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Message ID: 656     Entry time: Thursday, February 29, 2024, 07:40
Author: Darwin Ortiz Rosales 
Target Material: TiC 
Target Oven W.O#:  
Source: LP TUBE 
Status: Done 
Subject: 240228TiC conditioning 

Thursday, February 29, 2024, 07:40

Ta container tube, wrapped in 4 Ta foil heat-shields, and loaded with _________ D shaped discs in a 12mm graphite cartridge with usable 11mm

conditioning tube WO = 44692-13

End-caps on the graphite cartridge have holes for outgassing.  One spring each end in the Ta container

initial heating @ 2A/min to 85 A then 2A/min to 120A TGHT

OMEGA slope = 0.99

Vacuum limits up to 400A: 5.0e-04 Torr -- 1.0e-02 Torr


Thursday, February 29, 2024, 07:43

Initial IGP1=  9.31e-7 Torr


Thursday, February 29, 2024, 17:43

Temperature profile suggests 1900 C at 400A.  Now at 400A.  Will keep at this current for 4 hours.

manually ramped the last few amps.

TGHT= 400A, 7.3 V OMEGA = 1901C


Thursday, February 29, 2024, 22:20

IGP1=2.1e-6 Torr

started ramping down at -2A/min

 

Attachment 1: TiC_240228_Conditioning_Temperature_vs_Current.png  26 kB  Uploaded Friday, March 01, 2024, 10:13  | Show | Show all
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