Marla Cervantes wrote: |
Marla Cervantes wrote: |
Tuesday, October 30, 2018, 10:12
A new LP-SIS was coated and syntered (e-log 420 Evaporator_2)
The container was loaded with a graphite insert loaded with UCx
Graphite insert + UCx mass = 26.927 g
A current of 440 A TGHT and 230 A TBHT will be inputed to the contianer
IGP1 = 8.72e-7 Torr
The current was tapped manually to 440 A TGHT and 230 A TBHT (see fig. Heating test)
Maximum pressure during heating = 1.7e-3 Torr.
Target will stay at maximum current for 1 week.
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Wednesday, October 31, 2018, 10:09
The current tripped off, around 5:00 am, the pressure was below 1e-5 Torr (see fig. current-trip_off).
On a previous test, we measured the maximum temperature of the power supply = 33.3 C (e-log 227).
Power supply overheating doesn't seem to be the problem.
EPICS windows are half withe and not answering correctly.
Also, TBHT says that IGP1 < 500 mTorr, and its interlock needs reset (see figure EPICS).
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Wednesday, October 31, 2018, 15:20
The problem was reported to controls, it will be also reported to power supply group.
In the meantime, the target will be ramp-up again with the auto ramp at:
TGHT = 20 A/min to 440 A
TBHT = 10 A/min to 230 A
The pressure before heating is 4.07e-7 Torr
Wednesday, October 31, 2018, 19:24
The maximum pressure during heating was 6.57e-6 Torr.
Current pressure 3.00e-6Torr
Wednesday, November 07, 2018, 18:37
IGP1 = 9.7e-7 Torr
TGHT = -2 A/min to 0A
TBHT = -1 A/min to 0A
Thursday, November 08, 2018, 16:16
EVAP1 was vented with Ar, and target was transferred to glove box.
The mass of the loaded graphite insert changed to 26.854 g
That is a difference of 0.075 g
The tantalum container "cathode" crystalized (see fig)
The rest of the tantalum container did not change. |