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  Evaporator_2, Page 15 of 34  Not logged in ELOG logo
ID Date Author Target Material Target Oven W.O#down Source Status Subject
  265   Tuesday, December 01, 2015, 11:35 Anders MjosEmpty41077-5LP-SISIn progressTest#2: Measuring temp with thermocouple (away from centre) & 2C-IR

 Data from thermocouple attached. Raw data and Excel sheet with plot.

  253   Wednesday, October 21, 2015, 17:39 John WongEmpty41077-3LP-SISIn progressSintering TaC on LPSIS (small block) container

 Wednesday, October 21, 2015, 17:35

This container is prepared for a backup UCx target (otherwise it will be used for development purposes).

The container is coated with TaC; one layer of Ta-heat shield is used. 

TGHT will be ramped up to reach 1900C (previous container had TGHT ramped up to 440A).  

TBHT will be ramped up to max 230A.  

Chamber is currently being pumped down.  

Heating can begin once the vacuum is good, currently at 4.8e-5 Torr. 


 Friday, October 23, 2015, 16:15

TGHT reached to 500A and temp measured at 1940C.  More about the temp plot can be found in the dropbox.

Initiated cooling down at 2A/min. 

Target will be inspected next Monday.


 

  254   Thursday, October 22, 2015, 11:41 Laura LambertEmpty41077-3LP-SISIn progressSintering TaC on LPSIS (small block) container

John Wong wrote:

 Wednesday, October 21, 2015, 17:35

This container is prepared for a backup UCx target (otherwise it will be used for development purposes).

The container is coated with TaC; one layer of Ta-heat shield is used. 

TGHT will be ramped up to reach 1900C (previous container had TGHT ramped up to 440A).  

TBHT will be ramped up to max 230A.  

Chamber is currently being pumped down.  

Heating can begin once the vacuum is good, currently at 4.8e-5 Torr. 


 

 Thursday, October 22, 2015, 11:36

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

Vacuum stabilized, initiated auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

Final setpoints TGHT = 300A, TBHT = 230A

IGP1 = 1.0e-6 Torr; TGHT = 45.18A, 0.17V; TBHT = 38.4A, 0.41V


 

  255   Thursday, October 22, 2015, 17:10 John WongEmpty41077-3LP-SISIn progressSintering TaC on LPSIS (small block) container

Laura Lambert wrote:

John Wong wrote:

 Wednesday, October 21, 2015, 17:35

This container is prepared for a backup UCx target (otherwise it will be used for development purposes).

The container is coated with TaC; one layer of Ta-heat shield is used. 

TGHT will be ramped up to reach 1900C (previous container had TGHT ramped up to 440A).  

TBHT will be ramped up to max 230A.  

Chamber is currently being pumped down.  

Heating can begin once the vacuum is good, currently at 4.8e-5 Torr. 


 

 Thursday, October 22, 2015, 11:36

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

Vacuum stabilized, initiated auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

Final setpoints TGHT = 300A, TBHT = 230A

IGP1 = 1.0e-6 Torr; TGHT = 45.18A, 0.17V; TBHT = 38.4A, 0.41V


 

 Thursday, October 22, 2015, 17:09

Pressure coming down to 1.5e-6 Torr. 

Increased ramping rate to 2A/min for both TGHT and TBHT.


 

  256   Monday, October 26, 2015, 16:14 Laura LambertEmpty41077-3LP-SISDoneSintering TaC on LPSIS (small block) container & temp measurements with 1xTa h.s

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

 Wednesday, October 21, 2015, 17:35

This container is prepared for a backup UCx target (otherwise it will be used for development purposes).

The container is coated with TaC; one layer of Ta-heat shield is used. 

TGHT will be ramped up to reach 1900C (previous container had TGHT ramped up to 440A).  

TBHT will be ramped up to max 230A.  

Chamber is currently being pumped down.  

Heating can begin once the vacuum is good, currently at 4.8e-5 Torr. 


 

 Thursday, October 22, 2015, 11:36

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

Vacuum stabilized, initiated auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

Final setpoints TGHT = 300A, TBHT = 230A

IGP1 = 1.0e-6 Torr; TGHT = 45.18A, 0.17V; TBHT = 38.4A, 0.41V


 

 Thursday, October 22, 2015, 17:09

Pressure coming down to 1.5e-6 Torr. 

