Logbooks Lab Maintenance Evaporator_1 Evaporator_2 Laser cutter Target Production Test-Stand RH-ISAC RH-Cyclotron RH-Meson Hall RH-Beamlines RH-ARIEL
  Evaporator_2  Not logged in ELOG logo
Entry  Monday, September 24, 2012, 15:12, Nikita Bernier, TaC, , , Done, Sintering Ta foil with TaC coating striptool1.PNG
    Reply  Monday, September 24, 2012, 18:09, Nikita Bernier, TaC, , , Done, Sintering Ta foil with TaC coating striptool2.PNGstriptool4.PNGstriptool5.PNG
       Reply  Wednesday, September 26, 2012, 15:06, Nikita Bernier, TaC, , , Done, Sintering Ta foil with TaC coating striptool6.pngSans_titre2.png
Message ID: 47     Entry time: Monday, September 24, 2012, 18:09     In reply to: 46     Reply to this: 48
Author: Nikita Bernier 
Target Material: TaC 
Target Oven W.O#:  
Source:  
Status: Done 
Subject: Sintering Ta foil with TaC coating 

Nikita Bernier wrote:

 Monday, September 24, 2012, 15:01

The target boat with TaC coating is being used again. The inside of the boat is covered with a 0.002 inches thick Ta foil with TaC coating, wrapped with a 0.002 inches thick Ta foil.

Chamber was pumped down to 6e-6 Torr before the Heat Shield cooling water valve was opened. A small vacuum bump was detected (See attachment #1). It is not clear if it was caused by a water leak or not.

After consulting with Peter, I will wait for the vacuum to be below e-07 Torr before turning the target heater on.

 

 

 

 Monday, September 24, 2012, 18:02

The vacuum was stable until 1e-06 Torr. The target heater was turned on and tapped up to 60 A (0.8 V). 

Evaporator #2 is now auto-ramping overnight at 0.2 A/min, up to 800-850 A, with the maximum voltage limited at 14 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum). 

 

 Tuesday, September 25, 2012, 15:11

Sintering process is going smoothly. See Attachment 1. The auto-ramping was increased to 1 A/min up to 800-850 A.

 

 

Tuesday, September 25, 2012, 16:11 

And the voltage limit was increased to 18 V ! See Attachment 2.

 

 Tuesday, September 25, 2012, 19:13

Around 806 A (readback), voltage increased more quickly than the current. It seems like resistance is building up. After reaching 836 A (readback), the current was tapped down to 800 A (readback)/ 816 A (setting) in an effort to save the Ta boat. See Attachment 3. The current will stay at 800 A for ~4 hours before ramping down.

 

 

Attachment 1: striptool2.PNG  22 kB  Uploaded Tuesday, September 25, 2012, 16:13  | Hide | Hide all
striptool2.PNG
Attachment 2: striptool4.PNG  20 kB  Uploaded Tuesday, September 25, 2012, 17:14  | Show | Hide all
Attachment 3: striptool5.PNG  18 kB  Uploaded Tuesday, September 25, 2012, 20:20  | Show | Hide all
ELOG V2.9.2-2455