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Entry  Wednesday, August 07, 2024, 15:37, Aaron Schmidt, , , , , Turning on EVAP2's turbo pump 
    Reply  Thursday, August 08, 2024, 11:17, Marla Cervantes, C, 44139-5 SK, LP TUBE, Done, Graphite foils conditioning GraphiteFoil-Conditioning-EVAP2.JPG
Message ID: 669     Entry time: Thursday, August 08, 2024, 11:17     In reply to: 668
Author: Marla Cervantes 
Target Material:
Target Oven W.O#: 44139-5 SK 
Source: LP TUBE 
Status: Done 
Subject: Graphite foils conditioning 

Aaron Schmidt wrote:

Wednesday, August 07, 2024, 15:36: Roughing. Had initially been roughed & TP started w/ Marla CS, however it timed out. Restarting.

Wednesday, August 07, 2024, 15:37: TP on.

Wednesday, August 07, 2024, 15:46: Tripped at 4 KRPM. Restarted. Up to 5 KRPM.

Failed to start.


Thursday, August 08, 2024, 10:00: TP started. 

Thursday, August 08, 2024, 10:12: TP Tripped but nearly spun up. Reset & Restarted. TP Green / on.


Thursday, August 08, 2024, 10:43

A cartridge was filled with graphite foils and loaded in an uncoated tantalum tube. The tube was wrapped with four Ta-sheets. A Ta-foil was placed in the tube's right end for measuring the temperature.

Green graphite target characteristics
Number of discs 822
Mass of discs 11.74 g
Mass of loaded cartridge with normal cap and hole-cap 31.1290 g
Mass of tube loaded, w/shields and tantalum cap 250 g

 

Note: A cartridge loaded with graphite foils has not been conditioned before. Thus, there is no reference on what current to use to reach 2000 °C.

The conditioning of a graphite composite target will be used as a reference, but note that the graphite foils are not expected to outgas as the composites since the foils do not contain binders and plasticizers. 

 

Reference: Elog 636  Graphite inside insert Experiment 2 (regular formulation discs)  

 

Initial ramps used in elog 636: 

  • 1A/min to 200A 

  • 0.5A/min while taking temperature readings periodically until 250A 

  • At 250 A will let pressure stabilize and then ramp at 1A/min to 2000C or 480A

  •  

Currently waiting for vacuum to reduce to IGP1= 8.2e-07


Thursday, August 08, 2024, 11:23

 

Slope: 0.98 (same as slope used for tantalum targets since temperature is measured on Ta foil) 


 Friday, August 09, 2024, 08:50

Good vacuum 3e-5 Torr

Bad vacuum 5e-5 Torr

Initial IGP1 = 5.06E-7 Torr

Starting ramp at 1A/min to 200 A


Friday, August 09, 2024, 09:40 Pressure started to rise, but temperature is not within pyrometer range yet. Current 42 A, Voltage 0.5 V

Friday, August 09, 2024, 10:46 Pressure started to reduce (peak 1.4e-5 Torr). Temperature is not within pyrometer range yet Current 100 A, Voltage 1.3 V

Friday, August 09, 2024, 11:28 Temperature started to be detected, but not stable enough. Current 135 A, Voltage 1.9 V

Friday, August 09, 2024, 12:54 Temperature 1129 °C, current 196 A, voltage 3 V.


Friday, August 09, 2024, 12:56

Next ramp 0.5A/min while taking temperature readings periodically until 250A


Friday, August 09, 2024, 14:45

IGP1 = 1.0e-6 Torr

Next ramp 1A/min to 480 A aiming at 2000 °C


Friday, August 09, 2024, 17:13

IGP1 = 1.9e-6 Torr, Current 327A, Voltage 5.3V

Ramp changed to 2A/min to 480 A aiming at 2000 °C


Coolded down after 4 hours at ~2000°C

at -2A/min

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