Increased ramping rate to 2A/min for both TGHT and TBHT.


 

 Monday, October 26, 2015, 16:10

Target container was ramped down over the weekend and taken out today.

Coating looks good.

Will add on another Ta layer and continue with temperature measurements.

See attachment for raw data.


 

  257   Monday, October 26, 2015, 16:17 Laura LambertEmpty41077-3LP-SISDonetemp measurements with 2xTa h.s on LPSIS (small block) container

 Monday, October 26, 2015, 16:16

Container previously sintered with TaC coating and temperature measurements taken with 1x Ta heat shield [see elog ID# 256]

2x Ta heat shields on this container.

Loaded into evap2 and currently pumping down.


 Tuesday, October 27, 2015, 10:07

HS water valves opened up this morning, no leaks detected.

Tapped up manually to 35A.

Waited ~10min, vacuum stable

Initiating auto-ramp at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.

Final setpoints: 300A for the TGHT and 230A for the TBHT


 Tuesday, October 27, 2015, 13:54

Reached final setpoints.

IGP1 = 5.3e-7 Torr.

Tapping up manually to 1900C


Tuesday, October 27, 2015, 16:42

Tapped up manually to 1900C

TGHT = 455A, 7.66V

IGP1 = 9e-7 Torr

Will remain at 455A overnight and ramp-down in the morning.


Wednesday, October 28, 2015, 09:32 

TGHT remained at 455A for ~17hrs.

IGP1 = 4.3e-7 Torr.

OMEGA = 1888C

See attachment for raw data of temperature measurements.

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Wednesday, October 28, 2015, 16:32

Vented and took out this afternoon.

Container looks good. 

See photos attached.


 

  258   Monday, November 02, 2015, 16:29 Laura LambertEmpty41077-3LP-SISDonetemp measurements with 3xTa h.s on LPSIS (small block) container

 Monday, November 02, 2015, 16:28

Container previously sintered with TaC coating and temperature measurements taken with 1x Ta heat shield [see elog ID# 256] and 2x Ta heat shield [see elog ID#257]

3x Ta heat shields on this container.

Loaded into evap2 and currently pumping down.


 Tuesday, November 03, 2015, 10:37

HS water valves opened up this morning, no leaks detected.

Tapped up manually to 35A.

Vacuum stable.

IGP1 = 6.8e-7 Torr.

Initiating auto-ramp at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.

Final setpoints: 250A for the TGHT and 230A for the TBHT


 Tuesday, November 03, 2015, 13:09

IGP1 = 7.7e-7 Torr

TGHT = 250A, 3.42V

TBHT = 185A, 3.0V

OMEGA = 1237C

Increasing ramping rate of TBHT to 2.0A/min.


 Tuesday, November 03, 2015, 13:47

Reached final setpoints.

IGP1 = 8.7e-7 Torr.

Tapping up manually to 1900C


 Tuesday, November 03, 2015, 15:45

Tapped up manually to 1900C

TGHT = 450A, 7.26V

IGP1 = 1.6e-6 Torr

Will remain at 450A overnight and ramp-down in the morning.


 Wednesday, November 04, 2015, 10:00

TGHT remained at 450A for ~18hrs.

IGP1 = 6e-7 Torr.

OMEGA = 1908C

See attachment for raw data of temperature measurements and picture showing voltage movement at max setpoint.

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Wednesday, November 04, 2015, 16:43

Vented and took out this afternoon.

Container looks good.

No visible changes to container compared to 2xTa heat shield temp measurements.


 

  259   Thursday, November 05, 2015, 16:20 Laura Lambert 41077-3LP-SISIn progressSintering TaC coating on 'temporary endcaps' springs

 Thursday, November 05, 2015, 16:19

Springs coated with TaC and loaded into container for sintering.

3x Ta heat shield.

EVAP2 currently pumping down.


 Friday, November 06, 2015, 08:39

Opened HS water valves, no leaks detected.

Tapped up manually to 35A.

IGP1 = 5.5e-7 Torr.


 Friday, November 06, 2015, 10:08

IGP1 = 5.8e-7 Torr.

Vacuum stable.

