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Entry  Thursday, September 15, 2016, 16:37, Laura Lambert, SiC, 39530-9, HP-FEBIAD, In progress, Sintering SiC#35 
    Reply  Monday, September 19, 2016, 18:48, John Wong, SiC, 39530-9, HP-FEBIAD, In progress, Sintering SiC#35 - Change OMEGA/MiKRON slopes 
       Reply  Tuesday, September 20, 2016, 15:40, Laura Lambert, SiC, 39530-9, HP-FEBIAD, In progress, Sintering SiC#35 sintering_target_data.xlsx
          Reply  Thursday, September 22, 2016, 12:14, John Wong, SiC, 39530-9, HP-FEBIAD, In progress, Sintering SiC#35 
             Reply  Monday, September 26, 2016, 13:49, Laura Lambert, SiC, 39530-9, HP-FEBIAD, Done, Sintering SiC#35 comparison_of_temperature_drop_-_3x_snapshots.JPG
Message ID: 322     Entry time: Thursday, September 15, 2016, 16:37     Reply to this: 323
Author: Laura Lambert 
Target Material: SiC 
Target Oven W.O#: 39530-9 
Source: HP-FEBIAD 
Status: In progress 
Subject: Sintering SiC#35 

 Thursday, September 15, 2016, 16:23

Target container contains 487 discs of SiC 

Target packed length = 16cm. 

Mass of SiC(green)  = 58.8795g

Container is wrapped with 1x heatshield around each side of cooling fins; no end caps are inserted yet - coated spring inserted both sides to hold discs in place.

Sintering temp = 1800C

Chamber is currently being pumped down. 


 Friday, September 16, 2016, 10:50

Tapped up manually to 50A

Waited ~1hr , vacuum stable.

IGP1 = 1.24e-5 Torr

Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

TGHT max = 500A.  TBHT max at 230A. 

Slope on OMEGA = 1.15


 Monday, September 19, 2016, 10:53

OMEGA = 1230C

TGHT = 360A, 4.75V

TBHT = 204A, 2.68V

IGP1 = 5.3e-6 Torr

Increasing ramping rate to 1.0A/min and 0.5A/min for the TGHT and TBHT respectively.


 Monday, September 19, 2016, 11:57

OMEGA = ~1300C

TBHT = 230A, 3.16V

TGHT = 409A, 5.55V

Lowering ramping rate to 0.2A/min while vaccum high

IGP1 = 3.05e-5 Torr


 Monday, September 19, 2016, 13:22

OMEGA = 1350C

TGHT = 425A, 5.82V

IGP1 = 1.97e-5 Torr

Stepping ramping rate back up to 1.0A/min


 

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