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Message ID: 485     Entry time: Friday, May 29, 2020, 10:26
Author: Marla Cervantes 
Target Material: Empty 
Target Oven W.O#: 43044-8 
Source: LP-SIS 
Status: Done 
Subject: TaC coating/sintering  

 Friday, May 29, 2020, 08:52

Ta tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature= 1900 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 was pumped down

Good vacuum= 3.00 e-5 Torr

Bad vacuum = 5.00 e-5 Torr

Ramped TGHT and TBHT to 40A at 0.5A/min

Initial IGP1 = 3.7e-7 Torr


Friday, May 29, 2020, 10:23

Autoramp deliver 40 A

TGHT = 0.47 V, 40.72 A

TBHT = 0.5 V, 38.78 A

IGP1 = 4.5 e-6 Torr and going down

Autoramp TGHT and TBHT at 1A/min to 400A and 230A respectively.


Friday, May 29, 2020, 11:27

Autoramp was stopped at 70 A, since pressure kept increasing, current was manually decreased to 65 A in both TGHT and TBHT.

The system will remain at current conditions until pressure reduce.


Friday, May 29, 2020, 12:44

 Autoramp TGHT and TBHT at 1A/min to 400A and 230A respectively.


Saturday, May 30, 2020, 00:23 

Autoramp deliver 400 A at TGHT and 230 A at TBHT

TGHT = 7.8 V, 453.9 A

TBHT = 4.21 V, 232.9 A

IGP1 = 9.7 e-6 Torr and going down

Omega = 1893 degC

Autoramp TGHT and TBHT at -1A/min to 400 A

Initiating auto-cool at -2.0A/min and -1.0A/min for the TGHT and TBHT respectively

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