Initiating auto-ramp at 0.2A/min and 0.1A/min with final setpoints of 450A and 230A for the TGHT and TBHT respectively.

See photos attached to view how springs were coated and loaded into container.


 Monday, November 09, 2015, 09:07

TGHT reached 450A, 7.2V ~8pm sat, nov 7th.

OMEGA = 1775C

IGP1 = 3.2e-7 Torr.

Tapping up manually to 1900C.


 

  260   Monday, November 09, 2015, 12:56 John Wong 41077-3LP-SISIn progressSintering TaC coating on 'temporary endcaps' springs (Slope changed to 1.04)

Laura Lambert wrote:

 Thursday, November 05, 2015, 16:19

Springs coated with TaC and loaded into container for sintering.

3x Ta heat shield.

EVAP2 currently pumping down.


 Friday, November 06, 2015, 08:39

Opened HS water valves, no leaks detected.

Tapped up manually to 35A.

IGP1 = 5.5e-7 Torr.


 Friday, November 06, 2015, 10:08

IGP1 = 5.8e-7 Torr.

Vacuum stable.

Initiating auto-ramp at 0.2A/min and 0.1A/min with final setpoints of 450A and 230A for the TGHT and TBHT respectively.

See photos attached to view how springs were coated and loaded into container.


 Monday, November 09, 2015, 09:07

TGHT reached 450A, 7.2V ~8pm sat, nov 7th.

OMEGA = 1775C

IGP1 = 3.2e-7 Torr.

Tapping up manually to 1900C.


 

 Monday, November 09, 2015, 12:30

Checked the temp on the inner surface (not at the spring) of the container was around 2050C at 500A. 

The TaC coated spring is reading at 1900C; that's what the OMEGA is reading with the setting for 2-colors and slope at 0.98.

Lower TGHT to 450A/ 7.12V.

By comparing the data from the previous temp curve (OMEGA slope at 0.98) with no material inside the container,  the voltage and current plot is aligned with the curve.

Changed OMEGA setting slope to 1.04.  Current temp is reading at 1917C at 450A.

For 2-Color setting, the emissivity should be negligible.  That makes me believe that different materials has different slope setting for the temp reading.  

One thing to note is that, the sintering temp of TaC is around 1900-2000C.  It was clear that the container was fully sintered with TGHT at 450A.

Will need to gather more data with different material to understand the slope setting better. 

Try: 

SiC at 1700C, slope at 1.04

ZrC at 1900C, slope at 104

Ta at 1900C, slope at 0.98.

Compare the data...


 

  261   Monday, November 09, 2015, 14:22 Laura Lambert 41077-3LP-SISDoneSintering TaC coating on 'temporary endcaps' springs (Slope changed to 1.04)

John Wong wrote:

Laura Lambert wrote:

 Thursday, November 05, 2015, 16:19

Springs coated with TaC and loaded into container for sintering.

3x Ta heat shield.

EVAP2 currently pumping down.


 Friday, November 06, 2015, 08:39

Opened HS water valves, no leaks detected.

Tapped up manually to 35A.

IGP1 = 5.5e-7 Torr.


 Friday, November 06, 2015, 10:08

IGP1 = 5.8e-7 Torr.

Vacuum stable.

Initiating auto-ramp at 0.2A/min and 0.1A/min with final setpoints of 450A and 230A for the TGHT and TBHT respectively.

See photos attached to view how springs were coated and loaded into container.


 Monday, November 09, 2015, 09:07

TGHT reached 450A, 7.2V ~8pm sat, nov 7th.

OMEGA = 1775C

IGP1 = 3.2e-7 Torr.

Tapping up manually to 1900C.


 

 Monday, November 09, 2015, 12:30

Checked the temp on the inner surface (not at the spring) of the container was around 2050C at 500A. 

The TaC coated spring is reading at 1900C; that's what the OMEGA is reading with the setting for 2-colors and slope at 0.98.

Lower TGHT to 450A/ 7.12V.

By comparing the data from the previous temp curve (OMEGA slope at 0.98) with no material inside the container,  the voltage and current plot is aligned with the curve.

Changed OMEGA setting slope to 1.04.  Current temp is reading at 1917C at 450A.

For 2-Color setting, the emissivity should be negligible.  That makes me believe that different materials has different slope setting for the temp reading.  

