Thursday, June 6, 2019, 16:43
A graphite insert with tantalum wires in its caps was loaded in a tantalum tube.
The system will be heated to 2000 C again (see elog 446)
Currently the chamber is being evacuated.
Friday, June 7, 2019, 16:40
Autoramp was set to 450 A at 1A/min to reach 2000 C
The temperature will be hold at 2000 C for a 4 days.
Tuesday, June 11, 2019, 16:46
Autoramp is set to -2 A/min to 0 A
Wednesday, June 12, 2019, 17:01
The tube present sever crystallization but is not broken and has some resistance against pressure. |