Tuesday, April 30, 2019, 09:33
Container was coated with TaC and wrapped with 2 Ta heat shields.
Desired temp = 1900 C, Omega slope set = 0.990, Auto ramping TGHT at 1A/min to reach 400A, TGHT will be tapped up accordingly to reach desired Temp.
TBHT will be set fixed at 230A (max). TBHT at 1A/min to reach 230A.
Good vac at 3.0e-5 Torr
Bad vac at 5.0e-5 Torr.
Chamber is currently being pumped down (since yesterday evening).
Tuesday, April 30, 2019, 10:25
Current pressure at IGP1 = 5.17e-7 Torr
Manual tapping to 40A on TBHT and TGHT
TBHT 38.59A, 0.43V
TGHT43.69, 0.23V
waiting for pressure to stabilize.
Tuesday, April 30, 2019, 15:15
Current pressure IGP1= 5.29e-07 Torr
Auto ramping TGHT at 1A/min to reach 400A, and TBHT at 1A/min to reach 230A.
Wednesday, May 01, 2019, 08:41
Target current of 400A reached around 00:19 am
Will tap up to 444A on TGHT as projected from plot of temperature vs current (attachment 1)
Current IGP1=5.91e-07 Torr
Wednesday, May 01, 2019, 09:54
At 444A 1900C not reached. Continue tapping to 1900C (attachment 2)
1900 C reached at 459 A on THGT.
will leave at 1900C for 4 hours.
Wednesday, May 01, 2019, 14:21
IGP1= 6.7e-7 Torr
After 4.5 hours, TGHT was ramped down @ 2A/min and TBHT @1A/min overnight
Thursday, May 02, 2019, 10:46
Vented Evap 2 and removed the target container. |