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Message ID: 462     Entry time: Monday, October 07, 2019, 09:18
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#:  
Source: TARGET BOAT 
Status: In progress 
Subject: Sintering TaC coating on endcaps and springs 

Friday, October 04, 2019, 11:37

Each endcap is separated with a disc of graphite foil and rolled into packs of 5 within a foil envelope in a target boat.

There are also 3 coated springs, one in between endcaps and two on either end

The boat is wrapped with 2-layers of Ta heatshields.

Chamber pumping down

OMEGA slope = 0.99

Will Tap TGHT up manually to 40 A then autoramp to 400A at 1A/min.

Final desired temperature on OMEGA (tap)= 1800C


Monday, October 07, 2019, 09:08

Sunday night heating started at 1A/ min on TGHT to 54 A

heating paused for 1 hour to allow IGP1 to equillibrate.  Then restarted at 1A/min to 400A as planned. 

This morning IGP1 = 1.3e-06 Torr

TGHT = 401A, 4.2V

OMEGA = 1550 C


Monday, October 07, 2019, 09:36

manually tapping to 1800 C


Monday, October 07, 2019, 14:09

Temperature @ ~1800 for 3.5 hours

TGHT= 495.4, 9.2 V

IGP1= 1.1e-06 Torr Pressure Steady there begin cooling

Cooling @ -2A/min

 

 

 

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