One thing to note is that, the sintering temp of TaC is around 1900-2000C.  It was clear that the container was fully sintered with TGHT at 450A.

Will need to gather more data with different material to understand the slope setting better. 

Try: 

SiC at 1700C, slope at 1.04

ZrC at 1900C, slope at 104

Ta at 1900C, slope at 0.98.

Compare the data...


 

 Monday, November 09, 2015, 14:20

IGP1 = 3.3e-7 Torr.

TGHT = 450A, 7.12V

OMEGA = 1915C

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Tuesday, November 10, 2015, 13:23

Vented and opened this morning.

springs look [mostly] sintered.

see photo attached.

 

  262   Tuesday, November 10, 2015, 14:34 Laura LambertSiC41077-3LP-SISDonetemp measurements with 3xTa h.s on LPSIS (small block) container with SiC

 Tuesday, November 10, 2015, 14:20

Container previously sintered with TaC coating and temperature measurements taken [see elog ID# 256, 257, 258]

3x Ta heat shields

2 packs of 5 SiC discs ~2inches from the end of the right side wrt ionizer tube into page.

Loaded into evap2 and currently pumping down.

see photos attached.


 Monday, November 16, 2015, 11:24

HS water valves opened up this morning, no leaks detected.

Tapped up manually to 35A.

Vacuum stable.

IGP1 = 3.4e-7 Torr.

Initiating auto-ramp at 1.0A/min and 0.5A/min for the TGHT and TBHT respectively.

Final setpoints: 250A for the TGHT and 230A for the TBHT


Monday, November 16, 2015, 13:29

Vacuum too high.

IGP1 = 2.9e-5 Torr.

Decreasing ramping rate down to 0.5A/min and 0.2A/min for the TGHT and TBHT respectively.


 Tuesday, November 17, 2015, 09:12

IGP1 = 1.45e-7 Torr.

TGHT = 250A, 3.28V

TBHT = 230A, 3.33V

OMEGA = 1194C

Tapping up manually to 1900C


 Tuesday, November 17, 2015, 11:22

Tapped up manually to 1800C, realized SiC should only be tapped up to 1700C, backed off immediately down to 415A from 460A/ 1800C.

See attachment for photo of striptool/ time spent above 1700C [~20min].


 Tuesday, November 17, 2015, 15:46

TGHT remained at 1700C for ~4hrs.

TGHT = 420A, 6.44V.

IGP1 = 2.3e-7 Torr.

Initiating cool-down at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.

See attachment for raw data of temperature measurements.


 Wednesday, November 18, 2015, 13:32

Vented in air and took out this morning.

Looks good, no visual changes with the container.


 

  270   Monday, January 11, 2016, 15:47 Laura LambertSiC41077-3LP-SISDoneConditioning SiC test target for test stand measurements

Monday, January 11, 2016, 15:25

Small center block LP-SIS container previously sintered with TaC coating

3x Ta heat shields

Container is loaded with 260 discs of SiC with a total length of 8.5cm

Loaded into evap2 and pumped down this morning

HS water valves opened up, no leaks detected

Tapped up manually to 30A

Vacuum stable

IGP1 = 1e-6 Torr

Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively

Final setpoints: 400A for the TGHT and 230A for the TBHT

Final desired temperature: 1700C


 Tuesday, January 12, 2016, 12:55

TGHT = 138A, TBHT = 80A

IGP1 =  7.7e-6 Torr.


Vacuum stable and coming down.

Increasing ramping rate to 0.5A/min and 0.2A/min for the TGHT and TBHT respectively.


 Wednesday, January 13, 2016, 09:32

TGHT reached 400A ~11.5hrs ago

TBHT reached 230A ~8hrs ago

OMEGA = 1400C

IGP1 = 1.75e-7 Torr

Tapping up manually to 1700C...


 Wednesday, January 13, 2016, 10:14

Previous temperature measurement of OMEGA = 1400C is wrong due to window port being coated with SiC [see attached photos]

Will remain at TGHT = 420A for 4hrs then cool down this afternoon


Wednesday, January 13, 2016, 14:29

Remained at max setpoints for 4.5hrs.

