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Message ID: 680     Entry time: Thursday, January 30, 2025, 09:21
Author: Darwin Ortiz Rosales 
Target Material: Empty 
Target Oven W.O#: 45447-30 
Source: HP-SIS 
Status: In progress 
Subject: TaC coating sintering 

Thursday, January 30, 2025, 09:17

Left to pump down on previous night

The coated container was wrapped in 4 Ta foil heatshields.

Vacuum IGP1 initial =8.1 e-06 Torr

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~500A (adjustable)

Heating autoramp starged at 0.5A/min(1A/120s) to 60A on both TGHT and TBHT

Then at 0.5A/min  to 90 A, both TGHT and 230A TBHT

When pressure stable will ramp at 2A/min to ~500A on TGHT and 230A on TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr


Thursday, January 30, 2025, 09:20

currently ramping to 90A


Thursday, January 30, 2025, 12:30

Ramping to 120A @ 0.5 A/min


Thursday, January 30, 2025, 13:59

Ramping to 140 A at 1A/min (to check pressure change.  So far with slower heating, pressure has not spiked very high).

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