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Message ID: 694     Entry time: Thursday, June 12, 2025, 12:35
Author: Sophie Worsley 
Target Material: TaC 
Target Oven W.O#: 41882-2 
Source: TARGET BOAT 
Status: Done 
Subject: TaC Diffusion Barrier Batch 1 

 Thursday, June 12, 2025, 12:33

A boat wrapped in 3 Ta heatshields

Sintering S1.1s, S2.1s, bare Ta x2 (S0.1s)

Vacuum IGP1 initial = 6.76 e-7 Torr

Target temperature on OMEGA= 1800-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final TGHT current= ~420A (adjustable)

 1A/min  to =400 A TGHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr


 Friday, June 13, 2025, 08:53

Set final value (A) to 400A

Set current increments (A) to 1A/min


Friday, June 13, 2025, 14:48

Slight increases in pressure apparent in graph - small peaks appeared


Friday, June 13, 2025, 16:00

Heating ramp stalled around 1760 C and 402A, started manually increasing to 1785 C and 410A


Friday, June 13, 2025, 16:10

 Reached 1785 C and 410A


Friday, June 13, 2025, 20:12

OMEGA at 1785 C

Started rampdown @-2A/min

 

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