Thursday, May 11, 2017, 11:21
Turns out SiC HP-FEBIAD that has finished conditioning is loaded in the wrong container and it should be a SiC HP-FEBIAD cold transfer line...so rush on new target.
Container coated with TaC using new method: Ends taped off, with liquid poured in and swirled around entire container, then poured back out - 'flushing technique'
Container is wrapped with 1x heatshield around each side of cooling fins, not incl center block.
Loaded into EVAP2 and currently pumping down.
Thursday, May 11, 2017, 13:40
IGP1 = 1.85e-6 Torr.
HS water valves opened.
No leaks detected.
Tapped up manually to 35A.
Vacuum stable.
IGP1 = 3.2e-6 Torr
IGP2 = 4.2e-6 Torr
Initiated auto ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.
Final setpoints for TGHT = 450A and TBHT = 230A, with final desired temp of 1900C
OMEGA slope = 0.98
Friday, May 12, 2017, 07:57
IGP1 = 4.3e-7 Torr.
IGP2 = 4.4e-7 Torr
TGHT = 233A, 2.8V
TBHT = 130A, 1.6V
Increasing ramping rate to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Friday, May 12, 2017, 08:54
Comparing direct readouts with epics:
IGP1: direct = 1.9e-6 Torr; epics = 1.3e-6 Torr
IGP2: direct = 1.55e-6 Torr; epics = 1.4e-6 Torr
TGHT: direct = 320A, 4.38V; epics = 321A, 4.19V
TBHT: direct = 181A, 2.40V; epics = 178A, 2.34V
Friday, May 12, 2017, 10:28
IGP1 = 1.07e-6 Torr
IGP2 = 1.15e-6 Torr
TGHT = 450A, 6.37V
TBHT = 230A, 3.21V
OMEGA = 1197C
Increasing max setpoint of TGHT = 700A
Friday, May 12, 2017, 13:06
IGP1 = 2.4e-6 Torr
IGP2 = 2.5e-6 Torr
TGHT = 696A, 11.21V
TBHT = 233A, 3.26V
OMEGA = 1758C
Increasing max setpoint of TGHT = 800A
Friday, May 12, 2017, 13:32
TGHT maxed out at 715A but continued ramping.
This was noticed when current set of TGHT = 750A but readout = 715A
This is due to max voltage limit = 12.0V and readout =11.58V
Increasing TGHT max setpoint to 14.0V and restarting auto ramp from 714A
Friday, May 12, 2017, 14:45
Container has reached max setpoint of ~1900C
TGHT setpoint = 775A
TGHT = 769A, 12.54V
TBHT = 233A, 3.28V
IGP1 = 2.94e-6 Torr
IGP2 = 2.99e-6 Torr
OMEGA = 1912C
Will remain at max setpoint over weekend.
See attached photos of temperature measurements using MIKRON while TGHT current set point = 770A.
Photos are not super accurate but good as a rough idea.
Ex. for left side the point in the camera is actually pointed slightly closer to the end of the container but in the photo it looks more centered.
Saturday, May 13, 2017, 10:52 by Anders
Ramping down heaters. Temp 1912 C. Vacuum IGP1 = 5.4e-7 Torr
Monday, May 15, 2017, 13:10
Vented in air and taken out this a.m.
Target container looks good.
Fully sintered coating.
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