Monday, August 20, 2018, 17:58
14.9 g of np-SiC fibrous target discs are loaded into the container (previously coated with TaC and sintered, see elog ID 414).
Total loaded length 9.5 cm.
A 1.5" width graphite sheet is used as under layer to prevent TaC diffused to the discs; this was observed during the heat treatment, (see dropbox SEM images).
Both end caps are in. With ionizer pointing out, right cap is expended BUT NOT left cap - will need to expend this after the conditioning.
No Ta heat-shield is used.
Final conditioning temperature: 1500 C (As per e-log 414, TGHT = 450A/7.31V, 3.28kW)
Keeping TBHT at 0A for now - will ramp up after TGHT reach to the desired temperature.
OMEGA slope set at 0.99
Good vac = 3.0e-5 Torr,
Bad vac = 5.0e-5 Torr.
Tuesday, August 21, 2018, 10:24
Pressure at 1.2e-6 Torr.
Initiated autoramping at 2A/min for TGHT to reach 400A - monitoring temp and vacuum.
TBHT set at 10A.
Tuesday, August 21, 2018, 15:13
Temp reached to 1350C. TGHT at 400A/6.7V. Pressure at 1.9e-6 Torr after holding at the temp for 100 min.
Tuesday, August 21, 2018, 15:28
Tapped up TGHT to 450A/7.8V (3.5kW). Temp measured at 1465 +/- 5 C. Pressure coming down from 3.5 e-6 Torr.
Tuesday, August 21, 2018, 15:32
Tapping up TBHT to 230A
Tuesday, August 21, 2018, 16:25
TBHT at 230A/4.33V. Pressure started to increase from 150A, and reached to 3.3e-6 Torr after TGHT reached to the setting.
Temperature measured at 1475 C +/- 5C. Holding at this temperature until vacuum comes to stabilization (est.2-3 hours)
Tuesday, August 21, 2018, 16:45
Checked with Mikron (slope set at 0.99); temp on left end-cap measured at 1490 +/- 20C (that's close enough). Temp on ionizer tube about 1900C
Tuesday, August 21, 2018, 22:12
Pressure at 1.7e-6 Torr. Temp holding at 1480C, TGHT at 450/7.7V, TBHT 230A/4.27V.
Cooling down at 2A/min for TGHT and 1A/min for TBHT
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