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Message ID: 9     Entry time: Friday, June 17, 2011, 11:58
Author: John Wong 
Target/No.#: UCx (flakes) 
Source: LP-SIS 
Station:  
Module:  
Target Oven W.O#:  
Heat Shield W.O#:  
Status: Problems/Solutions 
Subject: Making UC2 flakes (stock# 2011_A & _B) 

Fri Jun 17 10:28:47 2011

First batch of UO2/C mixture of carbonization (Stock# 2011_A):   

UO2 used = 50.120g (left overs + container = 411.23g)

C(grv) used = 10.653g (or 21.25% w/w)

Mass of organics = 4.842g (or 9.66% w/w) 

Mass of dried cast = 47.420g 

Waste collected in jar = 18.195g (including UO2, C and Org) 

Waste accountable for UO2 = 12.57g

The carbonization process started from May 26 to June 4 (9 days).  

See attachment #1 and #2 for the striptools during the UO2/C carbonization

Total Mass UC2 flakes = 35.310g 


 Fri Jun 17 11:56:15 2011

Attempted to make the second batch of UO2/C mixture of carbonization on June 13, but it failed.  The milling jar gasket seal partially came out during the high speed milling.  As a result, the UO2/C mixture squirted out and contaminated the planetary mill (See attachment #3 & #4).  RPG and all other groups were informed.  The planetary mill and the lab were properly cleaned up (see attachment #5), no activities were found after the cleaning.  Attachments #6, #7, #8 are some of the discussion about the UO2 spill.  

All the UO2 taken out from the container (50.23g) is accountable for waste.  

 


 June 28, 2011 - Re-making 2nd batch of UO2/C mixture was successful.  

Stock#2011_B:

UO2 used = 50.29g

C(grv) used = 10.0g 

Mass of Organics = 4.84g 

Mass of Dried green = 71.96g (the cast was let dry over night <24hrs due to time restriction.  It might not be completely dried as a result of such heavy mass remained.  However, the UO2 waste was very minimum, <5.0g) 

Total Mass UC2 flakes = 56.853g 

 


 

 

 

 

 

Attachment 1: UO2_C_IG1_CG2_2011_A.jpg  101 kB  | Show | Hide all
Attachment 2: UO2_C_TGHT_IG1_2011_A.jpg  85 kB  | Show | Hide all
Attachment 3: UO2_mill_spill_01.png  440 kB  Uploaded Friday, June 17, 2011, 13:13  | Show | Hide all
Attachment 4: UO2_mill_spill_02.png  243 kB  Uploaded Friday, June 17, 2011, 13:13  | Show | Hide all
Attachment 5: UO2_spill_cleanup.png  457 kB  Uploaded Friday, June 17, 2011, 13:17  | Show | Hide all
Attachment 6: UO2_spill_discussion_01.png  65 kB  Uploaded Friday, June 17, 2011, 13:29  | Show | Hide all
Attachment 7: UO2_spill_discussion_02.png  106 kB  Uploaded Friday, June 17, 2011, 13:29  | Show | Hide all
Attachment 8: UO2_spill_discussion_03.png  60 kB  Uploaded Friday, June 17, 2011, 13:29  | Hide | Hide all
UO2_spill_discussion_03.png
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