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Message ID: 37     Entry time: Sunday, July 22, 2012, 20:51
Author: John Wong 
Target Material: NiO 
Target Oven W.O#: 38481-7 
Source: HP-FEBIAD 
Status: Done 
Subject: Sintering NiO#1 

 Sunday, July 22, 2012, 20:30

The NiO target materials were loaded into the container today.  

Total discs = 500, (10 discs/pack) 


length (after loaded) = 9.0cm 

Target container is wrapped with Ta-heat shields, and will be removed after the sintering process. 

One regular end cap is inserted (with Ni-foil inserted as a divider).  The caps, however, are very loose (tried 2 caps and still loose).  Hopefully the thermo diffusion bonding will seal the cap... 

The other end is inserted with a D-cap for out-gassing proposes, and will be replaced with the regular end-cap after the process. 

(see attachment#1)


Sunday, July 22, 2012, 20:48 

The camber has been pumped down and currently IG1=1.3e-6 Torr.

The HS cooling water was turned on and no leaks were detected.  

TGHT and TBHT were stepped up to 50A. 

Auto-ramping is initiated at 0.2A/min for TGHT max = 250A, TBHT max = 230A. 


 Thursday, July 26, 2012, 23:31

TGHT and TBHT have reached to 250A (local @ 242A/2.88V) and 230A, respectively, and have stayed for ~4hrs (see attachment#2)  

Currently, IGP1 = 4.9e-7 Torr, IGP2 = 3.5e-7 Torr, CG1B = 13mTorr. 

Initiating auto-cool down at 2A/min.  


 Monday, July 30, 2012, 15:11

The chamber was vented and the target was removed.

There was significant condensation oily fluid coated Cu-heatshield lid and around the ionizer opening.

Overall, the target looks very good.  The NiO target material was nicely sintered.  No shrinkage or loose particles were observed (see attachment #3).

The endcap, however, was not properly fitted and it just fell off, (see attachment #4). 

Both ends of the target are currently opened; the expension tool for the endcap is in order and hopefully this will solve the problem.

The target is being stored in the fumehood


 

Attachment 1: NiO#1_sinteringevap2.png  476 kB  | Show | Hide all
Attachment 2: NIO#1_TGHT_TBHT_250_220.png  22 kB  Uploaded Friday, July 27, 2012, 00:36  | Hide | Hide all
NIO#1_TGHT_TBHT_250_220.png
Attachment 3: Sintered_NiO.GIF  66 kB  Uploaded Monday, July 30, 2012, 16:16  | Show | Hide all
Attachment 4: Endcap.GIF  99 kB  Uploaded Monday, July 30, 2012, 16:18  | Show | Hide all
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