Fri Jun 17 10:28:47 2011
First batch of UO2/C mixture of carbonization (Stock# 2011_A):
UO2 used = 50.120g (left overs + container = 411.23g)
C(grv) used = 10.653g (or 21.25% w/w)
Mass of organics = 4.842g (or 9.66% w/w)
Mass of dried cast = 47.420g
Waste collected in jar = 18.195g (including UO2, C and Org)
Waste accountable for UO2 = 12.57g
The carbonization process started from May 26 to June 4 (9 days).
See attachment #1 and #2 for the striptools during the UO2/C carbonization
Total Mass UC2 flakes = 35.310g
Fri Jun 17 11:56:15 2011
Attempted to make the second batch of UO2/C mixture of carbonization on June 13, but it failed. The milling jar gasket seal partially came out during the high speed milling. As a result, the UO2/C mixture squirted out and contaminated the planetary mill (See attachment #3 & #4). RPG and all other groups were informed. The planetary mill and the lab were properly cleaned up (see attachment #5), no activities were found after the cleaning. Attachments #6, #7, #8 are some of the discussion about the UO2 spill.
All the UO2 taken out from the container (50.23g) is accountable for waste.
June 28, 2011 - Re-making 2nd batch of UO2/C mixture was successful.
Stock#2011_B:
UO2 used = 50.29g
C(grv) used = 10.0g
Mass of Organics = 4.84g
Mass of Dried green = 71.96g (the cast was let dry over night <24hrs due to time restriction. It might not be completely dried as a result of such heavy mass remained. However, the UO2 waste was very minimum, <5.0g)
Total Mass UC2 flakes = 56.853g
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