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Entry  Wednesday, August 17, 2016, 17:31, Laura Lambert, Empty, 39814-V2-1, LP-IG-LIS, In progress, sintering TaC coating on SiC#34 container...round2 leak.JPGwater_leak.JPEG
    Reply  Tuesday, August 23, 2016, 12:15, John Wong, Empty, 39814-V2-1, LP-IG-LIS, Done, sintering TaC coating on SiC#34 container...round2 
Message ID: 314     Entry time: Wednesday, August 17, 2016, 17:31     Reply to this: 316
Author: Laura Lambert 
Target Material: Empty 
Target Oven W.O#: 39814-V2-1 
Source: LP-IG-LIS 
Status: In progress 
Subject: sintering TaC coating on SiC#34 container...round2 

 Wednesday, August 17, 2016, 17:30

Container coated with TaC using 'flushing technique', cleaned ionizer tube with acetone, so no coating inside ionizer tube

Wrapped with 3 x Ta heat shields, incl center block

Currently pumping down in evap2


Thursday, August 18, 2016, 10:14 

HS water valves opened...leak detected  see attachment for photo from archives

Vented and opened up.

Anders performed leak check, nothing found.

Replaced all seals with blue seals.

Pumping down now


 Thursday, August 18, 2016, 16:12

HS water valves opened...leak detected again  see attachment for photo of striptool

Vented and opened up.

working with Anders on finding leak...


 Monday, August 22, 2016, 10:38

leaks FIXED!

HS water valves opened, NO leaks detected!

Tapped up manually to 70A

Vacuum stable, IGP1 = 2.5e-6 Torr

Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 350A

Initiating auto ramp for TBHT @ 0.1A/min to a max setpoint of 230A

Once max setpoints achieved, will tap up manually to final desired temperature of 1900C


 Monday, August 22, 2016, 14:58

TGHT = 115A, 1.3V

TBHT = 89A, 0.97V

IGP1 = 4.1e-7 Torr.

Increasing ramping rate to 1.0A/min and 0.5A/min for the TGHT and TBHT respectively.


 Monday, August 22, 2016, 16:01

IGP1 = 1.25e-6 torr

TGHT = 174A, 2.2V

TBHT = 118A, 1.4V

Lowering ramping rate to 0.2A/min and 0.1A/min for the TGHT and TBHT respectively for overnight ramping.


 

Attachment 1: leak.JPG  64 kB  Uploaded Thursday, August 18, 2016, 11:22  | Show | Show all
Attachment 2: water_leak.JPEG  25 kB  Uploaded Thursday, August 18, 2016, 17:15  | Show | Show all
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