Friday, January 18, 2019, 15:00
Container was coated with TaC and wrapped with 3 Ta heat shields.
Desired temp = 1900 C, Omega slope set = 0.990, Auto ramping TGHT at 1A/min to reach 400A, TGHT will be tapped up accordingly to reach desired Temp.
TBHT will be set fixed at 230A (max). TBHT at 1A/min to reach 230A.
Good vac at 3.00-5 Torr
Bad vac at 5.0e-5 Torr.
Chamber is currently being pumped down. Sintering will proceed next week.
Monday, January 21, 2019, 10:17
Current pressure at IGP1 = 1.31e-7 Torr
Manual tapping to 50A on TBHT and TGHT
TBHT 38.75A, 0.41V
TGHT 37.5A, 0.07V
waiting for pressure to stabilize.
pressure IGP1 8.0 e-7 Torr
Auto ramping TGHT at 1A/min to reach 400A, and TBHT at 1A/min to reach 230A.
Tuesday, January 22, 2019, 09:34
TGHT reached 400A , 1800 C, however temperature dropped to 1785 C.
TGHT increased to 444A manually. Temperature stabilized at 1880 C.
After 10 hours, TGHT was ramped down @ 2A/min and TBHT @1A/min
Tuesday, January 22, 2019, 14:36: Evap 2 PS off. Turbo off (Around 14:10) Vented Evap 2 and removed the target container with Darwin. - AS.
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