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Entry  Wednesday, June 14, 2017, 15:51, Laura Lambert, SiC, 40282-4, TARGET BOAT, In progress, Sintering SiC pellets 
    Reply  Friday, June 16, 2017, 10:42, Marla Cervantes, SiC, 40282-4, TARGET BOAT, Done, Sintering SiC pellets 
       Reply  Friday, June 16, 2017, 15:14, Laura Lambert, SiC, 40282-4, TARGET BOAT, Done, Sintering SiC pellets 20170619_111816.jpg20170619_111848.jpg
Message ID: 375     Entry time: Friday, June 16, 2017, 10:42     In reply to: 374     Reply to this: 376
Author: Marla Cervantes 
Target Material: SiC 
Target Oven W.O#: 40282-4 
Source: TARGET BOAT 
Status: Done 
Subject: Sintering SiC pellets 

Laura Lambert wrote:

 Wednesday, June 14, 2017, 15:49

Pellets previously made by Marla and weighed.

Pellets are placed inside a small graphite sample tube.

Graphite sample tube loaded with pellets is loaded into a previously TaC coated boat.

Boat is wrapped with 3x Ta heat shields.

Loaded into evap2.

Chamber currently pumping down.


 Thursday, June 15, 2017, 11:24

HS water valves were opened this morning, no leaks detected.

Tapped up manually to 50A, 0.44V

Vacuum currently rising starting to settle.

IGP1 = 1.51e-6 Torr.

One vacuum stabilizes will initiate auto ramp at a rate of 1.0 A/min up to a final set point of 150 A.

Final desired temperature of 1800C.


 

 Friday, June 16, 2017, 10:37

IGP1 = 7.91e-7 torr.

TGHT = 167 A, 2.3 V.

Tapped up manually to 350A yesterday, remained there overnight.

IGP1 = 4.55e-7 torr

TGHT=350 A, 5.6 V,

Changed slope to 0.98

Checked temperature readings with mikron to confirm slope

Mikron LS = 1260C, RS=1290C

OMEGA= 1295C

Initiating auto ramp at 1.0A/min to a final set point of 450A.

Final desired temperature of 1600C (no longer need to go to 1800C).

*note: graphite sample tube has graphite endcaps inserted


 

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