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Entry  Thursday, February 18, 2016, 15:42, Laura Lambert, UC2, 41077-1, LP-SIS, In progress, Conditioning UCx#15 
    Reply  Friday, February 26, 2016, 10:27, John Wong, UC2, 41077-1, LP-SIS, In progress, Conditioning UCx#15 
       Reply  Monday, February 29, 2016, 16:16, Laura Lambert, UC2, 41077-1, LP-SIS, Done, Conditioning UCx#15 UCx_15.jpg
Message ID: 127     Entry time: Monday, February 29, 2016, 16:16     In reply to: 126
Author: Laura Lambert 
Target Material: UC2 
Target Oven W.O#: 41077-1 
Source: LP-SIS 
Status: Done 
Subject: Conditioning UCx#15 

John Wong wrote:

Laura Lambert wrote:

 Thursday, February 18, 2016, 15:34

Target container was previously coated with TaC spray and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block - same method as for sintering TaC coating [new wrapping method-see elog112 eva2].

The target consists of 244 discs of UCx with 7.8cm in length.

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open

The chamber is currently pumping down.

TGHT will be ramped up to 520A at 0.1A/min

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


 Friday, February 19, 2016, 08:28

IG1 = 4.7e-6 Torr

Tapped up manually to 35A.

Waited ~1hr, vacuum stable

IG1 = 3.8e-6 Torr.

Initiating auto-ramp.


 

 Friday, February 26, 2016, 10:26

Target has been heated at 520A for 10 hrs.

Vacuum at 5.3e-6 Torr. 

Initiated cool down at 1A/min. 

Remember to vent with Ar. 


 

 Monday, February 29, 2016, 16:15

Vented in Ar.

Target removed from evap1 this morning.

Currently sitting in glovebox.

Weird red discharge on the end of the right side, inside the container [wrt ionizer tube into page] - same side with no endcap during carbonization.

Materials look good, both endcaps inserted.

Rh foil still needs to be implanted.


 Wednesday, March 02, 2016, 10:13

The discoloration appears to be a simple change in the morphology of the TaC coating, future tests would need to be done to confirm this estimation.

This should not effect the container/ target.

See photo attached.

Attachment 1: UCx_15.jpg  1.246 MB  Uploaded Wednesday, March 02, 2016, 10:14  | Show | Show all
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