Logbooks Lab Maintenance Evaporator_1 Evaporator_2 Laser cutter Target Production Test-Stand RH-ISAC RH-Cyclotron RH-Meson Hall RH-Beamlines RH-ARIEL
  Evaporator_2  Not logged in ELOG logo
Entry  Thursday, September 24, 2015, 09:48, Laura Lambert, Empty, 41077-5, , In progress, Sintering TaC coating container for UCx Target 
    Reply  Thursday, September 24, 2015, 12:18, John Wong, Empty, 41077-5, LP-SIS, Done, Sintering TaC coating container for UCx Target Screen_Shot_2015-09-24_at_11.51.11_AM.png420A_1900.pngTaC_coat_sintered.png
       Reply  Tuesday, October 06, 2015, 15:18, John Wong, Empty, 41077-5, LP-SIS, In progress, Test#1: Measuring temp with thermocouple (centre) & 2C-IR Temp_LPSIS_IR2C_vs_typeC.PNGTemp_LPSIS_IR2C_vs_typeC_heating_cooling.PNG
          Reply  Thursday, October 08, 2015, 12:26, John Wong, Empty, 41077-5, LP-SIS, In progress, Test#2: Measuring temp with thermocouple (away from centre) & 2C-IR Test_2_tempcurves.PNGTest1&2_IV_temp_.png
             Reply  Tuesday, December 01, 2015, 11:35, Anders Mjos, Empty, 41077-5, LP-SIS, In progress, Test#2: Measuring temp with thermocouple (away from centre) & 2C-IR 2015-10-08_Small_Centre_Block.xlsx2015-10-08.4ch2015-10-06.4ch2015-10-06_Small_Centre_Block.xlsx
Message ID: 250     Entry time: Thursday, September 24, 2015, 12:18     In reply to: 249     Reply to this: 251
Author: John Wong 
Target Material: Empty 
Target Oven W.O#: 41077-5 
Source: LP-SIS 
Status: Done 
Subject: Sintering TaC coating container for UCx Target 

Laura Lambert wrote:

Thursday, September 24, 2015, 08:39

IGP1 = 6.5e-7Torr

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

Waited ~20min.

Vacuum stable, IGP1 = 1.5e-6 Torr.

Initiated auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively with final setpoints of 250A and 230A.

Final temp of 1200C on auto-ramp in order to initiate temperature measurements starting at ~1200C.


Thursday, September 24, 2015, 10:24  

IGP1 = 8.7e-7 Torr

TGHT = 44A, TBHT = 38A

Increasing auto-ramp to 0.5A/min and 0.2A/min for the TGHT and TBHT respectively.


 

 

 Thursday, September 24, 2015, 12:04

 A few notes about the target container:The Ta-foil is cut in a full length of the target container, and that also covers up the back block, and the container is wrapped with 3 sheets (see attachment)

 The inner tube is coated with TaC, using the "flushing technique" - the coating looks much better; will see how it turns out after the sintering process

The target will be heated up to 1900C .  Due to the new wrapping of the Ta-heat shield, the heat distribution may be different.  So the target heater will be ramped up to achieve the desired temperature.  


Thursday, September 24, 2015, 18:45  

TGHT reached to 250A3.6V, TGHT at 230A and stayed for 1.5 hours.  Temp-L = 1280C, Temp-R = 1360C.  

Auto-ramp TGHT to 500A at 1A/min and heat at that current for overnight.  Will take temp reading tomorrow.  


Thursday, September 24, 2015, 23:08  

TGHT has reached to 500A/8.57V.  Temp-L = 1895C, Temp-R = 2073C. (Not sure why the temperature is real, will need to investigate more to get an absolute temp)

Just to be safe… Ramping down TGHT to 425A (according to e-log id 216, Temp-R reached to 1800C with TGHT at 425A/6.84V, but no temp measured for the left at that time)

Will check again later.


Friday, September 25, 2015, 11:52  

The target has been heated at 420A for ~12hours; temp measured ~1900C, slightly higher than the previous target container (W.O#40860-1); the Ta-wraping could affect the heat distribution.  

The temperature is also confirmed by using the 2-C digital pyrometer.  The tube inner surface is measured about 1900C, and the ionizer tube is about 2400C.  (see attachment #2).

Initiating auto-cooling at 2A/min for TGHT and 1A/min for TBHT.

The target will be inspected next Monday


 Wednesday, September 30, 2015, 16:01

The target container is fully sintered (see attachment#3) 

It is still in the discussion where this container will be used online for the UCx.  Nevertheless, the target contain is ready and it looks pretty good. 


 

Attachment 1: Screen_Shot_2015-09-24_at_11.51.11_AM.png  849 kB  | Show | Hide all
Attachment 2: 420A_1900.png  583 kB  Uploaded Friday, September 25, 2015, 12:56  | Hide | Hide all
420A_1900.png
Attachment 3: TaC_coat_sintered.png  808 kB  Uploaded Wednesday, September 30, 2015, 17:01  | Show | Hide all
ELOG V2.9.2-2455