The TGHT current is setup to go to 300A (for now) and the TBHT to 230A (final value).
|
Monday, March 14, 2016, 09:20
One thermocouple was not welded on correctly and is not working.
Cooling evap2 back down, to remove target and re-weld thermocouple.
Once thermocouple replaced, will ramp back up and continue with tests/ conditioning of target.
|
Monday, March 14, 2016, 13:12: Stopped turbo pump
|
After EVAP2 was vented the thermocouple problem was fixed: it was the wire at on connector inside the box not making proper contact. The lid of the heat shield was also replaced since the one initially mounted had no holes, so one couldn't see the center block. Restarted pumping down at 4:30pm. Just started again the autoramp program: TGHT set to 300A (for the time being) and TBHT to 230A. Temperature measurements will resume tomorrow morning. |
|
281
|
Monday, March 14, 2016, 13:12 |
Anders Mjos | Ta | 41790-1 | LP-SIS | In progress | Ta#47 LP-SIS (with new center block) conditioning |
Laura Lambert wrote: |
Aurelia Laxdal wrote: |
Started Ta#47 heating at Evap2 using the autoramp program. The TGHT current is setup to go to 300A (for now) and the TBHT to 230A (final value).
|
Monday, March 14, 2016, 09:20
One thermocouple was not welded on correctly and is not working.
Cooling evap2 back down, to remove target and re-weld thermocouple.
Once thermocouple replaced, will ramp back up and continue with tests/ conditioning of target.
|
Monday, March 14, 2016, 13:12: Stopped turbo pump |
|
280
|
Monday, March 14, 2016, 09:22 |
Laura Lambert | Ta | 41790-1 | LP-SIS | In progress | Ta#47 LP-SIS (with new center block) conditioning |
Aurelia Laxdal wrote: |
Started Ta#47 heating at Evap2 using the autoramp program. The TGHT current is setup to go to 300A (for now) and the TBHT to 230A (final value).
|
Monday, March 14, 2016, 09:20
One thermocouple was not welded on correctly and is not working.
Cooling evap2 back down, to remove target and re-weld thermocouple.
Once thermocouple replaced, will ramp back up and continue with tests/ conditioning of target.
|
|