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Thursday, January 14, 2016, 09:47

Vented in air and opened up this morning

Target looks good

Will insert and expand endcaps this afternoon


 

  176   Monday, February 02, 2015, 16:33 John WongEmpty41077-2LP-SISIn progressCoating/Sintering TaC on target container - For Graphite Insert

Monday, February 02, 2015, 16:28

Container is coated with TaC.  No Ta foil wrapped around. 

Chamber is being pumped down.

TGHT/TBHT will be ramped up to 580A/230A at 0.2A/min.


 

 

  177   Tuesday, February 03, 2015, 10:31 Laura LambertEmpty41077-2LP-SISIn progressCoating/Sintering TaC on target container - For Graphite Insert

John Wong wrote:

Monday, February 02, 2015, 16:28

Container is coated with TaC.  No Ta foil wrapped around. 

Chamber is being pumped down.

TGHT/TBHT will be ramped up to 580A/230A at 0.2A/min.


 

 

 Tuesday, February 03, 2015, 10:28

HS water valves opened; no leaks detected.

IGP1 = 5.9e-7 Torr


 Wednesday, February 04, 2015, 11:10

attempted to initiate manual ramp up of TGHT and TBHT yesterday, but not responding to EPICS

currently sitting under vacuum, waiting on fix...


 Wednesday, February 04, 2015, 14:16

controls fixed.

initiated auto-ramp.


 Thursday, February 05, 2015, 08:56

IGP1 = 4.1e-7 Torr

TGHT = 290A

TBHT = 225A

Increasing auto-ramp to 1.0A/min


 Thursday, February 05, 2015, 13:49

IGP1 = 1.4e-6 Torr

TGHT = 569A

TBHT = 232A

Increasing auto-ramp to 2.0A/min


 

  178   Thursday, February 05, 2015, 18:03 John WongEmpty41077-2LP-SISIn progressCoating/Sintering TaC on target container - For Graphite Insert

Laura Lambert wrote:

John Wong wrote:

Monday, February 02, 2015, 16:28

Container is coated with TaC.  No Ta foil wrapped around. 

Chamber is being pumped down.

TGHT/TBHT will be ramped up to 580A/230A at 0.2A/min.


 

 

 Tuesday, February 03, 2015, 10:28

HS water valves opened; no leaks detected.

IGP1 = 5.9e-7 Torr


 Wednesday, February 04, 2015, 11:10

attempted to initiate manual ramp up of TGHT and TBHT yesterday, but not responding to EPICS

currently sitting under vacuum, waiting on fix...


 Wednesday, February 04, 2015, 14:16

controls fixed.

initiated auto-ramp.


 Thursday, February 05, 2015, 08:56

IGP1 = 4.1e-7 Torr

TGHT = 290A

TBHT = 225A

Increasing auto-ramp to 1.0A/min


 Thursday, February 05, 2015, 13:49

IGP1 = 1.4e-6 Torr

TGHT = 569A

TBHT = 232A

Increasing auto-ramp to 2.0A/min


 

 Thursday, February 05, 2015, 18:02

Auto-cooling TGHT to 400A at 1A/min.  Need to take voltage reading tomorrow. 


 

  179   Tuesday, February 10, 2015, 13:19 Laura LambertEmpty41077-2LP-SISDoneCoating/Sintering TaC on target container - For Graphite Insert

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

Monday, February 02, 2015, 16:28

Container is coated with TaC.  No Ta foil wrapped around. 

Chamber is being pumped down.

TGHT/TBHT will be ramped up to 580A/230A at 0.2A/min.


 

 

 Tuesday, February 03, 2015, 10:28

HS water valves opened; no leaks detected.

IGP1 = 5.9e-7 Torr


 Wednesday, February 04, 2015, 11:10

attempted to initiate manual ramp up of TGHT and TBHT yesterday, but not responding to EPICS

currently sitting under vacuum, waiting on fix...


 Wednesday, February 04, 2015, 14:16

controls fixed.

initiated auto-ramp.


 Thursday, February 05, 2015, 08:56

IGP1 = 4.1e-7 Torr

TGHT = 290A

TBHT = 225A

Increasing auto-ramp to 1.0A/min


 Thursday, February 05, 2015, 13:49

IGP1 = 1.4e-6 Torr

TGHT = 569A

TBHT = 232A

Increasing auto-ramp to 2.0A/min


 

 Thursday, February 05, 2015, 18:02

Auto-cooling TGHT to 400A at 1A/min.  Need to take voltage reading tomorrow. 


