Tuesday, August 02, 2016, 13:41
Target container contains 471 discs of SiC [6 x 5 packs + 441 single discs]
Target packed length = 16cm.
Mass of SiC(green) = 52.7172g
Container is wrapped with 3 heatshields; no end caps are inserted yet - coated spring inserted both sides to hold discs in place.
Sintering temp = 1800C
TGHT max = 350A. TBHT max at 230A.
Chamber is currently being pumped down.
Slope on OMEGA = 1.04
Tuesday, August 02, 2016, 16:00
Tapped up manually to 30A - vacuum to high, lowered down to 20A to be able to initiate auto-ramp.
IGP1 = 2.3e-5 Torr
Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.
Friday, August 05, 2016, 11:57
Evap2 has reached TGHT = 350A, 5.33V
TBHT = 187A, 2.31V and still climbing...
OMEGA = 1365C
IGP1 = 7.88e-7 Torr
Increased max setpoint for TGHT to 400A.
Friday, August 05, 2016, 13:33
TGHT = 380A, 5.97V
TBHT = 197A, 2.45V
OMEGA = 1396C
IGP1 = 8.75e-7 Torr
Increasing ramping rate to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
New final setpoint for the TGHT = 450A
Friday, August 05, 2016, 14:17
TBHT = 230A, 2.97V
TGHT = 450A, 7.4V
OMEGA = 1572C
IGP1 = 3.2e-6 Torr
Increasing max setpoint for TGHT to 500A and re-initiating auto-ramp.
Friday, August 05, 2016, 15:18
At TGHT = 480A, OMEGA temperature dropped to 1400C due to coating on window.
Last reading was ~1600C
Tapped up manually to TGHT = 500A, 8.61V
Window fully coated therefore OMEGA reading is negligible at this point
Attempted to take temperature reading with other OMEGA from behind evaporator or using handheld manual temperature reader - all windows have a coating, therefore unsuccessful.
IGP1 = 1.75e-6 Torr
Reduced max voltage set for TGHT to 9.0V to minimize possibly voltage 'creep'
Will remain at these setpoints over wknd and ramp down monday morning.
Monday, August 08, 2016, 08:45
TGHT = 500A on the 'current set' and 466A on the readout, 8.74V
TBHT = 230A, 2.99V
IGP1 = 6.6e-8 Torr
OMEGA = 1460C [reading through coating on window port]
Evap2 has been at these setpoints for the wknd.
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Monday, August 08, 2016, 10:38
Quick observational note:
while ramping down OMEGA readings have slowly increased.
At ~350A OMEGA = ~1500C
At ~300A, OMEGA = ~1750C
Currently at 280A, OMEGA = ~2800C
Coating on window has affected the OMEGA readings in a weird way...
Monday, August 08, 2016, 15:17
Vented in air and opened up this afternoon.
Cleaned windows but left target loaded in evap2 for conditioning process.
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