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Entry  Thursday, June 09, 2016, 15:48, Laura Lambert, SiC, 41369-4, HP-SIS, In progress, Sintering SiC#33 - 1st beta-SiC target! target_with_end-coils.jpg
    Reply  Friday, June 10, 2016, 16:30, John Wong, SiC, 41369-4, HP-SIS, In progress, Sintering SiC#33 - 1st beta-SiC target! 
       Reply  Monday, June 13, 2016, 09:53, Laura Lambert, SiC, 41369-4, HP-SIS, In progress, Sintering SiC#33 - 1st beta-SiC target! current_vs_voltage_vs_temp.xlsxTapping_up_from_520A_to_1800C.JPG
          Reply  Wednesday, June 15, 2016, 17:58, John Wong, SiC, 41369-4, HP-SIS, In progress, Sintering SiC#33 - 1st beta-SiC target! 
             Reply  Thursday, June 16, 2016, 10:58, Laura Lambert, SiC, 41369-4, HP-SIS, Done, Sintering SiC#33 - 1st beta-SiC target! 
Message ID: 304     Entry time: Monday, June 13, 2016, 09:53     In reply to: 303     Reply to this: 305
Author: Laura Lambert 
Target Material: SiC 
Target Oven W.O#: 41369-4 
Source: HP-SIS 
Status: In progress 
Subject: Sintering SiC#33 - 1st beta-SiC target! 

John Wong wrote:

 

Laura Lambert wrote:

 Thursday, June 09, 2016, 15:39

First target using beta-SiC material!

Target container contains 450 discs of SiC [4 x 5 packs + 430 single discs]

Target packed length = 16cm. 

Mass of 533 discs SiC(green)  = 53.8758g

Container is wrapped with 3 heatshields; no end caps are inserted yet - coated spring inserted both sides to hold discs in place.

Sintering temp = 1800C, TGHT will be set accordingly.  TBHT max at 230A. 

Chamber is currently being pumped down. 


Friday, June 10, 2016, 13:24

HS water valves opened, no leaks detected.

Tapping up manually to 70A...

Auto ramp will be set for TGHT = 0.2A/min to a final setpoint of 520A

Auto-ramp for TBHT = 0.1A/min to a final setpoint of 230A.


 

 

 Friday, June 10, 2016, 16:27

TGHT stepped up to 70A/0.55V.  TGHT at 50A/0.62V. 

Pressure stabilized at 5.5e-5 Torr.

Initiated auto ramping.  TGHT at 0.2A/min --> 520A.  TBHT at 0.1A/min --> 230A.


 

 Monday, June 13, 2016, 09:51

TGHT = 425A, 5.65V

TBHT = 225A, 3.7V

IGP1 = 8.7e-6 Torr.

Increasing ramping rate to 1.0A/min...


 Monday, June 13, 2016, 15:56

Tapped up manually from 520A to 1800C

Extrapolated data on graph to determine correct current required to reach desired max temperature.

Will remain at 1800C for ~48hrs

See attachements for excel sheet and screenshot of striptool.


 

Attachment 1: current_vs_voltage_vs_temp.xlsx  14 kB  Uploaded Monday, June 13, 2016, 16:58
Attachment 2: Tapping_up_from_520A_to_1800C.JPG  81 kB  Uploaded Monday, June 13, 2016, 16:58  | Show | Hide all
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