 

 Tuesday, February 10, 2015, 09:35

Vented and opened this morning.

Container fully sintered.


 

  180   Tuesday, February 10, 2015, 14:01 Laura LambertEmpty41077-2LP-SISDoneConditioning graphite insert inside container - no heat shield

 Tuesday, February 10, 2015, 14:00

Container loaded into EVAP2 at noon.

no heat shields.

Chamber currently being pumped down.

TGHT/ TBHT will be ramped up to 580A/ 230A, tapped up manually.


 Tuesday, February 10, 2015, 14:39

HS water valves opened, no leaks detected.

Tapping up manually / recording data in excel


 Wednesday, February 11, 2015, 11:24

Reached max set points yesterday early evening.

Tapped down manually this a.m.

Will vent and open this afternoon.


 Wednesday, February 11, 2015, 15:54

Took out this afternoon.

container looks good.

graphite insert removed/ inspected - not much change, slightly lighter in colour.

[see attachments for graphs/ table]


 

  181   Wednesday, February 11, 2015, 16:12 Laura LambertEmpty41077-2LP-SISDoneConditioning graphite insert inside container - with heat shield

 Wednesday, February 11, 2015, 16:10

Container loaded into EVAP2.

3xTa heat shields.

Chamber currently being pumped down.

TGHT/ TBHT will be ramped up to 580A/ 230A or 1800C tapped up manually.


 Thursday, February 12, 2015, 09:39

HS water valves opened, no leaks detected.
Tapping up manually.


 Thursday, February 12, 2015, 12:07

OMEGA reached 1805C; TGHT = 415A, TBHT = 205A

Will continue to tap up manually to 2000C


 Thursday, February 12, 2015, 15:19

Reached TGHT = 500A, TBHT = 230A, OMEGA = 2035C.

Sat for ~2hrs.

Tapping up a further 25A on the TGHT.


 Thursday, February 12, 2015, 16:05

Tapped up manually to:

OMEGA = 2250C

DV = 5.65V

TGHT = 580A

TBHT = 230A


Friday, February 13, 2015, 10:05

Reached max setpoint last night.

Voltage starting to increase at contant TGHT @ 580A.  Lower TGHT to 525A, temp at 2150C (time 6:30pm) 

Initiating manual cool down.


Friday, February 13, 2015, 15:31

vented and opened up this afternoon.

everything looked good, container not broken! graphite insert looked good! the container was slightly bent, but nothing of significance.

however, the graphite insert bonded to the container so it was not taken out in one piece...

  273   Friday, February 12, 2016, 11:09 Laura LambertEmpty41077-1LP-SISDonesintering TaC coated small center block container

 Friday, February 12, 2016, 11:01

Container coated with TaC with new method - ends tapped off,  liquid poured/swirled around container, then poured back out - 'flushing technique'.

Container wrapped with 3 x Ta heat shields, incl center block - new method of each layer being one long single Ta foil covering entire container incl center block

IGP1 = 6.3e-7Torr

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

Waited ~20min.

Vacuum stable, IGP1 = 1.3e-6 Torr.

Initiated auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively with final setpoints of 400A and 230A.


 Monday, February 15, 2016, 08:56

IGP1 = 3.9e-7 Torr.

TBHT = 230A, 4.0V

TGHT = 400A, 6.58V

OMEGA = 1766C

Tapping up manually to 1900C...


 Monday, February 15, 2016, 10:18

IGP1 = 5e-7 Torr

TGHT = 450A, 7.55V

OMEGA = 1913C


 Monday, February 15, 2016, 14:30

IGP1 = 4.9e-7 Torr.

TGHT = 450A, 7.55V.

Material remained at ~1910C for ~4hrs.

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Tuesday, February 16, 2016, 14:17

vented in air and opened up this morning.

target container sintered nicely.


 

  309   Friday, July 15, 2016, 11:52 Laura LambertEmpty40860-3LP-IG-LISDonesintering TaC coating on SiC#34 container

 Friday, July 15, 2016, 11:49

Container previously coated with TaC using 'flushing technique', cleaned ionizer tube with acetone, so no coating inside ionizer tube

Wrapped with 3 x Ta heat shields, incl center block - new method of each layer being one long single Ta foil covering entire container incl center block

Currently pumping down in evap2


 Friday, July 15, 2016, 14:35

Turbo pump broken 

Currently being replaced...


