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Entry  Tuesday, May 07, 2013, 16:53, Nikita Bernier, BeO, , , Done, Sintering BeO pellets #6 
    Reply  Monday, May 13, 2013, 12:53, Nikita Bernier, BeO, , , Done, Sintering BeO pellets #6 600Down.png
       Reply  Monday, May 13, 2013, 17:17, Nikita Bernier, BeO, , , Done, Sintering BeO pellets #6 
Message ID: 72     Entry time: Tuesday, May 07, 2013, 16:53     Reply to this: 73
Author: Nikita Bernier 
Target Material: BeO 
Target Oven W.O#:  
Source:  
Status: Done 
Subject: Sintering BeO pellets #6 

 Tuesday, May 07, 2013, 16:48

 

5 BeO pellets were made.  Each weights about 1.3 g (including org mass). 

A piece of Re foil (0.002" thick) is used as the under layer to protect the reaction between Be(g) and the Ta-boat.  (see Pictures)

Another layer of Ta-foil is used as the heat-shield to wrap around the Ta-boat.

The chamber was pumped down. 

TGHT will be ramped up to 600 A (~1360°C) at 0.2 A/min. The vacuum limit parameter was set for good vacuum at < 3.0e-5 Torr and bad vacuum at > 4.0e0-5 Torr.

The pressure, voltage and current will be closely monitored. 

If the Ta-boat survives, the TGHT will continue to ramp up to max 800 A (~1580°C).

 

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