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Entry  Thursday, July 25, 2024, 15:46, Angelina Chen, np-Ta, , TARGET BOAT, In progress, Carbonization of Heat Stabilized np-Ta Fibres Disk (1st Attempt) 
    Reply  Friday, July 26, 2024, 10:05, John Wong, np-Ta, , TARGET BOAT, Done, Carbonization of Heat Stabilized np-Ta Fibres Disk (1st Attempt) Screenshot_2024-07-26_170518.pngScreenshot_2024-07-28_112630.pngScreenshot_2024-07-31_112557.pngScreenshot_2024-07-31_171808.png
Message ID: 666     Entry time: Thursday, July 25, 2024, 15:46     Reply to this: 667
Author: Angelina Chen 
Target Material: np-Ta 
Target Oven W.O#:  
Source: TARGET BOAT 
Status: In progress 
Subject: Carbonization of Heat Stabilized np-Ta Fibres Disk (1st Attempt) 

 Thursday, July 25, 2024, 15:18

Target container consists of two np-Ta fibres disk samples. Both disks are made from heat stabilized np-Ta fibres (150 C for 17 hours) and were pressed at 8 tons / 300 MPa.

Sample 1 was made from np-Ta fibres spun using Dope solution #1. Sample 1 disk has an average thickness of 0.727 mm and a diameter of 17.113 mm. Mass of the green sample 1 disk is 0.1957 g. 

Sample 2 was made from np-Ta fibres spun using Dope solution #6. Sample 2 disk has an average thickness of 0.688 mm and a diameter of 17.123 mm. Mass of the heat stabilized fibres used to make the green sample 2 disk is 0.1860 g. Mass loss from pressing the heat stabilized fibres was virtually zero. Therefore, although the mass of the green sample 2 disk was not measured, it can be extrapolated to be 0.1860 g. 

Target container was wrapped with Ta foil. Each sample disk was wrapped in graphite foil and placed inside the target container horizontally near the center. 

Omega slope was initially set to 0.980. After reviewing previous logbook on np-Ti (e-log ID#633), changed the Omega slope to 0.990. 

Chamber is currently being pumped down. The current reading (as of 15:40) is 4.70e-05 Torr. 

Two heating schedules will be tested. Heating schedule 1 entails heating both sample disks at ~1000 C until the pressure reaches below 1.00e-06 Torr. Once heating schedule 1 is completed, sample 1 will be removed. Heating schedule 2 entails heating sample 2 to ~1800 C until the pressure reaches below 1.00e-06 Torr. TGHT is estimated to be approximately 440A/7.6V to reach 1875 C (348A/5.8V to hold temperature at 1600 C). Refer to e-log ID#605. 


 

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