Monday, August 08, 2016, 15:19
Previously sintered over weekend [see elog i.d 311]
Target container contains 471 discs of SiC [6 x 5 packs + 441 single discs]
Target packed length = 16cm.
Mass of 533 discs SiC(green) = 52.7172g
Container is wrapped with 3 heatshields; no end caps are inserted yet - coated spring inserted both sides to hold discs in place.
Conditioning temp = 1800C.
TGHT max = 450A. TBHT max = 230A.
Chamber is currently being pumped down.
Monday, August 08, 2016, 16:38
Target was not removed from evap2 after sintering, vented and cleaned windows only.
IGP1 = 5.5e-6 Torr
Stepped up manually to 80A, vacuum stable.
IGP1 = 3.2e-6 Torr
Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT.
Thursday, August 11, 2016, 14:14
Tues the TGHT reached ~280A via auto-ramp
Evap2 was then tapped up manually to 480A/ ~1800C
Temperature readings on OMEGA have fluctuated up and down during conditioning process which was also observed for SiC#33
Also consistent with SiC#33, a lower current was required to reach 1800C during the conditioning process compared to the sintering process.
See attached link for data.
Tuesday, August 16, 2016, 16:25
TGHT remained at 480A, 9.2V for ~7 days.
IGP1 = 6.5e-6 Torr
OMEGA = 1470C [with window coating, so temperature reading compromised]
Initiating auto cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Wednesday, August 17, 2016, 13:40
Vented in air and opened this morning.
Target broke
Target clearly heated to high.
See attached snapshot of striptool from conditioning process.
Will update later with photos of broken container
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