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Message ID: 371     Entry time: Tuesday, May 16, 2017, 11:57
Author: Laura Lambert 
Target Material: SiC 
Target Oven W.O#: 41369-10 
Source: HP-FEBIAD-CTL 
Status: Done 
Subject: Sintering SiC#36 

 Tuesday, May 16, 2017, 10:56

Target container contains 460 discs of SiC 

Target packed length = 17cm. 

Mass of SiC(green)  = 55.5152g

Consists of 4 packs of 5 and 440 singles.

Container is wrapped with 1x heatshield around each side of cooling fins; no end caps are inserted yet - coated spring inserted both sides to hold discs in place.

Sintering temp = 1800C

Chamber is currently being pumped down. 


 Tuesday, May 16, 2017, 15:27

HS water valves turned on, no leaks detected.

Tapped up manually to 30A

Waited ~30min , vacuum stable.

IGP1 = 8.25e-6 Torr

Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

TGHT max = 400A.  TBHT max at 230A. 

Slope on OMEGA = 1.09 [see elog i.d. # 370 for reasoning behind OMEGA slope choice]


 Friday, May 19, 2017, 10:13

TGHT = 250A, 3.11V     DR = 248A, 3.3V

TBHT = 137A, 1.68V     DR = 140A, 1.73V

OMEGA = 1100C

IGP1= 6.9e-6 Torr     DR = 1e-5mbar

IGP2 = 5.9e-6 Torr     DR = 6.45e-6 Torr

Vacuum stable.

Increasing ramping rate to 1.0A/min and 0.5A/min for the TGHT and TBHT respectively.


 Friday, May 19, 2017, 10:33

Change in plan and switching ramping rate to 0.5A/min and 0.2A/min for the TBHT and TGHT respectively.


 Friday, May 19, 2017, 14:49

TGHT = 400A, 5.46

TBHT = 200A, 2.66

IGP1 = 2.7e-5 Torr

IGP2 = 2.2e-5 Torr

OMEGA = 1200C

Increasing max setpoint for TGHT to 550A

Decreasing ramping rate to 0.2A/min and 0.1A/min for over the weekend.


 Tuesday, May 23, 2017, 09:23

TGHT = 550A, 8.37

TBHT = 230A, 3.14

IGP1 = 1.6e-7 Torr

IGP2 = 1.6e-7 Torr

OMEGA = 1570C

Increasing max setpoint for TGHT to 600A at rate to 0.5A/min


 Tuesday, May 23, 2017, 11:45

TGHT = 600A, 9.36

IGP1 = 3.5e-7 Torr

IGP2 = 3.8e-7 Torr

OMEGA = 1675C

Increasing max setpoint for TGHT to 625A at rate to 0.5A/min


 Tuesday, May 23, 2017, 13:03

TGHT = 625A, 9.80V

IGP1 = 5.2e-7 Torr

IGP2 = 5.7e-7 Torr

OMEGA = 1715C

OMEGA no longer valid around 640A as temperature drops instantly after tapping up.

Could be due to target movement at high temperature.

No obvious window coating.

Tapped up manually to 660A, 10.49V.

Will remain at max setpoint overnight.


 Wednesday, May 24, 2017, 11:13

TGHT = 660A, 10.74V

TGHT power supply = 662A, 11.00V

TBHT = 230A, 3.16V

TBHT power supply = 232A, 3.25V

IGP1 = 4.2e-7 Torr

IGP1 direct readout = 5.9e-7 mbar

IGP2 = 4.6e-8 Torr

IGP2 direct readout = 5e-7 Torr

Evap2 reached max setpoint yesterday afternoon.

Window has thiny coating - see attached photo.

OMEGA = 1800

MIKRON = ~1800

Initiating auto cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Wednesday, May 24, 2017, 11:36

Change of plan.

TGHT = 620A, TBHT = 210A

Ramping back-up to max setpoints and will remain at those points until vacuum starts to decrease more.


 Friday, May 26, 2017, 15:24

IGP1 = 2.1e-7 Torr

IGP2 = 2.2e-7 Torr

TGHT = 660A, 10.72V

TBHT = 230A, 3.21V

All windows coated.

Remained at max setpoints for ~3.5days.

Conditioning process complete.

Initiating auto-cool at 2A/min and 1A/min for the TGHT and TBHT respectively.


 Tuesday, May 30, 2017, 14:41

Target vented in air and removed from evap2

Looks good!

Endcaps inserted and expanded.

See photos attached.


 

Attachment 1: window_at_max_setpoint_after_1_day.jpg  1.495 MB  Uploaded Wednesday, May 24, 2017, 12:41  | Show | Hide all
Attachment 2: 20170530_094047_Richtone(HDR).jpg  1.532 MB  Uploaded Tuesday, May 30, 2017, 15:41  | Show | Hide all
Attachment 3: 20170530_094118_Richtone(HDR).jpg  1.668 MB  Uploaded Tuesday, May 30, 2017, 15:42  | Show | Hide all
Attachment 4: 20170530_094137_Richtone(HDR).jpg  2.100 MB  Uploaded Tuesday, May 30, 2017, 15:42  | Show | Hide all
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