 Friday, July 15, 2016, 17:04

Turns out its not the turbo pump...TP controls and pump replaced, problem still happening.

Took out heat shield and used a closed loop to rule out leak in chamber, emptied all water lines - turbo pump now on.

Took v.long time to pump down. TP will remain on over wknd.

BP turns on, PV1 turns on, RV turns on - then takes very long time for vacuum to drop ~45min? before BV and TP can be turned on.

Possibly problem with threads on heat shield and not creating proper seal?

Will continue monday with evap2 mystery problem solving...


Monday, July 18, 2016, 16:14

Replaced heat shield and copper seals.

Container re-loaded.

Turbo pump on and good vacuum achieved! YAY!

Finished pumping down, opened HS water valves - no leaks detected.

Tapped up manually to 35A

Vacuum stable, IGP1 = 3e-6 Torr

Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 400A

Initiating auto ramp for TBHT @ 0.1A/min to a max setpoint of 230A

Once max setpoints achieved, will tap up manually to final desired temperature of 1900C


 Tuesday, July 19, 2016, 09:21

TGHT = 242A, 2.76V

TBHT = 162A

IGP1 = 5.05e-6 Torr

Increasing ramping rate to 1.0A/min and 0.5A/min for the TGHT and TBHT respectively.


 Tuesday, July 19, 2016, 13:04

TGHT = 400A, 4.4V

TBHT = 230A, 2.6V

OMEGA = 1120C

Reached max setpoints ~1hr ago.

Tapping up manually to 1900C...


Tuesday, July 19, 2016, 16:32

MORE problems with evap2 

TGHT reads 460A, 5.1V, 1170C - a lot of power is being lost somewhere...

Comparison from elog i.d. 291 [the last IGLIS container sintering of TaC coating] the TGHT read 460A, 7.5V, 1900C

Another problem: the read out on the power supply and read out on epics of the TBHT reads 215A; however, the 'current set' says 177A - two very different numbers?!

Ramping down evap2 at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively to further inspect chamber and hopefully solve this...


 Wednesday, July 20, 2016, 13:34

Chamber was vented in air and opened up for inspecting.

Fixed!

One of the steel plates used to stop reflection onto the door of the chamber was inserted improperly, resting on top of the 2 negative copper lines to the target leg, this was causing a short.

There was also a short from the right target leg touching the copper heat shield, the heat shield has been shaved down and corrected. It is no longer touching.

There were also 2 brackets that had fallen behind evap2 inside the cage, one was touching the positive lines - it wasn't quite touching the ground, but may have grounded it, causing another possible short.

The chamber was pumped back down and the HS water valves re-opened. No leaks detected.

Evap2 was tapped up manually to 35A.

Vacuum stable = 1.0e-6 Torr.

Initiating auto-ramp at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.

Final setpoints are TGHT = 400A and TBHT = 230A


 Wednesday, July 20, 2016, 16:25

TGHT = 315A, 4.5V

TBHT = 174A, 2.1V

IGP1 = 2e-6 Torr

OMEGA = 1518C

Lowering auto-ramp to 0.2A/min and 0.1A/min for the TGHT and TBHT overnight while unable to keep watch on the vacuum.


 Thursday, July 21, 2016, 09:09

Evap 2 reached max setpoints ~7.5hrs ago.

TGHT = 400A, 6.3V

TBHT = 230A, 2.9V

IGP1 = 5.1e-7 Torr.

OMEGA = 1882C

Tapping up manually to 1900C...


 Friday, July 22, 2016, 16:18

Container has remained at ~1900C for ~31hrs

TGHT reached 405A/1900C - then after ~23hrs dropped in temperature down to 1895C so was tapped up further to 410A/1910C for another ~8hrs.

TGHT = 410A, 6.57V

IGP1 = 3.1e-7 Torr

TBHT = 230A, 2.9V

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.

Will remove from evap2 after the weekend.


 Tuesday, July 26, 2016, 16:49

vented in air.

container looks good, fully sintered.

will update with photos tomorrow...


 

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