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Entry  Tuesday, October 30, 2018, 10:17, Marla Cervantes, UC2, 43044-7 , LP-SIS, In progress, UCx Fully loaded graphite insert thermal test - FL#1 Heat_test.JPG
    Reply  Wednesday, October 31, 2018, 10:30, Marla Cervantes, UC2, 43044-7 , LP-SIS, Problems, UCx Fully loaded graphite insert thermal test - FL#1 current-trip_off.JPGepics.JPG
       Reply  Wednesday, October 31, 2018, 15:23, Marla Cervantes, UC2, 43044-7 , LP-SIS, Done, UCx Fully loaded graphite insert thermal test - FL#1 Ta-container.png
Message ID: 230     Entry time: Wednesday, October 31, 2018, 15:23     In reply to: 229
Author: Marla Cervantes 
Target Material: UC2 
Target Oven W.O#: 43044-7  
Source: LP-SIS 
Status: Done 
Subject: UCx Fully loaded graphite insert thermal test - FL#1 

Marla Cervantes wrote:

Marla Cervantes wrote:

 Tuesday, October 30, 2018, 10:12

A new LP-SIS was coated and syntered (e-log 420 Evaporator_2) 

The container was loaded with a graphite insert loaded with UCx

Graphite insert + UCx mass = 26.927 g

A current of 440 A TGHT and 230 A TBHT will be inputed to the contianer


IGP1 = 8.72e-7 Torr

 The current was tapped manually to 440 A TGHT and 230 A TBHT (see fig. Heating test)

Maximum pressure during heating = 1.7e-3 Torr.

Target will stay at maximum current for 1 week.

 Wednesday, October 31, 2018, 10:09

The current tripped off,  around 5:00 am, the pressure was below 1e-5 Torr (see fig. current-trip_off).

On a previous test, we measured the maximum temperature of the power supply = 33.3 C (e-log 227).

Power supply overheating doesn't seem to be the problem.

EPICS windows are half withe and not answering correctly.

Also, TBHT says that IGP1 < 500 mTorr, and its interlock needs reset (see figure EPICS).

 Wednesday, October 31, 2018, 15:20

The problem was reported to controls, it will be also reported to power supply group.

In the meantime, the target will be ramp-up again with the auto ramp at:

TGHT = 20 A/min to 440 A

TBHT = 10 A/min to 230 A 

The pressure before heating is 4.07e-7 Torr


Wednesday, October 31, 2018, 19:24

The maximum pressure during heating was 6.57e-6 Torr.

Current pressure 3.00e-6Torr


Wednesday, November 07, 2018, 18:37

IGP1 = 9.7e-7 Torr

 TGHT = -2 A/min to 0A

TBHT = -1 A/min to 0A 


 Thursday, November 08, 2018, 16:16

EVAP1 was vented with Ar, and target was transferred to glove box.

The mass of the loaded graphite insert changed to 26.854 g

That is a difference of 0.075 g

The tantalum container "cathode" crystalized (see fig)

The rest of the tantalum container did not change.

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